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Sintered Components

Metal powders from Hgans go into a large share of the worlds production of
P/M parts. By combining complex shapes with specific and unique properties, the
uses for P/M parts are many. Our R&D works proactively by developing and
perfecting new powders to expand the potential range of applications. Parts for
automobiles, household and office appliances, fittings and power tools, are just a few
of the many existing applications for P/M parts made of our metal powders.
Some examples:

Sintered bearings is a well-established application. The porosity of sintered


parts allows absorption of oil for lubrication. Normal sintered density is less
than 6.2 g/cm, and powders containing Fe-Cu or Fe-C are often used.
Power tool parts often utilize diffusion alloyed powders, achieving a sintered
density around 7.0 g/cm. Subsequent heat treatment further increases wear
resistance and strength. Warm compaction is in some cases used to further
increase density and improve gear strength.
Lock parts require high strength, toughness, wear resistance and dimensional
stability. Diffusion alloyed powders admirably match these parameters for
the sintered part, achieving a density between 6.8 and 7.0 g/cm.
Belt pulleys or chain sprockets can be found in every automobile. They are
components ideally suited to the P/M process, as it permits an intricate
weight-saving geometry. Sponge iron usually forms the base powder,
ensuring ample green strength. Sintered density ranges from 6.5 to 6.8
g/cm.
Synchronizing hubs for automobile gear boxes are mainly produced by the
P/M process route. High strength, wear resistance and dimensional stability
are demands for this application. Diffusion alloyed powders are the common
choice of material to meet the demands. Densities are in the range 7.0 --- 7.2
g/cm.

Illustrated are a few of the many parts ideally suited for P/M production. From left:
lock part, bearings, belt pulley and power tool part.
This catalogue provides a comprehensive presentation of powder properties and
mechanical properties, covering a wide range of base powders, alloying elements and
process conditions.
Our specially-developed CASIP computer program is capable, given property-,
processing- and additive requirements, of identifying the ideal powder mix for a
specific sintered component.
Hgans press-ready mixes and Starmixes ensure uniform composition and
powder properties, both between and within lots. Hgans Densmix makes warm
compaction possible and thereby increasing density and strength of the material.
Comprehensive quality assurance, from ore to finished powders, ensures customers of
the best powders for their sintering operations.

Properties of Powders and Sintered Materials

Properties of Powders and Sintered Materials


The successful application of iron and steel powders as raw materials in the
manufacturing of structural parts, is related to a number of specific powder
properties:
Flowability (here expressed as flow rate) is an important factor, as is
Apparent Density during filling of the die cavity.
Powder compressibility affects the density that can be obtained, and
thereby also the properties after sintering.
Spring-back value is important for calculating the dimensions of the
compacting tool in relation to the final dimensions of the part.
Sufficient green strength is required to prevent cracks during ejection of
the part after compaction, and to allow transportation of compacts from
the press to the sintering furnace.
All these properties are affected by the particle shape and the particle size
distribution of a specific powder. Sponge iron powder exhibits more
irregular and porous powder particles, which results in higher green strength
compared to water atomized iron powders. Atomized powders have higher
compressibility compared to sponge powders.
On page 9 powder properties are presented as a comparison of some
common iron base powders. Flow and apparent density are presented for
pure powders. Compressibility, green strength and spring-back are presented
for powders with 0.6% Kenolube added to the mix.
Water atomization process allows alloying elements to be added to the
molten steel before atomization. A range of pre-alloyed powders are
available under the trademark Astaloy. By pre-alloying, mechanical
properties of the sintered material are improved while the compressibility is
lower as compared to pure iron powders.

Iron and steel powders for sintered components

STARMIX and DENSMIX introduce organic binders to the powder mix.


With bonded mixes, dusting of fine particle size additives is eliminated.
Segregation of alloying elements is avoided which improves dimensional
stability.

3
3
2

Flow (s/50 g)

Distaloy powders are based on pure iron powder or iron powder


pre-alloyed with 1.5% molybdenum (Astaloy Mo) to which alloying
elements of fine particle size are bonded by partial diffusion. This technique
avoids segregation of alloying elements and improves dimensional stability.
Good compressibility is maintained with only partial diffusion of alloying
elements to the iron powder particles.

2
1
1

With DENSMIX warm compaction is made possible. By heating both the


powder and press tool, density is improved by 0.1 0.2 g/cm3, which
improves the mechanical properties of the sintered material. Also the green
strength is greatly improved allowing some machining operations to be
carried out in green state. This substantially improves life time of the cutting
tool.

7.
7.
7.

Green density (g/cm)

7.

The sintered properties obtained with a specific iron powder grade depend
on several factors, including density, sintering time, temperature, atmosphere
and both type and content of added alloying elements. Extensive information
of this type is present in this technical catalogue for most of the available
powder grades.

6.
6.
6.
6.
6.
5.
5.

For a brief survey of sintered properties of some common materials, the


diagrams on page 10 show the tensile strength, hardness and elongation.

5.
5.

Materials 1 4 were compacted at 600 MPa, resulting in densities in the


range 6.85 7.10 g/cm3 while materials 5 12 were compacted to a density
of 7.10 g/cm3. All materials were sintered at 1120C for 30 minutes in
endothermic atmosphere for base iron powders, and in 90/10 N2/H2
atmosphere for diffusion alloyed powders and Astaloy powders.

0.4
0.3

Spring-back
(%)
Springback (%)

0.3
0.2
0.2
0.1
0.1
0.0
0.0

Properties of Powders and Sintered Materials


Apparent density

Flow rate
35
3.1
30

3.0
2.9

25

AD (g/cm)

Flow (s/50 g)

2.8
20
15

2.7
2.6
2.5
2.4

10

2.3
2.2

2.1
0

2.0
MH80.23
SC100.26
ABC100.30
NC100.24
ASC100.29

MH80.23
SC100.26
ABC100.30
NC100.24
ASC100.29

Green strength (0.6% Kenolube)

Compressibility (0.6% Kenolube)


10

Compacting pressure (tsi)


20
30
40
50

10

60

7.4

35

7.2

6.6
6.4
MH80.23

6.2

NC100.24

6.0

SC100.26

5.8

4000
25
20
15

ABC100.30

5.4

5.2
100 200 300 400 500 600 700 800 900
Compacting pressure (MPa)

2000

10

ASC100.29

5.6

3000

Green strength (psi)

6.8

Green strength (MPa)

Green density (g/cm)

5000

30

7.0

1000

0
0
100 200 300 400 500 600 700 800 900
Compacting pressure (MPa)

Spring-back (0.6% Kenolube)


10

Compacting pressure (tsi)


20
30
40
50

60

0.40
0.35
0.30

Spring-back
(%)
Springback (%)

e
n

60

40

7.6

Compacting pressure (tsi)


20
30
40
50

0.25
0.20
0.15
0.10
0.05
0.00
100 200 300 400 500 600 700 800 900
Compacting pressure (MPa)

Iron and steel powders for sintered components


Distaloy powders

Iron base powders

Astaloy powders

1000

900

900

900

800

800

700

700

700

600

600

600

500

500

500

400

400

400

300

300

300

200

200

200

100

100

100

400

400

400

350

350

350

300

300

300

250

250

250

200

200

200

150

150

150

100

100

100

50

50

50

12

12

12

10

10

10

0
1

1. NC100.24 + 2%Cu + 0.6%C


2. SC100.26 + 2%Cu + 0.6%C
3. ASC100.29 + 2%Cu + 0.6%C
4. PASC60

10

Pla

1000

800

Elongation (%)

Hardness, HV10

Tensile Strength (MPa)

1000

Spo

0
5

5. Distaloy AB + 0.5%C
6. Distaloy AE + 0.5%C
7. Distaloy DC + 0.5%C
8. Distaloy HP + 0.5%C

10

11

12

9. Astaloy 85 Mo + 0.5%C
10. Astaloy Mo + 0.5%C
11. Astaloy A + 0.5%C
12. Astaloy CrM + 0.4%C

Overview of Powder Grades


rs

Plain Iron Grades


Sponge Iron Powders
NC100.24 is one of the most widely used iron powder
grades in the powder metallurgy industry. The greenand edge strengths of the compacts are very high due to
the spongy structure of the powder particles. NC100.24
has a good compressibility and a low and consistent H2loss.
SC100.26 has the best compressibility of all Hgans
sponge iron powder grades. The green strength is also
high. It has slightly higher apparent density than
NC100.24 and should be used particularly where high
density after single pressing and sintering is desirable.

MH80.23 is specially designed to match the requirements


for self-lubricating bearings. Its particle size range is
chosen to give an optimum pore structure for this
application. MH80.23 can also be added to powder
mixes in small quantities to substantially improve green
strength.

12

.5%C
%C
C
4%C

11

Iron and steel powders for sintered components

Atomized Iron Powders


AHC100.29 is an atomized plain iron powder with good
compressibility. It is used in similar P/M applications as
SC100.26, but the apparent density is considerably
higher than that of the sponge iron powder grades.

ASC100.29 is an atomized iron powder with very high


compressibility, which makes it possible to single press
compacts with densities of up to 7.2 g/cm3. ASC100.29
is particularly suited for high density structural parts,
and also as a base material for soft magnetic
applications.
ABC100.30 is an atomized iron powder with
outstanding compressibility and chemical purity. It is
especially suitable for the production of high-density
structural components. Densities up to 7.4 g/cm3 are
achievable with single pressing. ABC100.30 is also used
in applications where very good soft magnetic properties
are required.

12

Pho

Overview of Powder Grades

Phosphorous-alloyed Grades
d

PNC60 consists of NC100.24 to which finely-divided


ferrophosphorus particles are added, giving a
phosphorus content of 0.60%. Green strength and
compressibility are almost equal to that of pure
NC100.24. Sintered parts made from PNC60 exhibit
high strength in combination with very high ductility.
The phosphorus enhances sintering, allowing shorter
sintering times and lower temperatures to be used.

