Die US BSA bel Te fate be) Od Peq Our Profile The company was founded in 1974 by Mr. Naresh Shah (Chalrman] BTech. Mech, IIT & MS. (USA). It started designing, manufacturing & exports of high pressure reactor, magnetic coupling, microreactors, industrial filters & heating cooling circulators with a vision to provide import substitute products in India at reasonable rates & international quality ‘Amar Equipment is a leader in pressure reactor designing & can supply the same with all desired certifications / approvals like 'S0, ASME, CE, UL etc. complying to various International safety regulations. We have over 39 years of rich experience in manufacturing ‘supplying high pressure reactorsystems globally. We have complete In-house setup well-equipped to design, manufacture & test all the ‘products & components with atest gauges, measuring instruments & machines ike *CNCturning centre ‘Cutting machines * Vertical machining centre (VMC) ‘= Rivetting machine * Conventional lathes += Drilling machines + Plasma cutting machine '*Weldingmachines Overhead Cranes, Grinding machines *=Buffing/ polishing/cleaningequipment + PMimachine sLasermarking + Packaging machines etc. Weare team of around 100 people with qualified staf, skilled workers &a core team of 15. highly siled & experienced professional engineers, equired to produce the desired quality ‘repetitively as per international quality standards & design codes, wor + Tobecomea leading global player in manufacturingall our products. * Tocontinuously upgrade the quality of our product & always offer the latest & the best * To develop & manufacture products that work virtually lifelong without maintenance. * Totry & cater to meet all customer demands & complaints, to ultimately see a delighted customer. * To make products that are technically complete, physically reliable, economically competent & ergonomically superior. cs Pioneers & largest manufacturer of high pressure reactor & magnetic drive couplings in India year after year since 39 yrs. Over 5000 successful installations world over with more than 2000 delighted customers. Exports to more than 50 countries world wide &S exclusive dealers indifferent pars of india forlocal support. The growth & success of our firm in terms (of quality, production & profitability has been positive sinceits inception, Pressure Leaf Vertical Honartal 833" Zera Holdup “70 0 250 9C Microreactors Sparkler Fiter Cooling & Heating Crevlators Continuous Fow tie Magnetic Drive Cauplings & StererTeel ‘An 180-001-2008 certified company. «= Alour pressure reactor / vessel designs areas per ASMEcodes-section VillDiv1/Div2. + Ourweldersare qualified as per ASME section IX codes for welded pressure vessels. CE marked autoclave of desired size, pressure & material can be supplied on request with EMC, LYD & P + DQ, IQ, PA, O@can be given on special request. + Most of our products comply to GMP /GMPstandards. + Explosion proof / flame proof motors, pumps, heaters, sensors & panels for hazardous area for g hydrogen. @ Management system as per DIN EN ISO 9001 : 2008 In accordance wit) TOV NORD CERT procedures lis hereby cried that AMAR EQUIPMENTS PVT. LTD. 4/6, Parmar Industrial Estate, Bail Bazar, Kale Marg, Kurla (West), Mumbai ~ 400 070, India applies a management system in ne wih the above standard for te foloing scope | Design, Manufacture and SuCc r= ‘SeNo, Description Page No. Z.__Autocave- salient features 1 2 Autoclave - applications 1 3. Material of construction (MOC) 23 4. Model no. / coding of autoclaves* 45 5, Stitred autoclave specifications {. Volume, MOC, pressures, temperatures, norales, valves, tings, body & head sealing 6 |. Head mounting style, motor & drive " 7 7 6. _Zeroleakage magnetic drive coupling & magnetically coupled ster 29 7. Stirred autoclave specifications |. Stirrer types 9 11. Heating, control panel, power supply, mounting. . 10 Ii, Stirred autoclaves- various model photographs u 8. tired autoctaves technical specifications. 2 9, GA& nozzle orientation drawing - sted autoclaves B 10. Fixed hed autoclaves- various models. rf 11, Multiple autoclave system 45 12, High throughput catalyst screening system 15 13, Bottomstired autoclave 16 14. Interchangeable tired metal autoclaves 16 15. Continuous flow stirred tank reactors (CSTR) 1s 16. Continuous flow, fixed / fluidized bed tubular reactor systern v 17. Vapour phase reactor v 18 High pressure systems for different applications 18 419, Gas induction reactors -hydrogenators / plot to plant scale pressure reactors. 13 20. Hydrogenation pilot plant / multipurpose pressure reactor 20 21. alkoxylation pilot plant / pilot plant fr styrene butadiene emulsion polymerisation. 2 22, Glass body autociaves 2 23, Interchangeable meta & glass autoclaves, 2 24, Racker / shaker hydrogenators, 23 25. _Non-stired high pressure vessels . 24 26. Acid digestion vessel 24 27. Supercritical id, CO2 system 24 28, System for hydrogen induced disbonding test 25 29. Autoclaves for corrosion testing. . 25 30. Optional accessories |. Gas pressure regulator, gas booster, gas mass flow meter / controle, digital pressure indicator / controller 26 Liquid / slurry / gas charging high pressure pot, ethylene oxide po, liquid metering pump system, auto cooling system. ...27 Cooling & heating circulator, flow control valves 28 Reflux condenser, condenser, receiver pot, back pressure regulator, pressure safety valve, chain pulley lifting system... 29, ‘cada software, liners, catalyst basket, catalyst fiers, catalyst addition device 30 I, Catalyst fitration system, catalyst slurry charging system, catch pot, vacuum pump 31 Il. Level, pH, turbidity, DO, Redox sensors, baffles, sight glas, torque sensor 32 31. Unit conversion table 32 32. Client testimoni 33 33. Some of our valued customers 3435 * Mode no. / coding of various autacave types, sits, MO, ratings, motor, heating & mounting style ete. options a ven in short to enable the user to _checkonalloptionsavaflable & wit the codes one cansendinqury/orderinshort Since development is continuous process the specifications in the catalogue can chonge without prior notice ‘Trademarks used nthe catalogue * Viton, Kare: & teflon are registered trademarks of Dupont + Grafolsreistered trademark of UCAR Carbon Co. ‘+ Monel & Inconel are registered trademark of Special Metals Corp. ‘+ Hastllo is registered trademark of Haynes International Abbreviations used inthe extalogue + QRC: Quick release coupling * NRV: Non-return valve * MOC: Matera of construction ‘+ LP: Flame proct/Explosion proof + Temp. Temperature + Pr: Pressure + @: Phase « tc iter + NA: Not applicable available ‘lithe oresureratinas aren bar whichis nearly same as kee (1 bar = 1.02 ems?)(eEneene + Stired &non-stirred reactors/pressure vessels, Sizes from 25mlto 1000Itrs. capacity. MOC $5-316/316L, Hastelloy B/C, Monel, Inconel, Nickel, Titanium, Tantalum, Zirconiumete + Max. design pressures upto 5000psig 350-bar) & temperatures upto SOO°C. Alldesigns as per ASME codes & CE certified autoclaves on request. High torque zero leakage magnetic drive coupling. Complete pilot plant wth automatic temperature, pressure, RPM, motor torque/ current, liquid & gas flow, pH, ORP, turbidity, level, controlling, autocooling system, chiller, condensor for distilation or reflux, thermicfluid heating / cooling system et. Fully automated PC controlled high pressure system / pilot plant to continuously monitor, control & record various parameters Multiple parallel 4or 6 reactors for high throughput catalyst screening /research, Gas induction reactors, Complete FLP certified / explosion proof systems suitable for group IC gases like H, Bottom stirred autoclaves. Glass-metal peek autoclaves. Interchangeable metal & glassautoclaves. Rocker / Shaker Hydrogenator. Continuous low stirred tank reactor + Fixed bed catalysttubularreactor. +» Gasrecycle vapour phase reactors. * Acid digestion vessel (ines It is used for reactions like alkylation, amination, bromination, carboxylation, catalytic reduction, chlorination, dehydrogenation, esterification, ethoxylation, halogenation, hydrogenation, methylation, nitration, oxidation, czonization, polymerization, sulphonation etc. athigh pressure / vacuum & temperature. + Toinvent new chemicals, study reaction parameters. +» Toproduce chemicalsin small quantityinbatch or continuous mode, + Forsynthesis, + Forquality control & processimprovements + Forheterogeneous mixing to carry out catalyticreactions. * Forhigh throughput catalyst screening, + Forcorrosion studies: Static, loop & electrochemical + Forreaction calorimetry. + Forsupercrtical CO, solvent extraction / reaction / drying / evaporation system + Forhydrogendisbonding test. + Soaking f diamonds preciousstones, In R&D centers, pilot plants & manufacturing faclities of fine & specialty chemicals, bulk drug (API) pharmaceuticals, dyes, intermediates, paints, oils, agrochemical, petrochemicals, petroleum etc. Industries & also in chemical engineering colleges / research institutes / defence organisations where high pressure reactions /testingiscartied out.Co Material of Construction (MOC) ‘All wetted parts are made from $5-316. Option: S5-3161, Hastelloy 8/C, Titanium, Monel, Nickel, Inconel, Zirconium, Tantalum, Carbon Steel etc. for different liquids corrosive toS5-316. ‘Note: Amaroffersallthe internal & optionally external wetted parts ‘nthe same material of construction as that of body & head to give complete corrosion resisting autocaves. ‘Most of the above material are available for stirred, non fabricated glass & shaker autocatves. ed, ‘GENERAL CORROSION PROPERTIESOFSOME METALS AND ALLOYS* RATINGS. Material Selection Guide AMAR. gives recommendation for material selection for particular media, however it doesnot guarantee 100% corrosion Fesistance of a particular M.0.C to a particular corrosive media, 4S it also depends on various parameters like temperature, pressure, concentration etc ofthe reactions. Reactor vessels of MOC $8216, upto 5 ltrs. are machined from rolled / forged bar stock & reactors above 5 ltrs. are normally fabricated from plates, The lid is always from rolled / forged bar stock upto 100 li, $316 autoclaves. The material listed below may not be ‘avallableinall possiblesizes. ©, Unsuitable. Not availablein form requiredornot suitable for fabrication requirements or not suitable for corrosion conditions. 