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Carbon black
Plasticizer
Chemical Analysis
Instrumental Analysis
FTIR
TGA
FOURIER TRASFORM
INFRARED SPECTROMETER
THERMOGRAVIMETRIC
ANALYZER
Chemical Method
Burning Test
Disintegration in Conc.HNO3
Beilstein Test
Elemental Analysis
Nitrogen
Sulphur
Halogen
Burning Test
Materials burn and continues to burn
Disintegration
No disintegration
Butyl, silicone,
EPDM
red hot.
Rub hot copper wire on
sample and heat that
copper wire on the
flame
Observe colour of flame.
Elemental Analysis
Rubbers mostly contain C and H
Few rubbers contain elements like N, S and
Halogen
Lassaignes test
Small
The
Nitrogen
Chlorine
Nitrile
rubber,
Polyuretha
ne
Neoprene,
Hypalon
Sulphur
Hypalon
Moisture content
Weighed sample is heated to 100c for 2hrs.
Ash content
anaysis
FTIR
Quick method.
A nalyse all type of samples like
Infrared Region
Near Infrared Region : 13000-4000
cm-1
Middle Infra red Region : 4000 200
cm-1
Far Infrared region : 200 10 cm-1
for
ORGANIC COMPOUNDS
FTIR GRAPH
IR Spectrum
The absorption peaks
Isoprene Rubber
SBR Rubber
Intensity
800
699
vs
887
vs
758
885
909
909
962
1370
990
1640
1490
FTIR
GRAPH
Thank you