PASC60 like PNC60 contains 0.60% phosphorus but is


based on ASC100.29, which gives the powder very high
compressibility. Sintered parts made from PASC60
exhibit high strength in combination with very high
ductility. An addition of graphite and/or copper will give
still higher strength with retained or even improved
dimensional stability. PASC60 is also suitable for
components requiring good soft magnetic properties.
s

13

Iron and steel powders for sintered components

Diffusion-alloyed Grades
Distaloy SA is based on the sponge iron grade SC
100.26, to which 1.75% Ni, 1.5% Cu and 0.5% Mo
have beendiffusion bonded. Distaloy SA is
recommended for densities up to 6.9 g/cm3 after
single pressing. With the addition of graphite, a
sintered tensile strength of 600 MPa can be achieved.
Distaloy SA has a high green strength. This powder is
well suited for parts requiring heat treatment.

Distaloy AB has the same chemical composition as


Distaloy SA, 1.75% Ni, 1.5% Cu and 0.5% Mo, but is
based on the high-purity atomized powder ASC100.29.
Distaloy AB can be single pressed to densities of around
7.2 g/cm3. With the addition of graphite, a sintered
tensile strength of 650 MPa can be achieved. After
heat treatment the strength can be raised to 1000 MPa.
Distaloy AE is in principle the same powder as Distaloy
AB but with Ni content increased to 4%. Cu and
Mo contents are 1.5% and 0.5% respectively. High Ni
content and good compressibility makes it possible to
produce materials with a sintered tensile strength of
750 MPa. Distaloy AE exhibits good hardenability and
dimensional stability.
Distaloy AF is similar to Distaloy AE but with higher
alloying contents: 5% Ni, 2% Cu and 1% Mo. With
the addition of graphite, a tensile strength up to 850
MPa can be obtained after single pressing and
sintering.

14

Overview of Powder Grades

e
.
h

Distaloy DC (DC = Dimensional Control) is a lowalloyed powder specially developed to obtain both a
stable dimensional change independent of the density
and a high strength after sintering. By adding graphite,
a tensile strength up to 700 MPa can be obtained after
single pressing and sintering. Distaloy DC is produced
by diffusion bonding 2% nickel to Astaloy Mo (itself
pre-alloyed with 1.5% molybdenum). This double
alloying technique ensures a good compressibility and a
small scattering of dimensions.
Distaloy DH (DH = Direct Hardening) is a low-alloyed
powder which exhibits an extremely good hardenability.
The additional copper increases the hardenability of
Distaloy DH further compared to Astaloy Mo. This
makes it suitable for all common heat treatment
processes including sinter hardening. With additions of
graphite, a tensile strength up to 700 MPa can be
obtained after single pressing and sintering. Distaloy DH
isproduced by diffusion bonding 2% copper to Astaloy
Mo (itself pre-alloyed with 1.5% molybdenum). This
double alloying technique ensures a good compressibility
and a small scattering of dimensions.
Distaloy HP (HP = High Performance) contains 4%
nickel, 2% copper and 1.4% molybdenum. Very high
strength is obtained after sintering with a dimensional
change that is close to zero. With additions of graphite,
a tensile strength up to 850 MPa can be obtained after
single pressing and sintering. Distaloy HP is produced by
diffusionbonding 4% nickel and 2% copper to Astaloy
Mo (itself pre-alloyed with 1.5% molybdenum). This
double alloying technique ensures a good compressibility
and a small scattering of dimensions.

15

Iron and steel powders for sintered components

Pre-alloyed Grades
Astaloy 85 Mo is a water-atomized steel powder
containing 0.85% Mo, balance iron. The lower
molybdenum content compared to Astaloy Mo gives
Astaloy 85 Mo a somewhat higher compressibility, and a
lower hardenability. The latter makes it easier to avoid
through-hardening of thin sections during surface heat
treatment. Astaloy 85 Mo is often used as-sintered with
addition of copper and/or nickel.

Astaloy Mo is a water-atomized steel powder pre-alloyed


with 1.5% molybdenum. This grade exhibits high
compressibility and a homogeneous microstructure after
sintering. This, in combination with its optimal
hardenability, makes this powder an excellent choice for
parts requiring surface hardening. The result is high
surface hardness and good core toughness. Astaloy Mo is
often used as-sintered with additions of copper and/or
nickel.
Astaloy A is a water-atomized steel powder which is prealloyed with 1.9 % Ni and 0.55 % Mo. This
composition results in a high hardenability. The material
is often used with the addition of copper making it
suitable for sinter hardening. Astaloy A can also be used
for different types of heat treatments with or without the
copper addition.
Astaloy B is a water-atomized steel powder which is prealloyed with 0.45 % Ni, 0.6 % Mo and 0.3% Mn. This
is an established alloying system used mainly in heat
treated applications often with additions of copper or
nickel.

16

Overview of Powder Grades

Astaloy CrL is a water atomized iron powder pre-alloyed


with 1.5% Cr and 0.2% Mo. The composition results in
high hardenability comparable to Astaloy A. This makes
it suitable for sinter hardening preferably with small
additions of copper. Astaloy CrL has a good
compressibility due to the low oxygen content. The fully
pre-alloyed composition results in a homogeneous
microstructure and dimensional stability.

d
r
r
is

Astaloy CrM is a water atomized iron powder prealloyed with 3% Cr and 0.5% Mo exhibiting an
excellent hardenability. The low oxygen content gives a
good compressibility. Very high strength and hardness
can be achieved after sintering. Astaloy CrM is also
suitable for high temperature sintering, sinter hardening
and plasma nitriding. The fully pre-alloyed composition
results in a homogeneous microstructure with very good
properties.

eal
d
e

e-

17

Conditions for sample preparation and testing


Powder mixing

Alloying elements and lubricants used to establish the data in this manual have been
copper powder (-150m) or (-30m), nickel powder (Inco 123), Kropfmhl graphite
UF4 96/97% C, zinc stearate, amide wax and Kenolube P11. The type and amount
of lubricant and added alloying additives can be found at the bottom of each page
with sintered properties. If nothing else is indicated, sintered properties are evaluated
on plain mixes. Sintered data are for some materials evaluated on bonded mixes,
Starmix or in case of warm compaction, Densmix.
Compacting

Compaction was made in carbide dies. The spring back was measured on cylinder
specimens with a diameter of 25 mm and a height of 20 mm. Steel dies give a springback that is usually 0.03-0.07% larger.
The spring-back is also dependent on other factors such as geometrical shape and
dimensions of the compacted part, tool design, type and amount of lubricant and
alloying elements.
For warm compacted specimens, the powder was heated to 130C (266F) and the
tool die and punches were heated to 140C (284F). Spring-back for compaction was
calculated based on the diameter of the tool die at room temperature and diameter of
the specimens after cooling down to room temperature.
Sintering

The sintering was mainly carried out in 90 N2/10 H2 atmosphere but data are also
presented for material sintered in endothermic atmosphere (CO2: 0.6%), synthetic
DA (75 H2/25 N2) or in the case of sinter hardening 80 N2/20 H2 atmosphere.
Carbon values in the graphs represent combined carbon contents. A mesh belt furnace
was used for sintering up to 1150C (2100F). Sintering at temperatures above
1150C (2100F) was carried out in a lifting hearth batch furnace.

Sinter hardening

For sinter hardening higher cooling rates were obtained by convective cooling in a
mesh belt furnace.
Three settings on the convective cooling unit were used to obtain different cooling
rates, off, 15 Hz and 60 Hz. Cooling rates were estimated from the microstructure of
materials for which the structure at different cooling rates is known from dilatometer
studies. Variation in cooling rate between different specimens sintered with the same
settings of the convective cooling unit was found; however 1C/s (1.8F/s), 2.5C/s
(4.5F/s) and 5C/s (9F/s) are good approximations of the cooling rates.
Sinter hardened specimens were tempered at 200C (392F) for 60 min.
High temperature sintering with sinter hardening

The lifting hearth furnace used for high temperature sintering is equipped with a
convective cooling unit. This was used to generate data for the combination of high
temperature sintering and sinter hardening. In a similar way as for the belt furnace,
cooling rates were estimated by studying microstructures of known materials. Three
settings were used corresponding to cooling rates of 1C/s (1.8F/s), 2.5C/s (4.5F/s)
and 5C/s (9F/s).
High temperature sintered specimens were tempered at 200C (392F) for 60 min.
Case hardening

The parts were carburized at a temperature of 920C (1688F). Material (60


kg/batch) was inserted in the furnace while the carbon potential was kept at a low
level. When the material reached 920C the carbon potential was set to 0.8% by
adding propane. Carburizing time is defined as the length of time with propane added
to the atmosphere. After carburizing the material was quenched in oil at 60C
(140F). Tempering was carried out at 180C (355F) for 60 minutes.

Test methods for powder properties and chemical analysis

Testing of powder properties and chemical analysis is made according to the following
standards:
Apparent density
Flow
Sieve analysis
Compressibility
Green strength
Carbon
H2-loss

ISO 3923-1 : 1979


ISO 4490 : 2001
ISO 4497 : 1983
ISO 3927:
2001
ISO 3995 : 1985
ISO 9556:
ISO 4491-2 : 1997

1989

Test methods for mechanical properties

Tensile strength, yield strength, Youngs modulus, elongation, hardness and


dimensional change were measured on standard tensile test specimens (ISO 27401999) with a length of 90 mm. Serrated heads were used to improve the gripping of
the dogs on the tensile testing machine, except in the case of hardened materials. The
elongation was measured over a 25 mm gauge length. The hardness was tested with
the Vickers and Rockwell B or Rockwell C methods. Impact strength was determined
according to EN 10045-1. The specimens were un-notched impact specimens
according to ISO 5754. Dimensional change during sintering was measured over the
total length of the tensile test specimens (90 mm). The dimensional change was
determined from green size to sintered size or in the case of hardened materials, from
green to hardened size.
Metallography

Case depth was measured according to ISO 4507-2000. The effective case depth is
read from the curve representing the variation of Vickers hardness at the point
corresponding to 550 HV0.1.
All microhardness profiles in the curves presented for each base powder, are starting
on the same hardness value at the position 0.05 mm from the surface. This value is
based on the microhardness of martensite evaluated on a number of specimens. Close
to the surface, the carbon content (and thus the hardness of the martensite) should
exhibit only minor deviations from carbon potential (0.8%) of the carburizing
atmosphere, independent of the added graphite content and the carburizing time. The
values at the subsequent levels are microhardness values measured on individual
specimens. Ni-containing materials were etched in Picral and materials not containing
Ni were etched in Nital.