4. Poorto fair 2. Falr.For mild conditions or when periodic eplacementis possible. Restricted use. 3, Fairtogood 4, Good Suitable when superioralternativeare uneconomical 5. Goodtoexcellent 6. Normallyexcellent Small variations in service condition may appreciably affect corrosion. Choice of material is thevefore guided wherever possible by @ combination of experience and laboratory and ste tests. Matas Wenig otreducira ela od Nevtral Alaina solitons Solutions, solutions | Caustic Anmenum | Acid fchng eg srdmild ‘yao sltons, hyeroeNo- mary ata, and eg ficPhos | Nen- | exuding | amines ire ‘hor, odd2ing ammonium sult, sat yeoide (est | solaons, conden | clones many sulfites evans) (ss3i6) Hastoye 5 6 5 6 ‘ 6 Hasctoy8 6 s 4 4 ° Inconel 620 3 é . é 3 Mone400 s ‘ . 1 ° tt200- 4 5 < 1 ° commerci ‘Gridcng esis Halogen and derives Newel | tng Halogen olde | Hyeroren or | medi, | Mois, Onyeg, | ci, ales, ahaine | acdtewe | eg, | Fuome | masteg | dives, Salutons | corde ehorine | above hyrehine| oy. 1@5.9e¢ | tions | below dewpeint_yerolis_ Hyaren| salts, den produas cone, peroues, point toric chromates halides =) 6 5 5 ‘ 3) teen eato 3 o 1 a S| 4 5 2 2 5 2) sam eat 5 a a ‘ a) 6am seeo0 eat0 *Fompernyhemiclengneshancoook 2Benen eros 55316 & 3161 has almost identical corrosion resistance properties, onlythat 316Lisalow carbon stainless ste! thas excellent corrosion resistance to ‘© Mostorganicacid systems like acetic, formicete ‘+ Ammonia & mostammonia compounds ‘+ Manysaltsexcept chlorides ‘+ Most commercial gases at moderate temperature & pressures ‘+ Hydrogen chloride, fluoride & chloride in scrupulously anhydroussysters Ithas poor resistance to + Organichalides + Dilute sulfuric, sutfurous, phosphoric & nitric acids at high temperatures & Pressures. ‘+ Halogenacidsat low temperature &indiluteforms + Caustics,Halogensalts chlorides PENcln cea aery It is @ nickel, chromium, molybdenum alloy that has the widest cortosion resistance & is the most widely used alloy or corrosive ‘media & next most popular after $316 Ithasexcellentcorosion resistanceto ‘Variety of chloride compounds & chlorine contaminated material ‘+ Strong oxidizing chloride solutions such as wet chlorine & hydrochloride & sodium hypochlorite solutions + Concentrated hydrochloric, sulfurie& phosphorieacids Depending on the application C276, C22 or C2000 can be selected butC276isthe most common & easilyavaiable grade. Hastelloy 82 It 15 @ nickel molybdenum alloy & offers excellent corrosion resistance to solutions of hydrachlorc, sulfuric & phosphoric acid in all concentrations & at all temperatures in the absence of oxidizingagents ene thas more better resistance than nickel in reducing environments Ithasexcellent corrosion resistanceto + Caustic Solutions + Chloride salts + Fluorine & hydrogen fluoride Ithas poor resistance to nitric acid & ammonia systems. Reyes Itoffersexcellentcorrosion resistance to ‘+ Handling concentrated alkalis + Hotcausticenvironment + Chlorinated solvents& Phenol! iu ukceyacucs Ihislighter material & has excellent corrosion resistanceto + Oxidiingagents such as aqua regia &othermixed acids + Nitric acidatall concentrations except redfuming nitricacid * Chloride fons, ferric chloride, cupric chloride & other hot chloride solutions. Mild reducing media suchas sulfuric &hydrochloricacid Titanium burns vigorously in presence of oxygen at high temperatures pressures, ‘The material becomes softer above 250°C & hence not advisable above 250°C. a Itoffers excellent corrosion resstanceto + Reducing environments + Allchiorides except ferric cupric ‘+ Hydrochloride & sulfuricacids below 70% concentrations. ‘+ Phospheric,rtricacids & alkaline solutions thas p00" resistance to oxidting agents. fener ‘Tantalum is practically inert to many oxidizing & reducing acids. It offers the best & most outstanding resistance to wide variety of corrosive media including hydrochloric, nitric, sulfuric & phosphoric acids tis attacked by hot alkalis & hydrofluoric acid ‘The costs are prohibitive however tantalum liner or inner wetted parts of tantalum & others part of Titanium or hastelloy C can be ‘offered. Small sizes such as SOml - 700ml can be manufactured ‘completely in Tantalum, The maximum temperatures are estricted upto 250°Conly. Chemical Composition of material of construction of autoclave (Major Elements in %) [Se No. [Matera fe N | Gr (Mo) ¢ Other 1. StaniessSteelSS216 6067942 | 182128 008 _205,15Ma 2 |Hastloy-c276 4755-62 145-465 1547001 ¢025,2.45W 3. Hasteloy82 2 erm) 1/2630) om cot 4 /Monet- 400 2/6) - |- | os 23-s1a, 035-0857, 30a 5. Inconel - 600 610 7380 1447 | — as = 6. Nick oa [soa | — | — | oas = 2.__|Tianum Gr 2/604 98% Pure Titanium 8._rconivm 702 955 — 2, ASHF = =EE cae Overhead stirred metal autoclaves “Multiple 4/6 overhead stirred metal autociaves Interchangeable meta stirred autoclaves, Glass overhead sted autociaves. Interchangeable stirted metal & glass autoclaves Bottom stirred metal autoclaves. “Multiple 4/6 bottom stirred metal autoclaves 'Non stirred pressure vessels eles le ela loly Ma/M6 iM s 1G 5 Ma / M6 {as induction /pilot-plant scale fabricated reactors Rocker/shaker hydrogenator P ‘Avalable for avtodave size {net water filling capacity) 50, 100,250, 40,750 ml, | 4.2.5, 10,20, 25,50, 75,100 ts 50, 100, 250, 40,750" 3,2, 5 508 100,450 & 750 i, 16 21s | 100, 250, 450, 750 ml, 1, 2 ltrs. 100,250, 450, 750m 1,2 ts. 25,50, 100,250, 450, 750ml, 25,50, 100, 250, 450 750 ml, 25,50, 100, 250, 450, 750 ml, 1.2.5, 10,20, 25, 50, 75,100. airs 1000 a ema ] 10, 250,500 mi 3, 2s pene "MOC options 55316 | ss z16t Hasteloy C276 Hastelloy €22 Hastelloy C2000 Hastelloy 82 | Monel - 400 | tnconel 600 Inconel 625 | Nickel -200 Titanium Gr.2/ Gr 4 Zirconium - 702 Tantalum Glass PEEK Code 316 316. Hes: Hea HCO a2 MIN IN INS NK tana 2R7 TAN Gis PEK ‘Available for | Available for ‘Max. design Seal eee cee Peer all all 575°C All, except Al 475°C al aL 550°C All, except Al S75 All except R al 50°C | All except ‘Al as0"c Al, except R al 450°C All, except R All asc | All, except R al 500°C All, except R All 3eC | Al except R al 325°C Al except R al 325°C AllexceptR&F | 25mi-2itr 275°C 6.16, R 100 mil-2 I 200°C G (only jacketed) 100 m= 2 It 180°C fora parlor pe ors ofthe te of rar Design pressure bar (kg/m) | sh 3 a 6/10 | 97/145 Corresponding Temp. Rating _at design pressure 200°C 150°C for bottom electrical heater & 200°C for jacketted 200°C 250% 20 50 300 75 350°C 100 1450 | 250°C, 350°C, 500°¢ 200 72800 | 250°C, 350°C, Source a a All Except G, ‘Available for autoclave volume 100 mi -2 Ie, 100 mi -2 ter, ‘Available in MOC as GGLS body with any material for head & parts 100 mi-2it. 316, HEB | Soltr-100 lt. 316, 3161, HCB, HC2, HCO, H82, Mia, 1N5, IN, NK2,TI2/T14, 287 2Smi-400ltr. | 316, 3161, HC6, HC2, HCO, H82, S0mi- 50m Mina, ING, INS, N2,T12/T14, 287, TAN 316, 3161, HC6, HC2, HCO, HB2, MINA, IN6, INS, NK2,TI2/TI4,2R7, TAN 316, 3161, HC6, HC2, HCO, HB2, MING, IN, 1N5, NK2, T12/714, 27, TAN Bite iol. jabove for many moteros to keep standard design & ols sublec to mox design temperoture column os perco Ee St. | Head & body sealing options Code | Avallabefor | Availabe for No “autoclave volume | autoclave types ._| Spit clamp with clamp bolts & Tat gasket N25mi- 100K. | Allexcept FAR | 2. | Split taper clamp with bolts T | 2S mi- i00itr. Allexcept FER [73._| Spir ciamp with Oring & without clamp bolts * VY) 25 mi-Fhe ‘Allexcept 6,16, FR 4_| Threaded clamp & vessel with'O' ing C35 mi-250mi_|_A,Mé, ME, IM, 8, BN, BME, P . | Nut & bolts with flange & gasket 2 | solt.-20001mF ‘This design is suitable for maximum 100 bar pressure at 225°C for Viton & 275°C for Kalrez Frings Pern es ‘Sr. | Head mounting options ‘Code | Available for ‘Avallable for ‘autoclave volume | autoclave types 1. | Removable head design | Allsizes| All, except R, IM 2._| Fixed head design with removable vessel & heater (Manual) Kk S0mi-dike ‘A, Md, 146, IM, PG 16 3._| Fixed head design with removable vessel & heater (Motorized) M__450mi-Shte ‘A, Ma, M6, IMP. G16. noe ‘Sr. | Stirring motor options: ‘Code Available for ) Available for 5 soem [3 Toor tana #5 | 25mi-10001t2 |All How to inquire / order autoclaves - reactors - pressure vessels 1. Metal / Gass / Multiple / Interchangeable SS & Glass / Interchangeable Metal Stirred Autoclave se | pce |S Se ee ae eee Ex to order ir stitred autoclave of 5S 316 with 100 bar pressure @ 250°C, with splt clamp bolt sealing, removable head with FP top mounted motor, electra ceramic heater &toley model coge shouldbe mage AU 216-100-250-N-H-XB-ECTL Formule autalaves prefix shouldbe Ma or M6 restallsame Sima or glasiwil be, 2 316-6150-N-H-X4FTL where 316isthe MOC of other wetted pars ike head &fitings) for interchangeable autoclavesmention thefts only 2d wl automatcalybe considered UseIMariGas prec 2. Bottom stired autoclave: The coding remainsthe same ae above, exceptremave the head mountings code, sivingmotorcade Neatng style code ‘temperaturecode ie, 800m 916-100: WT For multiple bottom stredautolves refiashouldbe BM 4/EM6 2. Non sired pressure vsse-the coding remain the same ag above, except remove the ring moter ype code inbetween e.P-2L-316-100-250-N- 4. Forgasinducton pit plant scalereactorsgiefolowingcode&detatsoftheinternaltenernal [Te He Hm Hose” How fitings required 5. Rocke/shaker hydrogenator- thas common singe setup to accommodate ll the vessel ses of diferent MOC ver Lf woe | worn Lf woeat | [-sineyenanee || wowing L[ feavaresinet og we HS [[_secs [{Serane |] Steet Lane [ weneaen ene fore 3Rocker Autoclave with 1007, 500m 2 as & $5316 vessels wit electra heating tabletop mounting, willgererateolloning code .300m-GLS-316-SOOML-GLS-316-2U8 GS 3164C-7T eo;0 Cc Stirred Metal Autoclaves Specifications (A) - 50ml-1001trs. volumes oA “The volumes are specified in terms of net water filling capacity (in closed condition with all Internal fittings). The lid & vessel are machined from forged / rolled bar stock or fabricated from plates depending on the volume & material of construction. Re (WErSieiodse sak Odeo) 55316 forallinternal & externalwetted parts ‘Optional: SS 3461, Hastelloy 8/C, Monel, Inconel, Nickel, Titanium, Ziconium, Tantalum for Internal & optionally external wetted parts Design Pressure / Maximum Allowable Working Pressure (MAWP) ‘Autoclave volumes Standard Optional Omi 00m 250i, 450m, 750ml, | 10Qbar(Ke/ mn") or 14S0psh 1) 200 bar {Ke em} or2900 psi Alte, 2k, Slr, 10k, 201,25. i) 350 bar {kg/m} 05000 psi upto 10 tice Solr, 75ir, 100. Sober ike/em* or 725 px 100bar (g/cm?) or1450 psi ‘Gilet hou elec he prasares fom the above anges avid specifying over pressures as or designs ar a5 pe ASME codes whchaead have ‘ult In factor of safety of 35. Winans ene Optional: 350°C (662 °F) or 500°C (932 °F) s > Drone kar ° r 7 As S ‘ tl] Pressure gauge, vent needle valve, safety rupture dsc (rated to rupture at MAWP}, internal @ cooling coll, thermowell (with RTD-PT-100 temp. Sensor) gas inlet & liquid sampling needle valves with a common dip tube (sparger| upto the bottom, Optional: wi 2} Ball valve with funnel for powder / slurry / liquid inlet (These are valves with 1/4"-2" si depending on autoclave volume they can be used for charging solids or iquid slurry at atmospheric pressure or higher pressure, If high pressure liquid charging pot is also ordered). b) Flush bottom valve with almost zero dead volume (some times additional ball valve at the ‘outlet of flush bottom valve can be provided on special request). €) Serpentine cooling cil instead of helical for easy cleaning (450mlto 100|trs.) d) Teflon coated S5 diaphragm or Hastelloy C/ Monel / Tantalum etc, diaphragm pressure gauge orcorrosive mediainnonSSautocaves | Options a) & (b) are standard for 10trs & above autoclaves. Eee 1) Split clamp bolt design (N): Split clamp type quick opening system with clamp bolts & tongue & groove sealing with 7 PTFE head gasket for temperatures upto 350°C & metallic grafoil head gasket for temperatures upto 500°C for reactors upto 100trs. The spit clamps are held in position together by a latch to prevent flying of clamps in event of accidental over pressure. This design's avallable upto 350bar pressure. a @ 1) Taper clamp design: ‘apersplitclamp type quick opening design with 2 clamp bolts & tongue & groove sealing with PTFE head gasket for temperatures upto 350°C & metalic grafoll head gasket for temperatures upto S00°Cfor reactors upto 100s. The spit clamps are tightened together with2 bolts with handto give leaktight seal. Thisdesignis available upto 350ber pressure 4Stirred Metal Autoclave Specifications Self sealing design (V) ‘The head & body can alternatively be sealed by a self sealing design in which there areno clamp bolts. Only the split clamps & Viton / Kalrez ‘0! ring can be used to give sealing under pressure. The head with '0' ring i fixed tothe body by just siding the split clamps with latch. Ths is very easy & convenient for closing & opening the autoclave. However with Viton ’0' ring max. temp. is 225°C & with Kalrez max temperature is275°C. Although Kalrez has better chemical resistance than Viton but the same s exhorbitantly expensive. This sealing can be offered for pressures of 100 bar only. While selecting a Viton ‘Oring customers have to check the suitability with solvents, ammonia etc. as Viton gets easily attacked by many of them. This design s available upto 2 it. size only. Threaded sealing C): For SO m- 250 ml vessels there is alternative ‘0’ ring seal design with threaded clamp & threaded vessel forease of opening & tighteningby hand. Penne Removable Head Design (H) Thisis the most commonly used option & available for all sizes of autoclaves. Here the body restson the stand / trolley & the head is lifted for charging, discharging & cleaning, Also the ‘vessels removable for charging / discharging / cleaning, This option ismore commonas he head & vessel can be taken out easily for pressure testing, iting accessories, servicing ete. & ismoreeconomical Optional: Fixed Head Design(K/) Availabe for SOmi-10\trautoclaves only In this system the head ofthe autocaveisfxed with motor stand & the vessel & heater are raised & lowered manvallyby slidingor manuallyby rotatingscrew or electrically by motor & {gear box. The vessel or heater can be slided manually up & down for assembly or disassembly for 80 mito 250 ml autoclaves, manually screwed up & down fr 400 mito lit autoclaves & motorized lifts provided for 400 ml & 101t.autoctaves. This system i useful when the head of the autoclave as lt of ittings& accessories, making tlficulttolftthe head & detachallthe fittings after every batch. Also removing the heater fr faster cooling & ease f itingorloweringthe vesselis advantageous (Referpg. 14 forpicture af all models) a) Topmounted ACmotor [Non flameproof (NX) -Flameproof (FLP)/ Explosion proof AC motor (for Group IMM 1B gases: XB) suitable in hazardous area fo all flammable liquids / gases except hydrogen & acetylene with variable frequency drive & stirrer RPM indication, The motor Is coupled tothe magnetic drive directly by specially designed coupling ensuring quick engagement & disengagement fof motor from autoclave head. The direct coupling eliminates pulleys, belts & minimizes transmission loses, noise, vibrations & maintenance. The frequency drive can indicate ‘motor current / Torque % (on selection). This is useful o monitor the change in viscosity of the liquid under stirring. The frequency drive is mounted on a common control panel. thas the facility to trip the motor on any overload, over voltage or overcurrent. RPM Range:100 - 1450 Motor Options: * Flameproof AC Motor group lIC (XC) CE Atex certified (Ideal for H, 9). ‘+ Motors with gear box can be offered for stirring highly viscous material at low rpm & are standard for 50-100 itreactors. ‘+ Motors with 2900 rpm for stirring at high speeds bb)Compact Motor Drive (8D): Compact iniine brushless / PMC motor & magnetic drive (refer Pg. 8 for the same) & speed controller with indicator for 300-1500 rpm. /wailable for autoclaves from 0 ml - 25 ltr. volume metal & glass autoclaves. Very compact, economical & light weight. No external rotational part.to Note: NX, XC & BO motors are CE marked, FX if 750 mi xed head desen sth motorized vessel tng lowering TAS Non it? i, CFL? mater AC motor FL motor Ew Motor with Variable speeddrive “gear box: o 7a 0s q Zero Leakage Magnetic Drive Coupli (Tee These couplings are extremely useful for high pressure or high vacuum applications where leakages are not permitted for continuous running. They have replaced the gland ‘Sumechanical seating, eee acy Jt is azero leakage maintenance free coupling directly driven by the motor. It consists of extemal magnet rotor, which is driven by the motor. A stationery shell is threaded / bolted / press fitted to reactor head & completely isolates the external rotor from the {inner rotor. As the external rotor rotates, the internal rotor also rotates in synchronism. The reactor’s shaft is threaded / bolted / keyed to the inner rotor. High energy ‘permanent rare earth magnets are fixedinside the inner & outer rotors, Awater cooling. jacket protects the magnets & other components from excessive temperature arising fromthereactor. Paneer ary Over Gland / Mechanical Sealing + The gland/mechanical sealing need replacement after every 200-1000 hrs of working depending on application & have limitation of maximum pressure where as magnetic, drive can run virtually life long without leakage with minimum maintenance & can be designed or pressures upto 5000psi * Very useful forlongor round the clock reactions asingland/mechanicalsealingifthere isany leakage midway, thewhole batch maygo waste. * Zero leakage implies zero breakdown & zero maintenance, hence large savings in maintenance costs foryears. + Safe whileusingtoxic& hazardous chemicalsasits leakage stotally prevented. + Nowasteof expensive liquids through leakage. + Almost nolossessince theseare friction ree in synchronous operations. * Minimum vibration transmission &hencesmooth running. ‘= The coupling is flexible & hence any over load results in coupling slippage, thus preventingany breakageof coupling, shaft orfailure of motor. We ke ea eee) + Topmountedcompactintegral inline motor & magnetic drive. * Zero leakage duringrotation under vacuum & under pressure. + Noexternalrotation, otationinsidehousing, + Noiseless vibration free with infinite variable speed regulator &indicator. * No stand for motor mounting required, hence no alignment, vibration & noise problems. + Lightweight, economical & very compact & hence occupies very less table space. PMOC/DCBrushless