Modelling

Modelling
Design of experiment (DOE) methodology has been used to plan and
evaluate the experiments from which the material data originates. Three
level response surface models are utilized. From the model, each material
property is described by a polynomial based on the independent variables in
the investigation (such as density, combined carbon, sintering time etc.).
Properties are then predicted and plotted from this model. The predicted
properties do not exactly match the measured data, but a good estimation is
obtained. Advantages of this method are that any erroneous data points are
found during the data modelling and that properties can be evaluated on a
lower number of experiments and yet form a model with high accuracy.

21

Comments on Case Hardening


Material properties after case hardening operation are presented for ASC100.29,
Astaloy 85 Mo, Astaloy Mo, Distaloy AB, Distaloy AE, Distaloy DC, Distaloy DH
and Distaloy HP. These data show the response of a case hardening on these
materials.

Austenitizing and carburizing were carried out at 920C (1688F) for all materials
investigated. This temperature is recommended for Astaloy Mo and also for Distaloy
DC, Distaloy DH and Distaloy HP which are based on Astaloy Mo. Diffusion
alloyed grades based on pure iron powders such as Distaloy AB and Distaloy AE are
preferably austenitized at a somewhat lower temperature in the range 870C (1600F)
to 890C (1635F). A lower carburizing temperature will demand longer carburizing
time to obtain the same case depth.
Mechanical properties of a case hardened material are not homogeneous.
From the micro hardness profiles, it is observed that hardness decreases from the
surface to the center of the specimen. A similar behavior can also be expected for
tensile and yield strength while elongation can be assumed to increase with increasing
distance to the surface. Youngs modulus is mainly dependent on porosity and is
independent of the case hardening operation. Presented data on tensile strength, yield
strength and elongation should be viewed as a component test where the component
is a tensile test bar. Properties obtained are dependent on the dimensions of the
specimen.

Iron and steel powders for sintered components

Plain iron grades


Sponge Iron Powders
NC100.24
SC100.26
MH80.23

Atomized Iron Powders


AHC100.29
ASC100.29
ABC100.30

33

Iron and steel powders for sintered components

34

NC100.24

Sponge Iron Powders


NC100.24

35

Iron and steel powders for sintered components

36

NC100.24
g/cm3

Apparent density versus mixing time

3.0

1. Zn-stearate

2.9

2.8

2. Kenolube P11

2.7

3. Amide wax

2.6

2.5

2.4
2.3

10

40

30

20

50

Spring back versus compacting pressure

0.4

1. 0.8% Zn-stearate
0.3

2. 0.6% Kenolube P11

0.2
0.1
0.0

200

400

300

600

500

800

700

Green density versus compacting pressure

g/cm3
7.2

Lubricated die
0.8% Zn-stearate or
0.6% Kenolube P11

7.0

6.8

6.6

6.4

6.2

6.0

200
15

400

300
20

25

30

600

500
35

40

45

800

700
50

55

Compacting pressure (MPa and tsi)

37

Iron and steel powders for sintered components

NC100.24
103 psi

HV10

300

44

150

250

36

125

200

29

100

150

22

75

100

15

50

50

25

0
7.1

MPa

6.1

Tensile strength

6.3

6.5

6.7

6.9

103 psi

Yield strength

MPa

6.1

300

44

%
0.3

250

36

0.2

200

29

0.1

150

22

-0.0

100

15

-0.1

50

-0.2

0
7.1

-0.3

6.1

6.3

6.5

6.7

6.9

Hardness

6.3

6.5

6.7

6.9

7.1

6.9

7.1

Dimensional change

6.1

6.3

6.5

6.7

Sintered density (g/cm3)


Elongation

%
24

1120C (2050F)

21

1220C (2230F)

19
16
13
11
8

6.1

6.3

6.5

6.7

6.9

7.1

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11, P: 300, 500 and 700 MPa resp.
S: 1120C (2050F) and 1220C (2230F), 30 min in synthetic DA.
Dimensional change: Green to as sintered.

38

NC100.24

NC100.24 + C
103 psi

HV10

600

87

150

500

73

125

400

58

100

300

44

75

200

29

50

100

15

25

MPa

6.1

Tensile strength

6.3

6.5

6.7

6.9

103 psi

Yield strength

MPa

0
7.1

6.1

300

44

%
0.2

250

36

0.1

200

29

0.0

150

22

-0.1

100

15

-0.2

50

-0.3

0
7.1

-0.4

6.1

6.3

6.5

6.7

6.9

Hardness

6.3

6.5

6.7

6.9

7.1

6.9

7.1

Dimensional change

6.1

6.3

6.5

6.7

Sintered density (g/cm3)


Elongation

%
12

0.2% C

10

0.5% C
0.8% C

8
6
4
2
0

6.1

6.3

6.5

6.7

6.9

7.1

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11, P: 300, 500 and 700 MPa resp.
S: 1120C (2050F), 30 min in Endogas. Dimensional change: Green to as sintered.

39

Iron and steel powders for sintered components

NC100.24 + Cu
103 psi

HV10

400

58

150

350

51

125

300

44

100

250

36

75

200

29

50

150

22

25

15
7.0

MPa

100
6.0

Tensile strength

6.2

MPa

6.4

6.6

6.8

103 psi

Yield strength

6.0

300

44

%
1.2

250

36

1.0

200

29

0.8

150

22

0.6

100

15

0.4

50

0.2

6.0

6.2

6.4

6.6

6.8

0
7.0

Hardness

6.2

6.4

6.6

6.8

7.0

6.8

7.0

Dimensional change

0.0
6.0

6.2

6.4

6.6

Sintered density (g/cm3)


Elongation

%
12

2% Cu

10

4% Cu

8
6
4
2
0

6.0

6.2

6.4

6.6

6.8

7.0

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11, P: 300, 500 and 700 MPa resp.
S: 1120C (2050F), 30 min in synthetic DA. Dimensional change: Green to as sintered.

40

NC100.24

NC100.24 + 2% Cu + C
103 psi

HV10

600

87

200

500

73

175

400

58

150

300

44

125

200

29

100

100

15

75

MPa

6.0

Tensile strength

6.2

MPa

6.4

6.6

6.8

0
7.0

103 psi

Yield strength

50
6.0

600

87

%
0.6

500

73

0.5

400

58

0.4

300

44

0.3

200

29

0.2

100

15

0.1

6.0

6.2

6.4

6.6

6.8

0
7.0

Hardness

6.2

6.4

6.6

6.8

7.0

6.8

7.0

Dimensional change

0.0
6.0

6.2

6.4

6.6

Sintered density (g/cm3)


Elongation

%
12

0.2% C

10

0.6% C

8
6
4
2
0

6.0

6.2

6.4

6.6

6.8

7.0

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11, P: 300, 500 and 700 MPa resp.
S: 1120C, (2050F), 30 min in Endogas. Dimensional change: Green to as sintered.

41

Iron and steel powders for sintered components

NC100.24 + 4% Cu + C
103 psi

HV10

700

102

200

600

87

175

500

73

150

400

58

125

300

44

100

200

29

75

MPa

100
6.0

Tensile strength

6.2

MPa

6.4

6.6

6.8

15
7.0

103 psi

Yield strength

50
6.0

600

87

%
1.2

500

73

1.0

400

58

0.8

300

44

0.6

200

29

0.4

100

15

0.2

6.0

6.2

6.4

6.6

6.8

0
7.0

Hardness

6.2

6.4

6.6

6.8

7.0

6.8

7.0

Dimensional change

0.0
6.0

6.2

6.4

6.6

Sintered density (g/cm3)


Elongation

%
6

0.2% C

0.6% C

4
3
2
1
0

6.0

6.2

6.4

6.6

6.8

7.0

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11, P: 300, 500 and 700 MPa resp.
S: 1120C (2050F), 30 min in Endogas. Dimensional change: Green to as sintered.

42

NC100.24

NC100.24 + 2.5% Cu + 2.5% Ni


MPa

103 psi

Tensile strength

HV10

600

87

150

500

73

125

400

58

100

300

44

75

200

29

50

100

15

25

6.1

6.3

6.5

6.7

6.9

103 psi

Yield strength

MPa

0
7.1

6.1

600

87

%
0.6

500

73

0.4

400

58

0.2

300

44

-0.0

200

29

-0.2

100

15

-0.4

6.1

6.3

6.5

6.7

6.9

0
7.1

-0.6

Hardness

6.3

6.5

6.7

6.9

7.1

6.9

7.1

Dimensional change

6.1

6.3

6.5

6.7

Sintered density (g/cm3)


Elongation

%
12

1120C (2050F)

10

1220C (2230F)

8
6
4
2
0

6.1

6.3

6.5

6.7

6.9

7.1

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11, P: 300, 500 and 700 MPa resp.
S: 1120C (2050F) and 1220C (2230F), 30 min in synthetic DA.
Dimensional change: Green to as sintered.

43

Iron and steel powders for sintered components

NC100.24 + 2.5% Cu + 2.5% Ni + C


103 psi

HV10

700

102

200

600

87

175

500

73

150

400

58

125

300

44

100

200

29

75

MPa

100
6.0

Tensile strength

6.2

MPa

6.4

6.6

6.8

15
7.0

103 psi

Yield strength

50
6.0

600

87

%
0.6

500

73

0.5

400

58

0.4

300

44

0.3

200

29

0.2

100

15

0.1

6.0

6.2

6.4

6.6

6.8

0
7.0

Hardness

6.2

6.4

6.6

6.8

7.0

6.8

7.0

Dimensional change

0.0
6.0

6.2

6.4

6.6

Sintered density (g/cm3)


Elongation

%
6

0.2% C

0.6% C

4
3
2
1
0

6.0

6.2

6.4

6.6

6.8

7.0

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11, P: 300, 500 and 700 MPa resp.
S: 1120C (2050F), 30 min in Endogas. Dimensional change: Green to as sintered.