motorwith DC drive & RPMindicator. ‘Available for autoclaves from SOmI-25 Irs. volumes. Se coupled decty tomotor Tonermagnet reactor head ‘Cross-Sectional vow of Magnetic srve connected toresctor essWEEE asc) ‘+ M-Series: Magnetic drives formetalautoclaves + MM-Series = Inline motor & magnetic drive for metal autoclaves. "Note: The number ater the series indicates the torque capacity in Kg-m for S316 for other MOC ‘theactualtorquemay vary. Magnetic Drive Coupling Specifications f Wen whee st Se Static torque capacity icy he teed No. | Mode! No. Kg-cm, Nem. Necm. Abin. for reactor volume (a) | Moa/mnaos 8 078 785 6.04 sOmi-250m | (bo) Mzo/ninaz0 20 196 195 aa 530 ml - 250 ml 400 m2. te) | moyenne 0 3.92 382 347 400 mi 5 le. (@)_|_ Mso/ninago 80 7.85 785 ea 5-25 te (e)__Mzoo/wi200 | 200 196 1960 170 10-100 te ‘_|_aoo 400 392 3520 340 400-s0ok. | (e)_ | m600 600 588 3880 545 $500 - 1000 It (o)_|_t200 1200 176 11760 1030 1000-2000 it. (| M1800 1800 a7 17700 1562 2000 - 3000 It (| M2a00 2400 235.2 23520 2182 3000 - 5000 It, | [ta [3000 3000 294 29400 275, 5000 - 10,000 te. Note: Magnetic devs of higher torque capacty for eactos of any make canbe designed on request. Higher of lower than recommended foraue Gives be sed ox particular reactor size depending on motor hp /visostes / sires design ete ine eee Description Standard _ Optional MO. wetted parts ss-316 Hastelloy C, Monel, Inconel, Ziconlum, Titanium, PEEK* Design pressure / max Fall Vacuum to 350bar for (a)to(@), Upto 350 bar for (@) &() allowable working pressure | _00bar for (e) & (), 50 bar for (-(k 100 bar forte) -(K) ‘Max. working temp. at ‘00°C with water eooling jacket = rated pressure £& 200 °C PEEK MOC ‘Maximum RPM 1450 for (a) to (a) Upto 3000rpm for (a) to (4) 750 for (e)& () 1500 rpm for (e) &(f), 300 for () to (k) + For PEEK MOC, design pressure 10 bar @ 260°C avaliable in model nob) & (Cont Ema & ef ew a) Singleortwo stage, 4/6 bladed ptchbladeturbinetypeimpeller a eo” Oeil Optional: b} Propeller, c)Rustonturbine. Paddle e) Hollow shaft for max. gas dispersion at higher rpm, Ideal for hydrogenation or any gas- liquid reaction f) Anchor / anchor with PTFE blades for viscous liquids at low rpm (max. 200 rpm). 8) Spiral for highly viscous polymers/ mixtures with downward thrust at low rpm (max. 200 ‘om. h ae 1) Specially designed for highly viscous material forinside and outside mixing a i Note: » Other speciaily designed stirrerslike helixane (helix cum anchor) etc. canbe offered on request. ‘ a + Gearbonhastobe prowdeacolngcoihastobe removed & hugged or)Cc Stirred Autoclaves - Specifications Electricalceramic band heating mantle EC) with ceramic wool insulation & $S cladding. Optional: a) Flameproof / explosion proof IIB + H, certified, aluminium cast Heater for H, gas with ‘otally enclosed heating elementinside metal tubes (EA). Optionally the heater alsohas inbuilt cooling coils & is useful when internal cooling coils are not possible. I is suitable formax. 250°C inside the autoclave, Heating rates are lower in FLP heatersin comparison toceramicband heaters by) $5-304 jacket for oll/ steam heating with insulation & cladding 1S). ¢} Hfdirect electricheating snot permitted (due to spot heating), heater canbe providedon lo Jacket with ol inside, The heater can heat the oll wich can in tu heat autocave worm we: = ch a8 wees 4) External heater temperature thermocoupleis provided for cascade temperature control 30 panel toensurasafety of heater, vessel & accurate temperature contro. Itisstandard feature in aluminum east heaters. @) Allceramicbandheaters are CE marked. oneal = : Compact SS-304 (for corrosion resistance & longer life) control panel with microprocessor based accurate programmable PID temperature controller cum indicator with temperature alarm system (settable), safety alarm & heater trp system for malfunctioning of controler/ sensor/ temperature rse beyond set limit. The motor speed drive is mounted on the same panel forstired autoclaves. 3 phase panels are provided with phase current indicator. This hrelpsindentityngifany ofthe 3heaters have falled. Motor, heater, cooling solenoid valve/ ppump/ sensors etc utilities ae connected to panel by simple plug & socket arrangement. ‘The panel is very easy to open & all internal components are plug socket type, making replacement easy. Digital pressure indicator/ controller/ flow indicator/totaliser/ motor ‘urtentindicator/ heater temperature cascade controller/ torque indicator levelindicator/ pH/ D0 /ORP / turbidity et. indicators are provided additionally on same common control paneldependingon the optionalaccessoriesselected. Optional: 4) Digital temperature indicator in flameproof enclosure mounted on trolley & non FLP SS panelmountedremotelyin sate area b) Complete flame proof (FLP) Group ia/8or IC control panel mounted ontrolley ‘Note:FLP pane's should be opted onlyf'the heater & motors areFLP and areais totally ex- proofas LP panels are too bulky & inconvenient for operation & maintenance. ©) Touch screen panel with SCADA software for single or multiple autoclaves. 4) Panels with RS 485 port fr PC communication through SCADA software without local display. «©) CE marked conteol panels with IVD & EMC testing can be supplied on request. es S0Hz, 19 220V for autoclaves upto 10Ltrs. (or any size autoclave with heating through jacket) &30, 415V for20ltrs.& bigger autoclaves with electrical eating. KW powerratingof the panetcan be calculated from table on Page 12. COptional:10, 110V0r39, 230V with SOHz or 60H. Autoclave Mounting Options ) ‘Trolley (TL, table/ bench top (TT) floorstand (5) 2 ‘Complete autoclave with motor drive assembly is mounted on easily movable $5-304trolley forcorrosion resistance & longer life) with 4 lockable wheels & the trolley top is big enough to mount the optional accessories & aso the control panel. Table / bench top model is for keeping the autoclave on platform. Table top mounting is offered for sizes from 25mI to. a 2itrs only. In table top model the panel & accessories ifany have to be mounted separately. Infloorstend mounting the autoclave mounting plateissupported by 4, $S-304legs without Wheels & there will be no space for mounting any accessories or panel. Tis is useful when there is space constraint or panelis mounted remotely Refer page 11 for pictures of various, ‘mounting options. 400 Bench Top Resctor 50Glens Meo ‘ (3) 100 mi beneh top model [c)2 fr removable head teller model {450i Bench Top Mosel (6) 5c metal vessel with (300m EEK / PTFE wetted pats bench too made! (e)201tr toe model (rn Shertrotey model (i) 25 tray mode 1Cc Boe eee | (Ih) 100 i 450m 250-mi 2 Site Technical Specifications - Stirred Autoclaves St Autoclave Minimum Vessel Vessel Motor Heater Overall dimensions Overall dimensions Powder/ Flush No. volume stirable 1/0 internal hp ©=—skw_—tabletop/floorstand trolley model** liquid bottom volume mm height model without panel* WxDxH inlet size valve mm WxDxH (mm) (mm) finch) dia. (mm) 1. | 25ml —12ml_— «30. AD_— toms 0.2 280K 280x300 NA. NA NA. 2 Som 20m 4063/44 275K 230x780 1010410x1300 NA 8 3. 100ml 20m 4083. 1/4 4 275x 230x780 10104101300 NA a 4 250ml som 65 | «801/405 275x230x780 10104101300 | NA. 8 5. | 450ml 60m 7518/48 =~ 320x270x900 —_1010%410%1340 1/4" 10 6 750ml 6Oml_ 75193 /4_4.25 320K 270x980 —1010x410x1340 1/4" 10 7. | Ait, 330ml 2086 | 968/41. 355x310x925 1040%x410%1350 1/4" 10 8. 2itrs. 130ml 1016 | 303, /4_—1.75-355x310%1065 1040%x410x1350 1/4" 10 9. Sitrs. 360ml 152,310 /4_ 2.8 420% 355x130 1100%410%1350 1/4" 10 20. toltys. it, 183 400/23 585x560K1550 1310x585x1550 1/2" 15 12, 20ltrs. 26Itrs. 248 495/25 585x 560x180 1310x585x1850 | 3/4" 15 12, 2sitrs, 26ltrs. 248595 /2_S_——SBS5XSG0KI950 1310x585x1950 | 3/4 15 13, Soltrs. Gltrs. 355/343 558/600 1105 «675x675x2350 1500x675%2350 1" 25 14, 75itrs, _Bitrs, 396/384 600/650 1 12 725x725%2350 1500x725x2350 1" 25 35. 100ltrs, _22itrs, 456/440 699/735 1135S _—_—780x 7802350 1550%x780x2350 | 1" 25 ‘7 Pane ste 300 200% 3CGmm For standard phase with temp, APM and Pressure controler) and 800 Wx 3701x345 H mm or tandard3 phase with em eMandeessre controllers), forotheraccessoriesitmay change > Theaimensionsarefortabletop modelsupto 2s. &floorstand modestromStrsto 00's. Note: + Theabovespecicationsare for design pressure of 100 bar (xcept 5010100 ifr 50/100} & 350"Ctemperatureand MOCSS316.Thesamemay change for higherbressure/ temperature & ferent MOC autolves. ‘+ Overalcimensionsarincieatv, they may change depending on the optonalaccessores or speciledesign maifcations opted ‘+ Maximumreaetion volume illbe75%ofnet filing volume. autodavevolume). + Total aquipmentsiecrclloadeMotorkw + Heaterkw + Auto Cling psp (0.37) if opted any accessorestselected) Since development isacontinuousproces the above specifications oe subject change without priv notice 52oC G. A. Drawing of Metal Stirred Autoclave with optional accessories 250m & 100rn in reir with fae ead design 2 iter fixed head with motorized lift (m) 55ultiple Stirred Autoclave System (M4, M6) 40r6 parallel reactor can be offered on the same mounting with common control panel with complete data acquisition on PC & optionally individual gas mass flow controllers to control ‘indicate the gas consumed (Ideal for hydrogenation). The system can have all reactors of ‘same (preferable) or different sizes, Simultaneous reactions can be carried on each reactor with different parameters & comparative studies can be done from the data received. It saveslotof space, cost & helps in advanced & faster researchi.e. high through put testing. Salient Features: ‘= 50ml-5 tr parallel4or6autoclaves can be offered. + Optional common PC / HMI/ Touch screen to monitor all the parameters ofall autoclaves, consingle screen. 1+ Verycompact & economical or MOG pressure & temp. ratings aves, itings, body &heod sealing ster ypes, motor & drive, heating, head cutoclove mounting style contalpane), technizaspeciictionetrefesteedmetolovtocloves, FLP M6 model with remate common ‘eontrol panel & PC ‘M4 model with bottom string ‘48 model with 100: autctves 4 commen panel High through-put catalyst screening system + Faster Screening of Catalysts by runningaallin parallel with similar conditions + Volumes: 25 ml, 50ml, 100 ml, 250 mi, 450 ml, 750ml, 4 or Snos. parallel autoclaves + Pressure: 30bar (Optional upto 200 bar) ‘+ Temperature: 150°C (Optional upto 250°C) + MOC:55316, Hastelloy8/C, Monel, Inconel, Titanium etc Fully automated process without human intervention with manual made for emergency/ ‘malfunction/bypass + SCADA software with suitable laptop for remote set points, recording & control of temperature, pressure, speed control, H2 gas flow rates, total H2 consumed with batch report & online / history graphs + Programming for leak test, N2 / H2 flushing, temperature profile, speed control, H2 purging, pressure control with H2 gas uptake, cooling, vent etc Safety alarm & interlock for high & low temperature / pressure & suitable safety rupture dises + Verycompactto fitin fume hood & highly advanced Complete SS construction )Ci Bottom Magnetic Stirred Autoclave (B, BM, BM6) + 25mi-750m! capacity * Miax. design pressures upto 200 bar & temperatures upto 200°C + MOC: $$ 316, $5 3161, Hastelloy B/C, Monel, Inconel, Titanium etc + Bottom magnetic stirring * 4 0r 6 parallel autociaves of different capacities can also be offered on the same ‘mounting with common control panel with complete data acquisition on PC (Refer pg. 15 for picture). + Very compact, most economical & maintenance free ‘or voles, fitngs, body heed sel, the technical specications et. refer sted metal utectoves Overall dimensions for Bottom Stirred Autoclave w > 4 225/ 50/100/250 ml 280 mm 320mm 480mm 450/750 mi 280 mm 320mm 570 mm 450ml & 750ml, ILtr. & 2Ltrs autoclaves). Amar does not promote this option as this is possible in autoclave having same diameter, only the heights being different the minimum stirrable volume is same hence it is advisable to go for only higher volume autoclave as ‘changing the internal fittings like cooling coll & thermowell is not advisable regularly (if not refitted properly, user may face leakage problem). For MOG, pressure temp. rotngs, volves, tings, body & heod sealing, stirrer types, motor & drive, heating z Farge tetmtnrinroctrdoctoars i J 4in 1, 100 mt 1035 mm 360mm 430mm 4n1, 400 mt 1200 mm 380 mm 570 mm (acre — Z is a) Autoclaves with common head, external fittings, panel, motor, trolley etc. & 7 interchangeable separate 2nos. vessel, heater & internal ittngs (possible for SOml & 100m, 450 /750 mi interchangeable b) Interchangeable, any 2 different size autoctaves with common panel, motor & trolley. f spaceisthe constraint, cost of panel, motor & trolley of one autoclave can be saved but the User loses the flexibility of using 2 autoclaves at a time. This option is possible for 50m! Ltrs, any two sizeautoclaves atatime. Gen ce en ou) This system is used when the productis developed / producedon continuousbasisforbetter ‘productivity In such system gases & liquids are added continuously in stirred reactor & product is recovered on continuous basis at high pressure & temperature. Such system may ‘employ 1 or more reactors in series. When connected in series the overflow of 1st becomes theinletto2nd& soon. Theyare available insizes from 100mIto 100 Lr. All the other specification as per stirred reactor, such system is normally supplied with ‘multipleinlets & outlets for addition & transfer/removal of gases & liquids for accessorlesto such ystemsrefer belowGio ne ened These reactors use a tubular vessel packed with a fixed bed of Catalyst. Reactant liquids & gases are fed to the reactor at controlled rate through pre-heaters & pre-mixer. Final 4B productsare collected from the outlet of the reactor & cooled & separated for recovery. ‘eine 1) aes . ‘These reactors are used in petroleum, petrochemical, polymer, pharmaceutical, specialty “s emia! ake industries to carry ou reacTons tke catbonfaton, FyGregenaton, mau hydrocracking hyaoformuaton part oxidaton, polmeration te mn salient Features -g 2 These are wedincontnuous modeforbetter productivity a = 5 ular miro reactors wath packed catlytbed gi or 2 pressuresupto 100bae x ‘= Temperatures upto 1200°C ‘+ 3Zone spit furnaceforheating + Possibility toconnect to GC for analysis ‘= Completely automated system with Scada software. PR ee eas {Referoptional accessories section on page 26 for detail working ofbelow accessories) a) Gas Feed System: May consist of forward pressure regulator & or gas booster & or ‘multiplegas low controllers. ') Liquid Feed System: May consist of charging pressure pots or one or more metering pumps. €)Back Pressure regulatorsmanualor automaticte maintain constant upstream pressure, 4) Consdensors: These are used for distillation / reflux or condensate return back or for cooling, ©) Gas/Liguid separator are used to separate the gases from the liquid by collecting the liquid & venting the gas. 4) Level Control System: with the help of dip pipes or overflow nozzles or optionally automated evel witch/sensor for level contol £2) Mounting: the total systems with all the accessories are mounted on MS or SS skid withall the interconnecting tubing/piping. h) Control System: a) Modular or common integrated compact controler to monitor & control all the parameters on single screen, b) Touch screen panel with indication & controlofalthe parameters. i) Software: Suitable scada software to control & monitorall the parameters remotely from the PCwith datalogging, online & history graphs. nae ——= = + Gasrecycling through catalyst basket volumesSO ml /100 ml ‘+ Multiphase reactor + MOC: 316, Hastelioy, ete Pressures upto 350 bar & 500°C temperature RPM: upto 3000 MER beeen) The same reactor setup can be used for liquid phase & vapour phase reaction with ‘minimum changes of internal components givingit great flexibility & cost economy, Availabe in 250 ml & 450 mlautoclave volumes. For liquid phase reactor all specification & optional accessories as per metal stirred autoclave,a ulm iia) lected High pressure fischer tropsch reactor with 125 booster, mass flow controller et accesories & SCADA software 0 pitch imovesnaton eauioment for processing high temperature caoon fide, ompesites using itch monomer 25 ie tanium high vacuun reactor i with homogenizer 8 anchor with PTFE wipe Blades Cine le Hydrothermalsynthesisof zeolites, synthetic clays Forbaunite digestion Foralkaline /sulphuricacid leaching of ores Fornapthenicacid corrosion studies Forerystalization Forsolubiity studies foxides Forcarryingoutpulping & pulp bleaching experiment Polymer minireactor for synthesis ns. Batch reactor for vsbreakng process 55CEST Me cae Cue Aa eet eae Caled (2) 11000 te 500 2501 Pei * Sizes >100 Irs. £1000 ltrs. working volumes, = MOCSS-316, 3161, Hastelloy B/C, Monel, Inconel, Nickel, Titanium, Zirconium ete, + Design pressures upto 100bar {kg /em') or 1450p). + Max. working temperatures upto 350°C. + Zera leakage magnetic drive coupling rom 20-300N-m torque capacity. * High mass transfer hollow shaft with gas induction impeller (ideal for hydrogenation, oxidation, ammination, chlorination, bromination ete, gas liquid reactions) pitch blade turbine, anchor, propeller, paddle etc. for other applications. « Very efficient for gas liquid mixing * Fabricated with dished ends & 100% Xray radiography of welded joints + Jacketed or single /double limpet coil with insulation & cladding, + Upto 440.ppm infinite variable speed with suitable gear box. + Body flanges with bolts & teflon /spiral wound metalic gaskets for shell & dish sealing (2) + Without body flange, monoblock design offered depending on pressures & application, + Internal cooling coil, vent, liquid / powder charging, dip tube, thermowell, flush bottom outlet, baffles, light & sight glass, handhole / manhole etc. nozzles, fitings, ex-proof control panel & accessories offeredasrequired + Suitable catalyst filtration & recycle system offered for hydrogenation. (refer page 31) + Lugsorfloor stand skid mounted structure. + Alldesigns as per ASME codes. += CE& PED certified reactors can be offered on special request 2st, 100 bar For other optional accessories refer page 26. v=C@ Ex-proof hydrogenation pilot plant with catalyst charging, catalyst filter with recycle & catch pot Pe etek ae CeeFully automated ex-proof alkoxylation pilot plant with touch panel & SCADA. 