44

NC100.24

NC100.24 + 3% Ni
103 psi

HV10

400

58

150

350

51

125

300

44

100

250

36

75

200

29

50

150

22

25

15
7.3

MPa

100
6.3

Tensile strength

6.5

6.7

6.9

7.1

103 psi

Yield strength

MPa
300

44

%
-0.2

250

36

-0.4

200

29

-0.6

150

22

-0.8

100

15

-1.0

50

-1.2

0
7.3

-1.4

6.3

6.5

6.7

6.9

7.1

6.3

Hardness

6.5

6.7

6.9

7.1

7.3

7.1

7.3

Dimensional change

6.3

6.5

6.7

6.9

Sintered density (g/cm3)


Elongation

%
22

1120C (2050F)

19

1220C (2230F)

17
14
11
9
6

6.3

6.5

6.7

6.9

7.1

7.3

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11, P: 300, 500 and 700 MPa resp.
S: 1120C (2050F) and 1220C (2230F), 30 min in synthetic DA.
Dimensional change: Green to as sintered.

45

Iron and steel powders for sintered components

NC100.24 + Cu + C
103 psi

HV10

600

87

200

500

73

175

400

58

150

300

44

125

200

29

100

100

15

75

50

MPa

Tensile strength

103 psi

Yield strength

MPa

600

87

%
1.0

500

73

0.8

400

58

0.6

300

44

0.4

200

29

0.2

100

15

-0.0

-0.2

Hardness

Elongation
0.2% C

10

0.6% C

8
6
4
2
0

Copper content (%)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11, P: 500 MPa (density
approximately 6.6 g/cm3) S: 1120C (2050F), 30 min in Endogas.
Dimensional change: Green to as sintered.

46

Dimensional change

Copper content (%)


%
12

SC100.26

SC100.26

47

Iron and steel powders for sintered components

48

SC100.26
g/cm

Apparent density versus mixing time

3.2

1. Zn-stearate

3.1

2. Kenolube P11

3.0
2.9

2.8

3. Amide wax

2.7
2.6
2.5

10

40

30

20

50

Spring back versus compacting pressure

0.4

1. 0.8% Zn-stearate

0.3

2. 0.6% Kenolube P11

1
2

0.2
0.1
0.0

200

400

300

600

500

800

700

Green density versus compacting pressure

g/cm
7.4

Lubricated die
0.8% Zn-stearate or
0.6% Kenolube P11

7.2

7.0

6.8

6.6

6.4

6.2

200

400

300
20

25

30

600

500
35

40

45

800

700
50

55

Compacting pressure (MPa and tsi)

49

Iron and steel powders for sintered components

SC100.26
103 psi

HV10

300

44

150

250

36

125

200

29

100

150

22

75

100

15

50

50

25

MPa

6.3

Tensile strength

6.5

MPa

6.7

6.9

7.1

0
7.3

103 psi

Yield strength

0
6.3

44

%
0.3

250

36

0.2

200

29

0.1

150

22

-0.0

100

15

-0.1

50

-0.2

6.3

6.5

6.7

6.9

7.1

0
7.3

6.5

6.7

6.9

7.1

7.3

7.1

7.3

Dimensional change

300

Hardness

-0.3
6.3

6.5

6.7

6.9

Sintered density (g/cm3)


Elongation

%
24

1120C (2050F)

21

1220C (2230F)

19
16
13
11
8

6.3

6.5

6.7

6.9

7.1

7.3

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11, P: 300, 500 and 700 MPa resp.
S: 1120C (2050F) and 1220C (2230F), 30 min in synthetic DA.
Dimensional change: Green to as sintered.

50

SC100.26

SC100.26 + C
103 psi

HV10

400

58

150

350

51

125

300

44

100

250

36

75

200

29

50

150

22

25

15
7.3

MPa

100
6.3

Tensile strength

6.5

MPa

6.7

6.9

7.1

103 psi

Yield strength

6.3

300

44

%
0.3

250

36

0.2

200

29

0.1

150

22

-0.0

100

15

-0.1

50

-0.2

0
7.3

-0.3

6.3

6.5

6.7

6.9

7.1

Hardness

6.5

6.7

6.9

7.1

7.3

7.1

7.3

Dimensional change

6.3

6.5

6.7

6.9

Sintered density (g/cm3)


Elongation

%
12

0.2% C

10

0.5% C
0.8% C

8
6
4
2
0

6.3

6.5

6.7

6.9

7.1

7.3

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11, P: 300, 500 and 700 MPa resp.
S: 1120C (2050F), 30 min in Endogas. Dimensional change: Green to as sintered.

51

Iron and steel powders for sintered components

SC100.26 + Cu
MPa

103 psi

HV10

400

58

150

350

51

125

300

44

100

250

36

75

200

29

50

150

22

25

15

Tensile strength

100
6.1

6.3

MPa

6.5

6.7

6.9

7.1

103 psi

Yield strength

6.1

300

44

%
1.2

250

36

1.0

200

29

0.8

150

22

0.6

100

15

0.4

50

0.2

6.1

6.3

6.5

6.7

6.9

0
7.1

Hardness

6.3

6.5

6.7

6.9

7.1

6.9

7.1

Dimensional change

0.0
6.1

6.3

6.5

6.7

Sintered density (g/cm3)


Elongation

12
2% Cu

10

4% Cu

8
6
4
2
0

6.1

6.3

6.5

6.7

6.9

7.1

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11, P: 300, 500 and 700 MPa resp.
S: 1120C (2050F), 30 min in synthetic DA. Dimensional change: Green to as sintered.

52

SC100.26

SC100.26 + 2% Cu + C
103 psi

HV10

600

87

200

500

73

175

400

58

150

300

44

125

200

29

100

100

15

75

50
6.2

MPa

0
6.2

Tensile strength

6.4

MPa

6.6

6.8

7.0

7.2

103 psi

Yield strength

600

87

%
0.6

500

73

0.5

400

58

0.4

300

44

0.3

200

29

0.2

100

15

0.1

6.2

6.4

6.6

6.8

7.0

0
7.2

Hardness

6.4

6.6

6.8

7.0

7.2

7.0

7.2

Dimensional change

0.0
6.2

6.4

6.6

6.8

Sintered density (g/cm3)


Elongation

%
12

0.2% C

10

0.6% C

8
6
4
2
0

6.2

6.4

6.6

6.8

7.0

7.2

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11, P: 300, 500 and 700 MPa resp.
S: 1120C (2050F), 30 min in Endogas. Dimensional change: Green to as sintered.

53

Iron and steel powders for sintered components

SC100.26 + 4% Cu + C
103 psi

HV10

700

102

200

600

87

175

500

73

150

400

58

125

300

44

100

200

29

75

15

50
6.1

MPa

100
6.1

Tensile strength

6.3

MPa

6.5

6.7

6.9

7.1

103 psi

Yield strength

600

87

%
0.9

500

73

0.8

400

58

0.7

300

44

0.6

200

29

0.5

100

15

0.4

6.1

6.3

6.5

6.7

6.9

0
7.1

0.3

Hardness

6.3

6.5

6.7

6.9

7.1

6.9

7.1

Dimensional change

6.1

6.3

6.5

6.7

Sintered density (g/cm3)


Elongation

%
6

0.2% C

0.6% C

4
3
2
1
0

6.1

6.3

6.5

6.7

6.9

7.1

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11, P: 300, 500 and 700 MPa resp.
S: 1120C (2050F), 30 min in Endogas. Dimensional change: Green to as sintered.

54

SC100.26

SC100.26 + 2.5% Cu + 2.5% Ni


103 psi

HV10

600

87

150

500

73

125

400

58

100

300

44

75

200

29

50

100

15

25

MPa

Tensile strength

0
6.3

6.5

MPa

6.7

6.9

7.1

7.3

103 psi

Yield strength

0
6.3

87

%
0.5

500

73

0.4

400

58

0.3

300

44

0.2

200

29

0.1

100

15

-0.0

6.3

6.5

6.7

6.9

7.1

0
7.3

6.5

6.7

6.9

7.1

7.3

7.1

7.3

Dimensional change

600

Hardness

-0.1
6.3

6.5

6.7

6.9

Sintered density (g/cm3)


Elongation

%
12

1120C (2050F)

10

1220C (2230F)

8
6
4
2
0

6.3

6.5

6.7

6.9

7.1

7.3

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11, P: 300, 500 and 700 MPa resp.
S: 1120C (2050F) and 1220C (2230F), 30 min in synthetic DA.
Dimensional change: Green to as sintered.

55

Iron and steel powders for sintered components

SC100.26 + 2.5% Cu + 2.5% Ni + C


103 psi

HV10

700

102

200

600

87

175

500

73

150

400

58

125

300

44

100

200

29

75

15

50
6.3

MPa

100
6.3

Tensile strength

6.5

MPa

6.7

6.9

7.1

7.3

103 psi

Yield strength

600

87

%
0.6

500

73

0.5

400

58

0.4

300

44

0.3

200

29

0.2

100

15

0.1

6.3

6.5

6.7

6.9

7.1

0
7.3

0.0

Hardness

6.5

6.7

6.9

7.1

7.3

7.1

7.3

Dimensional change

6.3

6.5

6.7

6.9

Sintered density (g/cm3)


Elongation

%
6

0.2% C

0.6% C

4
3
2
1
0

6.3

6.5

6.7

6.9

7.1

7.3

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11, P: 300, 500 and 700 MPa resp.
S: 1120C (2050F), 30 min in Endogas. Dimensional change: Green to as sintered.

56

SC100.26

SC100.26 + 3% Ni
103 psi

HV10

400

58

150

350

51

125

300

44

100

250

36

75

200

29

50

150

22

25

15

MPa

100
6.4

Tensile strength

6.6

MPa

6.8

7.0

7.2

7.4

103 psi

Yield strength

300

44

%
0.2

250

36

-0.0

200

29

-0.2

150

22

-0.4

100

15

-0.6

50

-0.8

6.4

6.6

6.8

7.0

7.2

0
7.4

6.4

Hardness

6.6

6.8

7.0

7.2

7.4

7.2

7.4

Dimensional change

-1.0
6.4

6.6

6.8

7.0

Sintered density (g/cm3)


Elongation

%
22

1120C (2050F)

19

1220C (2230F)

17
14
11
9
6
6.4

6.6

6.8

7.0

7.2

7.4

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11, P: 300, 500 and 700 MPa resp.
S: 1120C (2050F) and 1220C (2230F), 30 min in synthetic DA.
Dimensional change: Green to as sintered.