2Cc Glass Body Autoclaves (G) = itis useful when one has to see the reaction & with PEEK / PTFE coating itis economical ‘option when chemicals/ acids corrosive to SS316 are used or nometalis permitted, Volume 100m, 250m, 450ml, 750m) Ltr. 8 2 moc Borosilicate lass cylinder wth top-bottom flange, head & other wetted partsof$5-316 Optional - + Glass with wetted parts of PTFE / PTFE coating, HastelloyC, Titanium, Monelete. + Glass vessel with glass jacket both on shell & bottom () can be offered forjacketed heating by thermic fluid. + Glass-PEEK inert autoclaves : All wetted parts of PEEK / PTFE / PFA coating (Including lid valves, fitings & magnetic drive) with jacketed vessel Design pressure : bar ke/em*}or 85 psig. Optional: 10bar upto it glass autoclave Design 150°C / 200°C (with electric plate heater from bottom / by temperature circulation of hotollthrough jacket) Powersupply: 19,220V,SOHz/60H2 Safetyshield : Polycarbonate transparent cover is provided from all 4 sides of glass vessel for safety incase of breakage due toaccidental overpressure. Note Alot sections as per sired mel atacoves, Ike stondod tings, body & head ong, sting motor ®& dive, ager drive, ental pone, mounting, os pe str autoclaves, except in goss 7 ‘utoclves sofety valve standod ited of ruptured Bottom discharges possibleoptonalyonlfor ony 2 jacketed alas reactor type ofjecketedlosscutocaves ‘Glass autoclave are alsoused in eactioncalorimetry. Interchangeable Stirred Metal & Glass Autoclaves (IG) Interchangeable glass cylinder assembly with top bottom $$ / other metal flanges, external bottom plate heater orjacketted glas, pressure safety valve & safety shield tofitin aexisting ‘standard metal autoclave for sizes from 100ml to 2Ltrs The top lid, motor drive, panel etc. are common. It's highly economical, compact & versatile. This option is available only with split clamp head sealing (N). For jacketted interchangeable autoclave fixed head design is ‘standard & for bottom heating model removable head design (H)isstandard, Designpressure(glassautoclave) _: 6bar kg/cm") or 85 psig, Designpressure(metal autoclave): 100bar Design temperature glassautoclave) : 150°C (for electrical heating) / 200°C (for jacket heating) Design temperature {metal autoclave) : 250/350/S00"C ‘ltherspedeatonssame above @ D a Fc Head inerchangeable 2 ie trehangeable SS & gh Jacked ales & metal autociave ‘ath bottom elec heating a 22Rocker/Shaker Hydrogenator (R) Plies * Charging, operating ete, very simple, also vigorous mixing reduces the reaction time considerably. * Very small compact system without gland hence minimum spares & maintenance. '= Very economical considering the interchangeabilty of different capacity bombs in one autoclave, + Used mainly for synthesizing or modifying organic compounds by catalytic hydrogenation. * Usedtostudy catalyst activity nies Volume + 100ml, 250ml, 500ml, 2 Ltr, 2Ltr with option of using more. thanone vessel of any ize & MOCin samesetup, Moc + $5-316& Glass Optional: Hastelloy C wetted parts. Design pressure 2obar {kg/em*) or 300psiformetalvessels &3 bar{kg/em')or45 psifor glass vessel. Designtemperature = 200°C for SS vessel & 150°C for glass vessel with optional Electrical heating arrangement & control panel with PID controller & alarm system, Drive £ U/2H.P.flame proof AC Group II, 16 orl motor with about 200oscillations/min. fixed rocking speed. Optional: Variable speed rocking with variable frequency drive Mounting + Table topor SS loorstand. Gaseylinder ‘Around 4 Ltrs. capacity H, gas cylinder of SS-304 with inlet, outlet valves, pressure gauge & flexible hose pipe with NAV to feed gasinto the vessel whileitisin motion. Standard fittings Vent valve, dip tube with sampling valve, 2” opening on. (formetalvessel topforpowder/liquidinlet & cleaning, thermowel, only) pressure safetyvalve. Overall Dimensions 850mm (W!} 700mm {0} x 700mm (H) (without panel) for Table Top models 850mm (W} x700mm (O}x1300mm (H) for Floor Stand models Panelsize 300mm (W)}x300mm (0) x300mm (H) PowerSupply 3, 415V, SOHz / 60H? for fixed speed & 19, 220V, SOHz / 6012 or variable speed shakers Safety Shield SS wire grid is provided for glass bottles for safety in case of breakage dueto over pressure, Shaker witn SS vee, lectcal heating & 30 contol pane "ble Top Mosel oor Stand Model 32DS Mal eke CRE ‘These are same in design & constructions as the stired autoclave except for, they do not hhave stirring motor, magnetic drive coupling, stirrer shaft & impellers. All other specifications for non-stirred autoclave is same as stirred autoclave. These can be custom ‘uit to suitmost high pressure applications, Volume: 25mito 100 ts. For MOG working pressure, temperture, standard fitings, body & heed sealing, heoting. control pane ‘mounting technical specseations refer metal sired auteioves Applications ain * Itcan be used as a gas/ liquid storage pressure pot (For pressures higher than 1500ps, where fabricated potis not desired) to charge liquid/ gasin the autoclave/ other pressure vesselat higher pressure. ~ i Certrehere 7 | |. Top Mode! They are used for dissolving or digesting inorganic or organic samples in strong acids or alalisn chemically resistant tefion-lined vessels & lid athigh temperature & pressures with ‘complete containment & recovery. They have no valves, nozzles, fittings or pressure gauge EE, evcentarupturedise 4 Volume 25mito750m Max. design pressure ) im I Bon eres) Supercritical Fluid Extraction (SE) system uses supercritical carbondioxide (C02) as solvent insteadof any oganicsolvent. — Application: eS 7 ee ee Te arr ae catranesphatnaceutcals, chericals compounds et. wi . + Sxvadtonotessentiloils ee + Extraction rom natura products, food, plymersete. eh eg . * Drying ofaerogels: hr ~ + Exvactionafnieotine &cafeine + cleaningofhigh precision components & photo esiss i ‘These system consists of stirred autoclave / pressure reactor or a non-stirted pressure ‘vessel. Liquid CO» is charged into through a booster a plunger pump. CO>is maintained atlow temperature to keep it in liquid stage at lower pressure by providing aheat exchanger before the pump. Suitable cryoslat bath is used to maintain low temperature of CO>. The ‘material to be extracted is placed in an extraction vessel & pressurized with CO to dissolve ‘thesample with desired temperature control. tis then transferred toa separator whereit is <=") ‘depressurized (by manual / automated back pressure regulator) resulting in precipitation of desired material & condensed CO2 can be recycled. Optionally CO» pumps with inbuilt peltier cooling {> supplied to avoid the heat exchanger & cooler before the pump. PC ‘operated complete automated system canbe offered. Volume +: 100ml-Siit Designpressure ——_: upto10,000ps) ‘Max. working pressure : upto 380bar ‘Max.temperature — : upto200°C moc :Ss316 a:jh Pressure Vessel System for Hydrogen Induced Disbonding Tests ‘Amar has manufactured & supplied system for Hydrogen Induced Disbonding (HID) tests {a per ASTM G146, These tests are used to simulate & study the effects of hydrogen environment under very high pressures from 150 ~ 250 bar & temperatures from 400 - 500°C on bimetalic plates that are to be used under similar conditions in refinery. The results would give the resistance of bimetallic steels & its alloy to hydrogen induced disbonding, Thus such tests can be used to decide the material metallurgy, its heat treatment, ‘manufacturing & fabrication technology for use in refineries in similar environments. The system can be manually operated or optionally completely automated. Initially the test samples are put inside the vessel & pressurized with hydrogen to very high pressure upto 150-200 bar & then heated to desired temperature of around 400 - 500°C for a period of ‘around 48 hrs. After the testis over, the vessel is cooled at a pre-defined rate of around 150°C /hr. till the temperature reaches 200°C. The vessel pressure is then released completely & cooled further toremavetthe test samples, Technical Specifications: y Sizes 1L,26,5t ‘moc 185326, Inconel 600, Haselloy C276ete. oy Design Pressure: 200bar/350bar 7 Design temperature : 500°C. StandardFittings : Pressure gauge, safety rupture disc, vent valve, thermowell with } ‘temperature sensor, gas inlet valve & manual back pressure: regulator Heater ElectricCeramic band heater with insulation. = Control Pane! Temperature control panel with vessel & heater cascade temperature control & high temperature alarm system. Optional Forward Pressure Regulator, Gas boosters for H, & N, gas, automated back pressure regulator, internal cooling coil with autocooling system, automatic pressure control valves, complete automated system with SCADA software, ET CTe ENR CU CLUC CAMs ‘Autoclaves for corrosion application are mainly usedin aggressive environments like H2S & supercritical watersin ollrefineries & defenceindustries. Ria merken = Normally corrosion test coupons are suspended in stati non-stirred) or stirred autoclave systems & corrosion is measured in terms of weight loss. In stirred autoclave system, sometimes the coupon holders are attached to the shaft & rotated during the testing ‘Autoclaves are then fed with the corrosive media & designed temperature & pressure are raised & maintainedin the autoclaves. Optionally suitable electrodes ike pH or ORP (MOC: § 55316 / Hast-C) are provided to measure the pH & redox potential under pressure. er ‘Autoclaves with working, counter / reference & auxillary electrodes can also be offered with potentional measurement system for electrochemical corrosion testing Ree In thissystem, the autoclave is connected with aspecial high pressure ‘pump which can re-circulate water/liquid continuously at very high velocity through the test spool & the autoclave connected in ine. Sizes 400 ml-25 tr ‘Max. design pressure: 100/200/350 bar ‘Max.temperature :S00°C Moc $5316,Hastelloy-C276,ci Optional Accessories Optional accessors are offeredto increase the versatility of the equipment, toadd value & feature to the standard product & to provide complete range of instrument/ equipment requited for @ particular application. Most of the optional accessories are common for stirred, non-stirred, glass, rocker & fabricated autoclaves unless specified aces ‘Tomanually charge diferent gases at desired pressures upto 140 bar (Kg/cm*) / 2000 psi or higher into the reactor from gas cylinder. Nitrogen, Oxygen & Hydrogen can be charged ‘through same regulator(with special adaptor) Regulator for other gases like NH3, CO, etc can also be offered, The regulator comes with inlet - outlet pressure gauges & SS braided