57

Iron and steel powders for sintered components

SC100.26 + Cu + C
103 psi

HV10

600

87

200

500

73

175

400

58

150

300

44

125

200

29

100

100

15

75

50

MPa

Tensile strength

MPa

103 psi

Yield strength

87

%
1.0

500

73

0.8

400

58

0.6

300

44

0.4

200

29

0.2

100

15

-0.0

-0.2

Dimensional change

600

Hardness

Copper content (%)


Elongation

%
12

0.2% C

10

0.6% C

8
6
4
2
0

Copper content (%)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11, P: 500 MPa Density approximately
6.9 g/cm3 S: 1120C (2050F), 30 min in Endogas. Dimensional change: Green to as sintered.

58

MH80.23

MH80.23

59

Iron and steel powders for sintered components

60

MH80.23
g/cm3

Apparent density versus mixing time

2.8

1. Zn-stearate

2.7
2.6

2. Kenolube P11

1
2
3

2.5
2.4

3. Amide wax

2.3
2.2
2.1

10

40

30

20

50

Spring back versus compacting pressure

0.3

1. 0.8% Zn-stearate
2. 0.6% Kenolube P11

0.2

0.1

0.0

200

100

g/cm3

400

300

600

500

700

Green density versus compacting pressure

7.0

Lubricated die
0.8% Zn-steatare or
0.6% Kenolube P11

6.8
6.6
6.4
6.2
6.0
5.8
5.6
5.4
5.2

200

100
10

15

400

300
20

25

30

600

500
35

40

45

700
50

Compacting pressure (MPa and tsi)

61

Iron and steel powders for sintered components

MH80.23 + C (1050C)
103 psi

HV10

300

44

150

250

36

125

200

29

100

150

22

75

100

15

50

50

25

MPa

0
5.0

Tensile strength

5.5

MPa

6.0

6.5

7.0

7.5

103 psi

Yield strength

0
5.0

44

%
0.3

250

36

0.2

200

29

0.1

150

22

-0.0

100

15

-0.1

50

-0.2

-0.3
5.0

5.5

6.0

6.5

7.0

7.5

5.5

6.0

6.5

5.5

6.0

6.5

Sintered density (g/cm3)


Elongation

%
7

0% C (DA)

0.5% C
0.8% C

5
4
3
2
1
5.0

5.5

6.0

6.5

7.0

7.5

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.75% Kenolube P11, P: 196, 392 and 589 MPa resp.
S: 1050C (1920F), 30 min in synthetic DA or Endogas (0.5 - 0.8% C).
Dimensional change: Green to as sintered.

62

7.0

7.5

7.0

7.5

Dimensional change

300

0
5.0

Hardness

MH80.23

MH80.23 + C (1120C)
103 psi

HV10

350

51

150

300

44

125

250

36

100

200

29

75

150

22

50

100

15

25

MPa

50
5.0

Tensile strength

5.5

MPa

6.0

6.5

7.0

7.5

103 psi

Yield strength

0
5.0

44

%
-0.0

250

36

-0.1

200

29

-0.2

150

22

-0.3

100

15

-0.4

50

-0.5

-0.6
5.0

5.5

6.0

6.5

7.0

7.5

5.5

6.0

6.5

7.0

7.5

7.0

7.5

Dimensional change

300

0
5.0

Hardness

5.5

6.0

6.5

Sintered density (g/cm3)


Elongation

%
7

0.2% C

0.5% C
0.8% C

5
4
3
2
1
5.0

5.5

6.0

6.5

7.0

7.5

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.75% Kenolube P11, P: 196, 392 and 589 MPa resp.
S: 1120C (2050F), 30 min in Endogas. Dimensional change: Green to as sintered.

63

Iron and steel powders for sintered components

MH80.23 + 2% Cu + C (1050C)
103 psi

HV10

350

51

150

300

44

125

250

36

100

200

29

75

150

22

50

100

15

25

MPa

50
5.0

Tensile strength

5.5

MPa

6.0

6.5

7.0

7.5

103 psi

Yield strength

0
5.0

44

%
0.3

250

36

0.2

200

29

0.1

150

22

-0.0

100

15

-0.1

50

-0.2

-0.3
5.0

5.5

6.0

6.5

7.0

7.5

5.5

6.0

6.5

5.5

6.0

6.5

Sintered density (g/cm3)


Elongation

%
7

0% C (DA)

0.5% C
0.8% C

5
4
3
2
1
5.0

5.5

6.0

6.5

7.0

7.5

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.75% Kenolube P11, P: 196, 392 and 589 MPa resp.
S: 1050C (1920F), 30 min in synthetic DA or Endogas (0.5 - 0.8% C).
Dimensional change: Green to as sintered.

64

7.0

7.5

7.0

7.5

Dimensional change

300

0
5.0

Hardness

MH80.23

MH80.23 + 2% Cu + C (1120C)
103 psi

HV10

600

87

175

500

73

150

400

58

125

300

44

100

200

29

75

100

15

50

25
5.0

MPa

0
5.0

Tensile strength

5.5

6.0

6.5

7.0

103 psi

Yield strength

MPa

7.5

87

%
0.3

500

73

0.2

400

58

0.1

300

44

-0.0

200

29

-0.1

100

15

-0.2

-0.3
5.0

5.5

6.0

6.5

7.0

7.5

5.5

6.0

6.5

7.0

7.5

7.0

7.5

Dimensional change

600

0
5.0

Hardness

5.5

6.0

6.5

Sintered density (g/cm3)


Elongation

6
0.2% C

0.5% C
0.8% C

4
3
2
1
0
5.0

5.5

6.0

6.5

7.0

7.5

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.75% Kenolube P11, P: 196, 392 and 589 MPa resp.
S: 1120C (2050F), 30 min in Endogas. Dimensional change: Green to as sintered.

65

Iron and steel powders for sintered components

MH80.23 + 5% Cu + C (1050C)
103 psi

HV10

600

87

150

500

73

125

400

58

100

300

44

75

200

29

50

100

15

25

MPa

0
5.0

Tensile strength

5.5

MPa

6.0

6.5

7.0

7.5

103 psi

Yield strength

0
5.0

87

%
0.3

500

73

0.2

400

58

0.1

300

44

-0.0

200

29

-0.1

100

15

-0.2

-0.3
5.0

5.5

6.0

6.5

7.0

7.5

5.5

6.0

6.5

5.5

6.0

6.5

Sintered density (g/cm3)


Elongation

%
6

0% C (DA)

0.5% C
0.8% C

4
3
2
1
0
5.0

5.5

6.0

6.5

7.0

7.5

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.75% Kenolube P11, P: 196, 392 and 589 MPa resp.
S: 1050C (1920F), 30 min in synthetic DA or Endogas (0.5 - 0.8% C).
Dimensional change: Green to as sintered.

66

7.0

7.5

7.0

7.5

Dimensional change

600

0
5.0

Hardness

MH80.23

MH80.23 + 5% Cu + C (1120C)
103 psi

HV10

600

87

300

500

73

250

400

58

200

300

44

150

200

29

100

100

15

50

MPa

0
5.0

Tensile strength

5.5

MPa

6.0

6.5

7.0

7.5

103 psi

Yield strength

0
5.0

87

%
2.0

500

73

1.5

400

58

1.0

300

44

0.5

200

29

0.0

100

15

-0.5

-1.0
5.0

5.5

6.0

6.5

7.0

7.5

5.5

6.0

6.5

7.0

7.5

7.0

7.5

Dimensional change

600

0
5.0

Hardness

5.5

6.0

6.5

Sintered density (g/cm3)


Elongation

%
6

0.2% C

0.5% C
0.8% C

4
3
2
1
0
5.0

5.5

6.0

6.5

7.0

7.5

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.75% Kenolube P11, P: 196, 392 and 589 MPa resp.
S: 1120C (2050F), 30 min in Endogas. Dimensional change: Green to as sintered.

67

Iron and steel powders for sintered components

MH80.23 + 8% Cu + C (1050C)
103 psi

HV10

600

87

175

500

73

150

400

58

125

300

44

100

200

29

75

100

15

50

25
5.0

MPa

0
5.0

Tensile strength

5.5

MPa

6.0

6.5

7.0

7.5

103 psi

Yield strength

87

%
0.3

500

73

0.2

400

58

0.1

300

44

-0.0

200

29

-0.1

100

15

-0.2

-0.3
5.0

5.5

6.0

6.5

7.0

7.5

5.5

6.0

6.5

5.5

6.0

6.5

Sintered density (g/cm3)


Elongation

%
6

0% C (DA)

0.5% C
0.8% C

4
3
2
1
0
5.0

5.5

6.0

6.5

7.0

7.5

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.75% Kenolube P11, P: 196, 392 and 589 MPa resp.
S: 1050C (1920F), 30 min in synthetic DA or Endogas (0.5 - 0.8% C).
Dimensional change: Green to as sintered.

68

7.0

7.5

7.0

7.5

Dimensional change

600

0
5.0

Hardness

MH80.23

MH80.23 + 8% Cu + C (1120C)
103 psi

HV10

600

87

175

500

73

150

400

58

125

300

44

100

200

29

75

100

15

50

25
5.0

MPa

0
5.0

Tensile strength

5.5

MPa

6.0

6.5

7.0

7.5

103 psi

Yield strength

87

%
2.0

500

73

1.5

400

58

1.0

300

44

0.5

200

29

0.0

100

15

-0.5

-1.0
5.0

5.5

6.0

6.5

7.0

7.5

5.5

6.0

6.5

7.0

7.5

7.0

7.5

Dimensional change

600

0
5.0

Hardness

5.5

6.0

6.5

Sintered density (g/cm3)


Elongation

6
0.2% C

0.5% C
0.8% C

4
3
2
1
0
5.0

5.5

6.0

6.5

7.0

7.5

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.75% Kenolube P11, P: 196, 392 and 589 MPa resp.
S: 1120C (2050F), 30 min in Endogas. Dimensional change: Green to as sintered.

69

Iron and steel powders for sintered components

MH80.23 + 0.45% P + C (1050C)


103 psi

HV10

600

87

175

500

73

150

400

58

125

300

44

100

200

29

75

100

15

50

MPa

5.0

Tensile strength

5.5

MPa

6.0

6.5

7.0

0
7.5

103 psi

Yield strength

25

600

87

%
0.6

500

73

0.4

400

58

0.2

300

44

-0.0

200

29

-0.2

100

15

-0.4

5.0

5.5

6.0

6.5

7.0

0
7.5

-0.6

5.0

Hardness

5.5

6.0

6.5

5.0

5.5

6.0

6.5

Elongation
0% C (DA)

0.5% C
0.8% C

5
4
3
2
1

5.0

5.5

6.0

6.5

7.0

7.5

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.75% Kenolube P11, P: 196, 392 and 589 MPa resp.
S: 1050C (1920F), 30 min in synthetic DA or Endogas (0.5 - 0.8% C).
Dimensional change: Green to as sintered.

70

7.5

7.0

7.5

Dimensional change

Sintered density (g/cm3)


%
7

7.0

MH80.23

MH80.23 + 0.45% P + C (1120C)


103 psi

HV10

600

87

175

500

73

150

400

58

125

300

44

100

200

29

75

100

15

50

25
5.0

MPa

0
5.0

Tensile strength

5.5

MPa

6.0

6.5

7.0

7.5

103 psi

Yield strength

87

%
0.6

500

73

0.4

400

58

0.2

300

44

-0.0

200

29

-0.2

100

15

-0.4

-0.6
5.0

5.5

6.0

6.5

7.0

7.5

5.5

6.0

6.5

7.0

7.5

7.0

7.5

Dimensional change

600

0
5.0

Hardness

5.5

6.0

6.5

Sintered density (g/cm3)


Elongation

%
6

0.2% C

0.5% C
0.8% C

4
3
2
1
0
5.0

5.5

6.0

6.5

7.0

7.5

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.75% Kenolube P11, P: 196, 392 and 589 MPa resp.
S: 1120C (2050F), 30 min in Endogas. Dimensional change: Green to as sintered.

71

Iron and steel powders for sintered components

MH80.23 + 2% Cu + 0.45% P + C (1050C)


103 psi

HV10

600

87

175

500

73

150

400

58

125

300

44

100

200

29

75

100

15

50

25
5.0

MPa

0
5.0

Tensile strength

5.5

MPa

6.0

6.5

7.0

7.5

103 psi

Yield strength

87

%
0.6

500

73

0.4

400

58

0.2

300

44

-0.0

200

29

-0.2

100

15

-0.4

-0.6
5.0

5.5

6.0

6.5

7.0

7.5

5.5

6.0

6.5

5.5

6.0

6.5

Sintered density (g/cm3)


Elongation

%
6

0% C (DA)

0.5% C
0.8% C

4
3
2
1
0
5.0

5.5

6.0

6.5

7.0

7.5

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.75% Kenolube P11, P: 196, 392 and 589 MPa resp.
S: 1050C (1920F), 30 min in synthetic DA or Endogas (0.5 - 0.8% C).
Dimensional change: Green to as sintered.

72

7.0

7.5

7.0

7.5

Dimensional change

600

0
5.0

Hardness

MH80.23

MH80.23 + 2% Cu + 0.45% P + C (1120C)


103 psi

HV10

600

87

300

500

73

250

400

58

200

300

44

150

200

29

100

100

15

50

MPa

0
5.0

Tensile strength

5.5

MPa

6.0

6.5

7.0

7.5

103 psi

Yield strength

0
5.0

87

%
0.2

500

73

0.1

400

58

0.0

300

44

-0.1

200

29

-0.2

100

15

-0.3

-0.4
5.0

5.5

6.0

6.5

7.0

7.5

5.5

6.0

6.5

7.0

7.5

7.0

7.5

Dimensional change

600

0
5.0

Hardness

5.5

6.0

6.5

Sintered density (g/cm3)


Elongation

%
6

0.2% C

0.5% C
0.8% C

4
3
2
1
0
5.0

5.5

6.0

6.5

7.0

7.5

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.75% Kenolube P11, P: 196, 392 and 589 MPa resp.
S: 1120C (2050F), 30 min in Endogas. Dimensional change: Green to as sintered.

73

Iron and steel powders for sintered components

MH80.23 + 5% Cu + 0.45% P + C (1050C)


103 psi

HV10

600

87

200

500

73

175

400

58

150

300

44

125

200

29

100

100

15

75

50
5.0

MPa

0
5.0

Tensile strength

5.5

MPa

6.0

6.5

7.0

7.5

103 psi

Yield strength

87

%
0.6

500

73

0.4

400

58

0.2

300

44

-0.0

200

29

-0.2

100

15

-0.4

-0.6
5.0

5.5

6.0

6.5

7.0

7.5

5.5

6.0

6.5

5.5

6.0

6.5

Sintered density (g/cm3)


Elongation

%
6

0% C (DA)

0.5% C
0.8% C

4
3
2
1
0
5.0

5.5

6.0

6.5

7.0

7.5

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.75% Kenolube P11, P: 196, 392 and 589 MPa resp.
S: 1050C (1920F), 30 min in synthetic DA or Endogas (0.5 - 0.8% C).
Dimensional change: Green to as sintered.

74

7.0

7.5

7.0

7.5

Dimensional change

600

0
5.0

Hardness

MH80.23

MH80.23 + 5% Cu + 0.45% P + C (1120C)


103 psi

HV10

700

102

300

600

87

250

500

73

200

400

58

150

300

44

100

200

29

50

MPa

100
5.0

Tensile strength

5.5

MPa

6.0

6.5

7.0

7.5

15

103 psi

Yield strength

0
5.0

87

%
0.6

500

73

0.4

400

58

0.2

300

44

-0.0

200

29

-0.2

100

15

-0.4

-0.6
5.0

5.5

6.0

6.5

7.0

7.5

5.5

6.0

6.5

7.0

7.5

7.0

7.5

Dimensional change

600

0
5.0

Hardness

5.5

6.0

6.5

Sintered density (g/cm3)


Elongation

%
6

0.2% C

0.5% C
0.8% C

4
3
2
1
0
5.0

5.5

6.0

6.5

7.0

7.5

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.75% Kenolube P11, P: 196, 392 and 589 MPa resp.
S: 1120C (2050F), 30 min in Endogas. Dimensional change: Green to as sintered.

75

Iron and steel powders for sintered components

MH80.23 + 8% Cu + 0.45% P + C (1050C)


103 psi

HV10

600

87

200

500

73

175

400

58

150

300

44

125

200

29

100

100

15

75

50
5.0

MPa

0
5.0

Tensile strength

5.5

6.0

6.5

7.0

103 psi

Yield strength

MPa

7.5

87

%
0.6

500

73

0.4

400

58

0.2

300

44

-0.0

200

29

-0.2

100

15

-0.4

-0.6
5.0

5.5

6.0

6.5

7.0

7.5

5.5

6.0

6.5

5.5

6.0

6.5

Sintered density (g/cm3)


Elongation

6
0% C (DA)

0.5% C
0.8% C

4
3
2
1
0
5.0

5.5

6.0

6.5

7.0

7.5

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.75% Kenolube P11, P: 196, 392 and 589 MPa resp.
S: 1050C (1920F), 30 min in synthetic DA or Endogas (0.5 - 0.8% C).
Dimensional change: Green to as sintered.

76

7.0

7.5

7.0

7.5

Dimensional change

600

0
5.0

Hardness

MH80.23

MH80.23 + 8% Cu + 0.45% P + C (1120C)


103 psi

HV10

600

87

300

500

73

250

400

58

200

300

44

150

200

29

100

100

15

50

MPa

0
5.0

Tensile strength

5.5

MPa

6.0

6.5

7.0

7.5

103 psi

Yield strength

0
5.0

87

%
0.3

500

73

0.1

400

58

-0.1

300

44

-0.3

200

29

-0.5

100

15

-0.7

-0.9
5.0

5.5

6.0

6.5

7.0

7.5

5.5

6.0

6.5

7.0

7.5

7.0

7.5

Dimensional change

600

0
5.0

Hardness

5.5

6.0

6.5

Sintered density (g/cm3)


Elongation

6
0.2% C

0.5% C
0.8% C

4
3
2
1
0
5.0

5.5

6.0

6.5

7.0

7.5

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.75% Kenolube P11, P: 196, 392 and 589 MPa resp.
S: 1120C (2050F), 30 min in Endogas. Dimensional change: Green to as sintered.

77

Iron and steel powders for sintered components

78

AHC100.29

AHC100.29

79

Iron and steel powders for sintered components

80

AHC100.29
g/cm3

Apparent density versus mixing time

3.5

1. Zn-stearate

3.4

3.3

2. Amide wax

3.2
3.1

3.0
2.9
2.8

10

40

30

20

50

Spring back versus compacting pressure

0.4

1. 0.8% Zn-stearate

0.3

2. 0.6% Kenolube P11

1
2

0.2
0.1
0.0

400

300

g/cm3

600

500

900

800

700

Green density versus compacting pressure

7.6

Lubricated die
0.8% Zn-stearate
0.6% Kenolube P11

7.4

7.2

7.0

6.8

6.6

400

300
25

30

600

500
35

40

45

900

800

700
50

55

60

Compacting pressure (MPa and tsi)

81

Iron and steel powders for sintered components


1120C (2050F)
1250C (2280F)

AHC100.29
103 psi

HV10

44

150

36

125

200

29

100

150

22

75

100

15

50

50

25

0
7.5

MPa
300

Tensile str.