teflon high pressure hose pipe (4m long). Gas boosters are useful when the cylinder pressures are much lower than the autoclave fated pressures. In such case the booster takes gas at lower pressure from cylinder & ‘compresses the same to deliver at higher pressures upto S000 psig. They are generally pneumatically operated. Special gas booster pumps are availabe for liquid CO2 used in supereritical fluid extraction system. The booster systems are supplied with air fier regulator pressure relief valves inlet-outlet pressure gauges & valves. Complete SS mounting withallfitings & valves s optional Thermal Gas Mass Flow Meter / Controller - = bs ‘Thermal mass flow meters (MFM) can be used to measure accurate mass flow rate of gas (in ‘gm/hr or LPH) & totalized quantity of mass /volume [in gms Ir) charged in autoclave at any point. Mass flow controller (MFC) s used to charge the set flow rate of gas nto the autoclave at high pressures up to 350 bar (kg/cm) or It can be used in pressure control mode to indicate the gas low 8 total gas uptake to maintain desired set pressure inside the autoclave (ideal for hydrogenation). The same MFM / MFC can be used for multiple gases by just entering.the conversion factor for different gas densities provided the gases are inert toeach ‘other. The MFM/MEC comes with high pressure flexible hose, inet fiter with digital gas flow Indicator cum totaizer & additional pressure PID controller with pressure sensor i the MFC jsused in pressure control mode. User has to specify the max. flow rate range, pressure, g3s 4& mode (flow control or pressure control) for ordering MFM/MEC. Optionally MFM / MFC ‘certified for use in zone 1 hazardousarea offered on request. CRM neha amicus ‘These are used for higher & accurate gas or liquid flow rate indication or control where thermal mass flow meters are not suitable. Common meter can be used forall the gases & liquids with only change n pressure drops and flow rate anges. Digital Pressure Indicator / Controller It consists of $5336 pressure sensor (transmitter) & digital pressure indicator/ controller (mounted on common control pane!) with pressure alarm & optionally heater cut off for safety. Digital pressureindicator has pressure reading nbar & psi, where as controller reads ‘any one of the units, The controller is normally used with mass flow controller (MFC) or solenoid/flow control valve to maintain constant pressure inside the autoclave. With MFC, Coriolis ass Corie Mass Flow Flow Atte Contraler {25 low indicator & totalizer are also provided on the same panel. The pressure sensor has, temperature limitation upto 80°C & hence the same is provided with water cooling jacket. Optionally intrinsically safe pressure sensor with lIC certification is provided. Pressure sensorswith HastelloyC/ Inconel wetted parts can be offered on request. & + Allstandard high pressure hose sipplied are flexible 5 braided Teflon hose with 2000psi i? pressurerating unless specified. Resta . + Complete mounting ofall the accessories shollbe done on autoclave stand /troley “ _ + Alltheindicators/controllers are mounted on acommon SS panel 7 ContalVave 2Optional Accessories quid / Slurry / Gas Charging High Pressure Pot Its used to transfer liquid or gases in to the autoclave under pressure. It consists of high pressure S5-316 pot designed for working pressure 100bar (kg/em') or higher with port for nitrogen gas (N,), liquid / slurry inlet with valve & funnel, outlet valve, pressure gauge, pressure safety valve, high pressure hose & NRV, The liquid to be charged is ed into the pot from top funnel & pressurized with N, gas until its pressure is higher than the autoclave pressure & then under pressure the liquid is charged into the autoclave. The quantity & rate of flow of liquid charged is not known precisely in this system. However a level indicator or sight glass or weighing balance or flow meter can be provided optionally to measure the liquid charged or i's flow rate. Pots of different pressure, M.O.C. & sizes can be offered. These pots can also be used for storage of gases when gas cylinders are far off. With this ‘option approximate quantity or flow of gas consumed can also be determined by measuring the pressure drop, Sizes: 250ml, Yilte,1itr, 2ltes, Sls, 20 kes Enero consists of $$ 216 ethylene oxide (EO) horizontal pot with inlet, outlet valves, gasinlet with dip tube, thermowell, pressure gauge & high pressure hose pipe for 1Obar (ke/cm"} working pressure, Itisused for ethoxylation. It can be supplied with flame proof weighing balance to ‘measure the quantity of £0 charged. Sizes: 2 ltrs. &SItrs, (tienen tanec — _— ‘This system is used to charge the liquid at desired rate from as low as Iml/hr. to 100Ltr hr, when the autoclave is under pressurized condition. The system comes with metering pump, flow indicator, controller, iquid sump, pressure gauge, strainer & high pressure hose. Optionally pressure safety valve, flow totalizer is also provided. AMAR offers 2 types of pumps. 2). Low cost diaphragm pumps for pressures upto 100 bar & min. flow range of 60-600mI/hr. ‘tomax. 10-100|it/hr. The flow rates are varied by varying the motor speed with variable frequency drive ) High pressure more accurate HPLC type low flow metering pumps for high pressures upto 350 bar & flow range from 0.01 upto 100mi/min. These pumps can be used along. with precision weighing scales to measure the total liquid charged at any point of time. Optionally inline flow meterscanbe connected to measure the actual flow ofthe liquids Riverine — This ystems useful to control temperature overshoot for highly exothermic / outof control runaway reactions & fr faster cooling after the reaction isover. ‘The control pane! ofthe autoclave gives 230V, 10 output to connect external auto-cooling system, AMAR gives 2 options: {a} Solenoid valve, flameproof IC (for autoclaves upto 25 litr) or (b) pneumatically actuated ball valves for autoclaves above 25 ltr) connected atthe inlet of the Internal cooling coll with external source of water supply. This is standard for SOml - 250ml ‘autoclaves, however for bigger autoclaves ifthe cold water ine pressure is <2bar then it isbetter to opt for external pump & tank water cooling system. Normal tap water cooling is not effective at higher temperatures due to steam back pressure whereas pump & tankautocooling system gives positive pressure & faster cooling, a ® ‘Wlighing sale (a) with FUP cot (bl 7Cc Optional Accessories ©) Pump & Water Cooling Tank: It consists ofaSS 304 water tank & pumptocirculate water — the internal cooling coll of reactors. Cooling starts automatically ifthe rate of heating. rises suddenly. It comes with non FLP / FLP monoblock pump tank, pipeline & flexible hose pipes with ORC & is mounted on the autoclave trolley itself. It can also be used to Circulate water in the cooling col of external aluminum cast heater when internal coll is not possible. Ice can be putin the water or the hot water can be discharged & fresh water replenished on continuous basis for more effective and faster cooling. Mic ke ents It is used to reduce the autoclave temperature to as low as upto -50°C from room ‘temperature to carry out reactions at lower temperatures by circulating thermic luidinthe internal cooling coil / jacket of autoclave, It consists of single/double stage compressors, condensor, circulation pump & temperature controller for thermic fluid & reactor. The system can be with bath or closed loop bathlesstypeforefficient & faster heat transfer mise ceca — {tisopted only ifheating is jacket type & the area is totally lameproof or directelectric band heaters are not permissible. Heating can be done by circulating hot thermic fluid through the jacket of the autoclave. The system comes with SS tank, electric heaters, level switch, [pump for thermic fluid & reactor. The heating system is non flame proof & can be kept ata distance in safe area, if the reactor isin flame proof area. The system can be with bath or closed loop bathiess type for efficient & faster heat transfer. Open bath system can be ‘offered upto max. 150°Cinside the reactor (due to fuming of thermic fluid) & are available upto 25 lt. autoclaves only, whereas closed loop systems can be offer upto 250°C inside the reactor & upto 1000Itr. volume. Cin eeer ee 2 If heating & cooling both are to be done by circulating thermic fluid through reactor jacket then, common single fluid heating & cooling system (open bath/closed loop) for temperatures from-50 to 200°C inside the reactor can be offered, Open bath system can be offered upto max. 150°C inside the reactor (due to fuming of thermic fluid) & are available Uupto 25 lt. autoclaves only, whereas closed loop systems can be offer upto 250°C inside the + reactor & upto 1000 ltr. volume. ‘Note: All the above systems are supplied with 6 ft flexible insulated hose & optionally suitable thermicfluid. Gerrennees “Thesevalvescanbe connected atjacketinlet for controlling flow of team hot oll/ water for temperature control from PID or atthe inlet or outlet ofthe autoclaves for pressure contro ‘Amar gives 2 options. {a} On/off pneumatic ball valve actuated by 230V output from panel to FLP IIC solenoid valveinline of aiesupply Pd {b) Pneumatic proportionate flow control valves with 1 to P convertor (for accurate temperature/ pressure control). fa) eeOptional Accessories Gren Itis a jacketed tube 55-316 (0.01m*, 0.02m* or .05m? area} heat exchanger used to reflux the condensate back into the reactor & vent off the uncondensed vapours. is connected directly on the autoclave lid & works under fll autoclave pressure, Reflux condensers an be offeredin different MOC & area, rues Its a $5-316 shell & tube reverse flow heat exchanger for distilation/condensing the vent vapours from the autoclave upto 10Kg/cm* pressure. It can be offered in all different MOC, higher pressure & different surface areas such as 0.1, 0.2,0.5, 12m. The condensate can be collected separatelyin receiver or optionally refluxed backinto the reactor. [ees 88316 receiver pot can be connected at the outlet of the shell 8 tube or Refluxcondensor to collect the condensate separately. tis also provided with port to apply vacuum & offered in 250 mi tr, 1 ltr, 2 ts & Sites. volumes. Higher volumes & other MOC can be offered on specialrequest.Itcan be optionally provides with level indication. Back Pressure Regulator ummm Itis mounted on the vent line of the autoclave & is used for maintaining constant pressure inside the autoclave. The pressure is maintained by releasing the excess pressure into the atmosphere or through ahose to safe area. The pressure can be sentially onthe gauge, by ‘manually varying the knob until the gas comes out. Once the set pressure is exceeded the excess pressure is released until the autoclave pressure becomes equal to or below the set pressure. The pressure release is slow & gradual & the set pressure can be varied at any point. Alternately electronic digital back pressure regulator can be offered on request, here the pressureisset digitally & canbe released at preset rate of pressure release Pressure Safety Valve — High pressure autoclaves are provided with built in safety rupture disc, however additional safety can be offered by providing pressure safety valve whose release pressure can be set ‘manually for a wide range by increasing or decreasing the spring tension. The set pressure should normally be around the design pressure. Safty relief valves are standard supply for Blass & rocker autoclaves where rupture discs are not avallable for low pressures. These valves come with PTFE /Viton orings which may not be suitable for certain gases & solvents. Erne m nrc For autoclave volumes from 10 ltrs. to 250 its. the head & vessel are too heavy to lift ‘manually, Hence chainpulley block mounted onsame trolley with SS Stand can be offered for lifting the head with minimum efforts. Electricchainpulley hoists can be offered on request. s - iM 2Cc Optional Accessories Berm ee en ‘SCADA isa supervisory control & data acquisition software with all controllers / indicators, having RS485 modbus communication port or PLC & HMI / touch panel, for online display, set point changes & data logging of pressure, temp., Motor RPM, motor torque % & ‘optionally liquid / gas low rate with totaliser, heater temperature level, pH, ORP, turbidity ‘ete. remotely from PC as well as locally from panel. Itgives continuous online data logging at — predefined variable time interval, online graphicalrepresentation as wells historical data & ‘graphs on PC for single or multiple autoclaves. RS 485-232 convertor & cable upto 10m or higher is also supplied. Wireless data communication from PC to panel can be supplied on request Removable Teflon / Metal/ Glass liners can be offered for autoclaves from 100ml-SLtrs. size. ‘These liners canbe used for reactions that are corrosive, to prevent only the autoclave body from corrosion. Teflon & glass liners can be used upto 200°C, metal upto SO0"C. The heat transfer is also very poor with teflon & glass liners. Glass liners cannot be fabricated accurately. Hence, Amar recommends the use of complete corrosion resistance metal autoelaves made from special alloys like Hastelloy, inconel, Titanium ete. over glass/teflon liners. Liners should be used only if costs the constraintor corrosive chemicalsare tobe used sparingly. Matallinerscan be offeredin Hastelloy C, Inconel, Monel, Nickel, Titanium et. eters Itis provided toimprove the efficiency of the catalysts & for holding the catalyst so that t wil notbe destroyed or changedy thestirringaction of impeller. The baskets are made from$S ‘wire mesh & connected to the stirrer so that it rotates with the stirer. itis available for 450mi-100 Its. autoclave. The catalyst basket can be static which is stationery & dynamic which rotateswith the impeller. Eee, —— = These are small 7 microns sintered cup flters which are threaded to bottom ofthe sampling dip tube so that while sampling liquid, the catalyst does not come out. Its very useful when, the catalystis normaly very expensive or pyrophoric. These fitters may reduce the rate/flow ‘of the sampling liquid due to the resistance offered by the fine mesh, hence they need regular cleaning to prevent choking. Fiters are avallable for 450mI-100Ltrs. autoclaves. ‘These filters are availablein $5316 & HastelloyC. etree Its used for one time catalyst charging under pressure during the reaction It consists of a 3mi to 150ml (depending on Autoclave size) small container with airtight cap, that is ‘openable. The powder sfilledin the container which is then threaded to the autoclave head from below to a separate port with needle valve on the top. Under atmospheric & pressurized conditions the powder remains inside the container as the cap remains closed. ‘One hasto apply gas pressure greater than autoclave pressure fromthe needle valve on that port so that the cap opens & releases the catalyst inside the autoclave under pressure. Depending on the optional accessories selected, sometimes the catalyst addition device ‘may not be possible due to space constraint on the head. Available for autoclave sizes 100 mi 100 tr & upto 250°C, 30Optional Accessories CIriinoricnn hea) It consists of vertical $5 sintered fiter cartridges in a $$ housing. After the batch s over the reactor liquid is transferred to the catalyst filter under reactor/nitrogen pressure. [After the filtration is over, the catalyst is taken back in to the reactor by back washing, thus recycling the same & makingit available forthe next batch. Generally this systems. suitable & available for 101 & above reactor volumes. Conn system Itisa pressure reactor with magnetic drive stirring, inlet & outlet valves, pressure gauge & nitrogen/vent. Solvent & catalyst are charged in the vessel & the slurry formed by ‘mixing is transferred under nitrogen pressure into the reactor. The pressure rating & volume of this system is designed depending on the volume of catalyst, pressure & ‘temperature rating ofthe autoclave, This system is suitable for SOL & above reactor volume. Its used to collect the vent vapours / gases from the autoclave vent / rupture disc / safety value port, when the vapour / gas i highly hazardous to release directly into the atmosphere. Itis a pressure vessel, taken almost double the volume of the autoclave & designed for less than half the reactor design pressure. tis provided with inlet, outlet, vent, pressure gauge, safety valve & optionally a frame arrester. Its normally filed with water. The ‘gases / vapours collected are safely released through the flame arrester to avoid any hazard, tis suitable & available for autoclaves from 10 Ltr to 1000 Ltr. Suitable rotary vane or diaphragm vacuum pumps can be supplied for vacuum from 700mm of Hg upto 10” mm of Hg in the reactor depending on the pump type selected. It isused either before starting the bateh or for high vacuum distillation, Sultable analogue ‘or digital vacuumindicator with controliercan be offered on request. 2Cc Optional Accessories Cee a) Level transmitter / switch / indicator to measure or maintain level inside the reactor ‘under high pressure. b) pH/ turbidity / 00 / ORP sensors with indicators & controllers for high pressure & temperature application, 6) Removable internal baffles for better stirring (but cooling coll has to be removed in small {d) Quartz / sapphire view glass windows In jacketted vessels to see the reaction. ‘e} Sampling pot with condenser for cooling / condensing & collecting the sample taken at high pressure & temperature, £) Torque sensor for accurate measurement of the motor torque, where change in torque Indicates changein viscosity ofthe reaction. 4 " ‘ow Conversion Table @ eetick cleus ( 2: hastlloytaley mounted autoclave with darious optional accessories ike lameproot temperature indicator, motor, auto cooling system, aluminum cast ester, high pressure liquid charging potlashbottom vahe, ballvalve for powder ile, retux condenser, Hhmeproot ‘motor, removable head design, hastlloy pressure safety va, MPa atm bar kg/em* a | 9.8692 10 1017 145.08 oa | ose6s2 1 o1s7i 14504 iaieiey | stssree cian a 6gsasx10? | 0.06805 0.06895 | 0.07031 1 En °F 21.8x(°C)+32 a ‘Kg-cm Nm ‘Necm Ib-in 102 1 100 asseT aS areal ATE: 0907/2008 “sist cary hae ave olning AMAR make ates: & [Seat [Raper [Year of [Presse [Temp aCi STRAT mn ee ee OL CLE Aarti Drugs Ltd asianpaints O-BASF The Chemical Company CRODA —¥ pe reoors z)) IndianOit a 3; Alembicy, (© I x AUROBINDO © AstraZeneca? Gik a \ BAY ER] \ & R — PHARMNCEUTICNS gs Biocon Cipla ecremuova Caring for life x Clariant ; i AN @dishman carly, Limited PAV ESTEE Alive Divis Laboratories Ltd. “th aes Ging 6 = Glenmark Panuaceta.s SODAVARE GlaxoSmithKline cunear heuba uorocreicats timed Pan aa Y FR =a S£ipca Ain Jonnaor Macey a Healthy LifeSome of our valued customers rr we CHEMSYS paw INDUSTRIES Shell St fi. les TZ VINATI ORGANICS, LIMITED ® LARSEN & TOUBRO (ij/Mylan Orchid cheimicalty .& pharmaceuticals {te Procter & Gamble S& SANDOZ S.H. KELKAR & CO. WWF Limited @ LUPIN VY A Mactzops | MERCK C hoc 1 ; Navin FLUORINE R Uy Novartis INTERNATIONAL LIMITED, CD Pidilite em Ay Warcroup £\Shasun SIGMA-ALDRICH are SOLVAY SRF 9 syngenta ™*! | oe US. PHARMACOPEIA SI Sando ty . 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