250

Tensile and Yield strength

Yield str

6.5

6.7

6.9

7.1

7.3

6.5

Hardness

6.7

6.9

7.1

7.3

7.5

106 psi

29.0

120

180

26.1

100

73.7

160

23.2

80

59.0

140

20.3

60

44.2

120

17.4

40

29.5

100

14.5

20

14.7

80

11.6
7.5

GPa

Young's modulus

200

6.5

6.7

6.9

7.1

7.3

0.1

18

0.0

15

-0.1

12

-0.2

-0.3

6.6

6.8

7.0

7.2

Sintered density (g/cm)

6.8

7.4

7.6

-0.4

7.0

7.2

88.4

7.4

7.6

7.4

7.6

0.0

Dimensional change

0.2

21

6.6

Elongation

24

Ft lb

Impact energy

6.6

6.8

7.0

7.2

Sintered density (g/cm)

MANUFACTURING CONDITIONS: 0.8% Amide wax; P: 400 - 800 MPa conventional compaction,
S: 1120C (2050F) and 1250C (2280F), 30 min in 90/10 N2/H2. Dimensional change: Green to as sintered.

82

AHC100.29
0% C
0.5% C
0.8% C

AHC100.29 + C
103 psi

HV10

87

300

73

250

400

58

200

70

300

44

150

60

200

29

100

50

100

15

50

40

MPa
600
500

6.5

Tensile and Yield strength


Tensile str.

Yield str

6.7

6.9

7.1

7.3

0
7.5

6.5

HRB

Hardness

90

HV10
HRB

6.7

80

6.9

7.1

7.3

7.5

30

106 psi

29.0

90

180

26.1

75

55.2

160

23.2

60

44.2

140

20.3

45

33.1

120

17.4

30

22.1

100

14.5

15

11.0

11.6
7.5

GPa

Young's modulus

200

80

6.5

6.7

6.9

7.1

7.3

0.2

12

0.1

0.0

-0.1

-0.2

6.5

6.7

6.9

7.1

Sintered density (g/cm3)

7.3

7.5

-0.3

6.9

7.1

66.3

7.3

7.5

7.3

7.5

0.0

Dimensional change

0.3

15

6.7

Elongation

18

6.5

Ft lb

Impact energy

6.5

6.7

6.9

7.1

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Amide wax; P: 400 - 800 MPa conventional compaction,
S: 1120C (2050F), 30 min in 90/10 N2/H2. Dimensional change: Green to as sintered.

83

Iron and steel powders for sintered components


0% Cu
2% Cu
5% Cu

AHC100.29 + Cu
103 psi

HV10

87

150

73

125

400

58

100

70

300

44

75

60

200

29

50

50

100

15

25

40

MPa
600
500

6.5

Tensile and Yield strength


Tensile str.
Yield str

6.7

6.9

7.1

7.3

7.5

6.5

HRB

Hardness

90

HV10
HRB

6.7

80

6.9

7.1

7.3

7.5

30

106 psi

29.0

90

180

26.1

75

55.2

160

23.2

60

44.2

140

20.3

45

33.1

120

17.4

30

22.1

100

14.5

15

11.0

11.6
7.5

GPa

Young's modulus

200

80

6.5

6.7

6.9

7.1

7.3

2.0

12

1.5

1.0

0.5

0.0

6.5

6.7

6.9

7.1

Sintered density (g/cm)

6.7

7.3

7.5

-0.5

6.9

7.1

66.3

7.3

7.5

7.3

7.5

Dimensional change

2.5

15

6.5

Elongation

18

Ft lb

Impact energy

6.5

6.7

6.9

7.1

Sintered density (g/cm)

MANUFACTURING CONDITIONS: 0.8% Amide wax; P: 400 - 800 MPa conventional compaction,
S: 1120C (2050F), 30 min in 90/10 N2/H2. Dimensional change: Green to as sintered.

84

0.0

AHC100.29
0.2% C
0.5% C
0.8% C

AHC100.29 + 2% Cu + C
103 psi

HV10

102

225

87

200

500

73

175

70

400

58

150

60

300

44

125

50

200

29

100

40

15
7.5

75

MPa
700
600

100
6.5

Tensile and Yield strength


Tensile str.
Yield str

6.7

6.9

7.1

7.3

6.5

HRB

Hardness

90

HV10
HRB

6.7

80

6.9

7.1

7.3

7.5

30

106 psi

29.0

60

180

26.1

50

36.8

160

23.2

40

29.5

140

20.3

30

22.1

120

17.4

20

14.7

100

14.5

10

7.4

11.6
7.5

GPa

Young's modulus

200

80

6.5

6.7

6.9

7.1

7.3

0.5

0.4

0.3

0.2

0.1

6.5

6.7

6.9

7.1

Sintered density (g/cm3)

6.7

7.3

7.5

0.0

6.9

7.1

44.2

7.3

7.5

7.3

7.5

0.0

Dimensional change

0.6

6.5

Elongation

Ft lb

Impact energy

6.5

6.7

6.9

7.1

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Amide wax; P: 400 - 800 MPa conventional compaction,
S: 1120 C (2050F), 30 min in 90/10 N2/H2. Dimensional change: Green to as sintered.

85

Iron and steel powders for sintered components


15 minutes
30 minutes
45 minutes

AHC100.29 + 2% Cu + 0.8% C
103 psi

HV10

102

250

87

225

500

73

200

70

400

58

175

60

300

44

150

50

200

29

125

40

100
6.5

15

100
6.5

MPa
700
600

Tensile and Yield strength

6.7

6.9

7.1

7.3

7.5

90

HV10
HRB

Tensile str.
Yield str

HRB

Hardness

6.7

80

6.9

7.1

7.3

7.5

30

106 psi

29.0

60

180

26.1

50

36.8

160

23.2

40

29.5

140

20.3

30

22.1

120

17.4

20

14.7

100

14.5

10

7.4

11.6
7.5

GPa

Young's modulus

200

80

6.5

6.7

6.9

7.1

7.3

0.2

0.1

0.0

-0.1

-0.2

6.5

6.7

6.9

7.1

Sintered density (g/cm)

6.7

7.3

7.5

-0.3

6.9

7.1

44.2

7.5

6.5

6.7

6.9

7.1

7.3

7.5

Sintered density (g/cm)

MANUFACTURING CONDITIONS: 0.8% Amide wax; P: 400 - 800 MPa conventional compaction,
S: 1120C (2050F), various time in 90/10 N2/H2. Dimensional change: Green to as sintered.

86

0.0

7.3

Dimensional change

0.3

6.5

Elongation

Ft lb

Impact energy

AHC100.29
0.2% C
0.5% C
0.8% C

AHC100.29 + 5% Cu + C
103 psi

HV10

116

250

102

225

600

87

200

70

500

73

175

60

400

58

150

50

300

44

125

40

29

100
6.5

MPa
800
700

200
6.5

Tensile and Yield strength


Tensile str.
Yield str

6.7

6.9

7.1

7.3

7.5

HRB

Hardness

90

HV10
HRB

6.7

80

6.9

7.1

7.3

7.5

30

106 psi

29.0

60

180

26.1

50

36.8

160

23.2

40

29.5

140

20.3

30

22.1

120

17.4

20

14.7

100

14.5

10

7.4

11.6
7.5

GPa

Young's modulus

200

80

6.5

6.7

6.9

7.1

7.3

1.5

1.2

0.9

0.6

0.3

6.5

6.7

6.9

7.1

Sintered density (g/cm)

6.7

7.3

7.5

0.0

6.9

7.1

44.2

7.3

7.5

7.3

7.5

0.0

Dimensional change

1.8

6.5

Elongation

Ft lb

Impact energy

6.5

6.7

6.9

7.1

Sintered density (g/cm)

MANUFACTURING CONDITIONS: 0.8% Amide wax; P: 400 - 800 MPa conventional compaction,
S: 1120C (2050F), 30 min in 90/10 N2/H2. Dimensional change: Green to as sintered.

87

Iron and steel powders for sintered components


0% Ni
2% Ni
4% Ni

AHC100.29 + Ni
103 psi

HV10

87

150

73

125

400

58

100

70

300

44

75

60

200

29

50

50

100

15

25

40

MPa
600
500

6.5

Tensile and Yield strength


Tensile str.
Yield str

6.7

6.9

7.1

7.3

0
7.5

6.5

HRB

Hardness

90

HV10
HRB

6.7

80

6.9

7.1

7.3

7.5

30

106 psi

29.0

90

180

26.1

75

55.2

160

23.2

60

44.2

140

20.3

45

33.1

120

17.4

30

22.1

100

14.5

15

11.0

11.6
7.5

GPa

Young's modulus

200

80

6.5

6.7

6.9

7.1

7.3

-0.1

12

-0.2

-0.3

-0.4

-0.5

6.5

6.7

6.9

7.1

Sintered density (g/cm3)

6.7

7.3

7.5

-0.6

6.9

7.1

66.3

7.3

7.5

7.3

7.5

Dimensional change

0.0

15

6.5

Elongation

18

Ft lb

Impact energy

6.5

6.7

6.9

7.1

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Amide wax; P: 400 - 800 MPa conventional compaction,
S: 1120 C (2050F), 30 min in 90/10 N2/H2. Dimensional change: Green to as sintered.

88

0.0

AHC100.29
0% C
0.5% C
0.8% C

AHC100.29 + 2% Ni + C
103 psi

HV10

87

200

73

175

400

58

150

70

300

44

125

60

200

29

100

50

100

15

75

40

50

MPa
600
500

6.5

Tensile and Yield strength


Tensile str.
Yield str

6.7

6.9

7.1

7.3

7.5

6.5

HRB

Hardness

90

HV10
HRB

6.7

80

6.9

7.1

7.3

7.5

30

106 psi

29.0

90

180

26.1

75

55.2

160

23.2

60

44.2

140

20.3

45

33.1

120

17.4

30

22.1

100

14.5

15

11.0

11.6
7.5

GPa

Young's modulus

200

80

6.5

6.7

6.9

7.1

7.3

-0.1

-0.2

-0.3

-0.4

-0.5

6.5

6.7

6.9

7.1

Sintered density (g/cm)

6.7

7.3

7.5

-0.6

6.9

7.1

66.3

7.3

7.5

7.3

7.5

0.0

Dimensional change

0.0

10

6.5

Elongation

12

Ft lb

Impact energy

6.5

6.7

6.9

7.1

Sintered density (g/cm)

MANUFACTURING CONDITIONS: 0.8% Amide wax; P: 400 - 800 MPa conventional compaction,
S: 1120C (2050F), 30 min in 90/10 N2/H2. Dimensional change: Green to as sintered.

89

Iron and steel powders for sintered components


15 minutes
30 minutes
45 minutes

AHC100.29 + 2% Ni + 0.8% C
103 psi

HV10

87

250

73

225

400

58

200

70

300

44

175

60

200

29

150

50

100

15

125

40

100
6.5

MPa
600
500

6.5

Tensile and Yield strength

6.7

6.9

7.1

7.3

7.5

90

HV10
HRB

Tensile str.
Yield str

HRB

Hardness

6.7

80

6.9

7.1

7.3

7.5

30

106 psi

29.0

60

180

26.1

50

36.8

160

23.2

40

29.5

140

20.3

30

22.1

120

17.4

20

14.7

100

14.5

10

7.4

11.6
7.5

GPa

Young's modulus

200

80

6.5

6.7

6.9

7.1

7.3

-0.1

-0.2

-0.3

-0.4

-0.5

6.5

6.7

6.9

7.1

Sintered density (g/cm)

7.3

7.5

-0.6

6.9

7.1

44.2

7.3

0.0
7.5

7.3

7.5

Dimensional change

0.0

6.7

Elongation

6.5

Ft lb

Impact energy

6.5

6.7

6.9

7.1

Sintered density (g/cm)

MANUFACTURING CONDITIONS: 0.8% Amide wax; P: 400 - 800 MPa conventional compaction,
S: 1120C (2050F), various time in 90/10 N2/H2. Dimensional change: Green to as sintered.

90

AHC100.29
0% C
0.5% C
0.8% C

AHC100.29 + 4% Ni + C
103 psi

HV10

87

225

73

200

400

58

175

70

300

44

150

60

200

29

125

50

100

15

100

40

75

MPa
600
500

6.5

Tensile and Yield strength


Tensile str.
Yield str

6.7

6.9

7.1

7.3

7.5

6.5

HRB

Hardness

90

HV10
HRB

6.7

80

6.9

7.1

7.3

7.5

30

106 psi

29.0

90

180

26.1

75

55.2

160

23.2

60

44.2

140

20.3

45

33.1

120

17.4

30

22.1

100

14.5

15

11.0

11.6
7.5

GPa

Young's modulus

200

80

6.5

6.7

6.9

7.1

7.3

-0.1

-0.2

-0.3

-0.4

-0.5

6.5

6.7

6.9

7.1

Sintered density (g/cm)

6.7

7.3

7.5

-0.6

6.9

7.1

66.3

7.3

7.5

7.3

7.5

0.0

Dimensional change

0.0

10

6.5

Elongation

12

Ft lb

Impact energy

6.5

6.7

6.9

7.1

Sintered density (g/cm)

MANUFACTURING CONDITIONS: 0.8% Amide wax; P: 400 - 800 MPa conventional compaction,
S: 1120C (2050F), 30 min in 90/10 N2/H2. Dimensional change: Green to as sintered.

91

Iron and steel powders for sintered components


0% C
0.5% C
0.8% C

AHC100.29 + 2% Cu + 2% Ni + C
103 psi

HV10

102

300

87

250

500

73

200

70

400

58

150

60

300

44

100

50

200

29

50

40

15

MPa
700
600

100
6.5

Tensile and Yield strength


Tensile str.
Yield str

6.7

6.9

7.1

7.3

7.5

6.5

HRB

Hardness

90

HV10
HRB

6.7

80

6.9

7.1

7.3

7.5

30

106 psi

29.0

60

180

26.1

50

36.8

160

23.2

40

29.5

140

20.3

30

22.1

120

17.4

20

14.7

100

14.5

10

7.4

11.6
7.5

GPa

Young's modulus

200

80

6.5

6.7

6.9

7.1

7.3

0.5

0.4

0.3

0.2

0.1

6.5

6.7

6.9

7.1

Sintered density (g/cm)

6.7

7.3

7.5

0.0

6.9

7.1

44.2

7.3

7.5

7.3

7.5

Dimensional change

0.6

10

6.5

Elongation

12

Ft lb

Impact energy

6.5

6.7

6.9

7.1

Sintered density (g/cm)

MANUFACTURING CONDITIONS: 0.8% Amide wax; P: 400 - 800 MPa conventional compaction,
S: 1120C (2050F), 30 min in 90/10 N2/H2. Dimensional change: Green to as sintered.

92

0.0

AHC100.29
C
2% Cu + C
2% Ni + C

AHC100.29 (+ 2% Cu) (+ 2% Ni) + C (7.0 g/cm)


103 psi

HV10

87

200

73

175

400

58

150

70

300

44

125

60

200

29

100

50

100

15

75

40

50

MPa
600
500

0.0

Tensile and Yield strength


Tensile str.
Yield str

0.2

0.4

0.6

0.8

0.0

HRB

Hardness

90

HV10
HRB

0.2

80

0.4

0.6

30
0.8

106 psi

29.0

60

180

26.1

50

36.8

160

23.2

40

29.5

140

20.3

30

22.1

120

17.4

20

14.7

100

14.5

10

7.4

11.6
0.8

GPa

Young's modulus

200

80
0.0

0.2

0.4

0.6

0.65

12

0.40

0.15

-0.10

-0.35

0.0

0.2

0.4

Combined carbon (%)

0.2

0.6

0.8

-0.60

0.4

44.2

0.6

0.0
0.8

0.6

0.8

Dimensional change

0.90

15

0.0

Elongation

18

Ft lb

Impact energy

0.0

0.2

0.4

Combined carbon (%)

MANUFACTURING CONDITIONS: 0.8% Amide wax; P: conventional compaction (sintered density 7.0 g/cm),
S: 1120C (2050F), 30 min in 90/10 N2/H2. Dimensional change: Green to as sintered.

93

Iron and steel powders for sintered components

94

ASC100.29

ASC100.29

95

Iron and steel powders for sintered components

96

ASC100.29
g/cm3

Apparent density versus mixing time

3.5

1. Zn-stearate

3.4

2. Kenolube P11

3.3
3.2
3.1

3.0

3. Amide wax

2.9
2.8

30

20

10

50

40

Spring back versus compacting pressure

0.4

1. 0.8% Zn-stearate
0.3

0.2

2. 0.6% Kenolube P11

0.1
0.0

400

300

g/cm3

600

500

900

800

700

Green density versus compacting pressure

7.6

Lubricated die
0.8% Zn-st
0.6% Kenolube P11

7.4

7.2

7.0

6.8

6.6

400

300
25

30

600

500
35

40

45

50

900

800

700
55

60

Compacting pressure (MPa and tsi)

97

Iron and steel powders for sintered components

ASC100.29
103 psi

HV10

44

150

250

36

125

200

29

100

150

22

75

100

15

50

50

25

MPa

Tensile strength

300

0
6.5

6.7

MPa

6.9

7.1

7.3

7.5

103 psi

0
6.5

44

%
0.2

250

36

0.1

200

29

0.0

150

22

-0.1

100

15

-0.2

50

-0.3

-0.4
6.5

Yield strength

300

0
6.5

6.7

6.9

7.1

7.3

7.5

Hardness

6.7

6.9

7.1

7.3

7.5

7.3

7.5

Dimensional change

6.7

6.9

7.1

Sintered density (g/cm3)


%
24

Elongation
1120C (2050F)

22

1220C (2230F)

20
18
16
14
12
6.5

6.7

6.9

7.1

7.3

7.5

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11, P: 400, 600 and 800 MPa resp.
S: 1120C (2050F) and 1220 C (2230F), 30 min in syntethic DA.
Dimensional change: Green to as sintered.

98

ASC100.29

ASC100.29 + C
103 psi

HV10

87

150

500

73

125

400

58

100

300

44

75

200

29

50

100

15

25

MPa

Tensile strength

600

0
6.5

6.7

MPa

6.9

7.1

7.3

7.5

103 psi

0
6.5

44

%
0.2

250

36

0.1

200

29

0.0

150

22

-0.1

100

15

-0.2

50

-0.3

-0.4
6.5

Yield strength

300

0
6.5

6.7

6.9

7.1

7.3

7.5

Hardness

6.7

6.9

7.1

7.3

7.5

7.3

7.5

Dimensional change

6.7

6.9

7.1

Sintered density (g/cm3)


%
12

Elongation
0.2% C

10

0.5% C
0.8% C

8
6
4
2
0
6.5

6.7

6.9

7.1

7.3

7.5

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11, P: 400, 600 and 800 MPa resp.
S: 1120 C (2050F), 30 min in Endogas. Dimensional change: Green to as sintered.

99

Iron and steel powders for sintered components

ASC100.29 + Cu
MPa

103 psi

HV10

87

150

500

73

125

400

58

100

300

44

75

200

29

50

100

15

25

Tensile strength

600

6.3

6.5

MPa

6.7

6.9

7.1

0
7.3

103 psi

44

%
1.5

250

36

1.3

200

29

1.1

150

22

0.9

100

15

0.7

50

0.5

0
7.3

0.3

Yield strength

300

6.3

6.5

6.7

6.9

7.1

6.3

Hardness

6.5

6.7

6.9

7.1

7.3

7.1

7.3

Dimensional change

6.3

6.5

6.7

6.9

Sintered density (g/cm3)


%
14

Elongation
2% Cu

12

4% Cu

10
8
6
4
2

6.3

6.5

6.7

6.9

7.1

7.3

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11, P: 400, 600 and 800 MPa resp.
S: 1120 C (2050F), 30 min in syntethic DA. Dimensional change: Green to as sintered.

100

ASC100.29

ASC100.29 + 2% Cu + C
103 psi

HV10

87

225

500

73

200

400

58

175

300

44

150

200

29

125

100

15

100

MPa

Tensile strength

600

0
6.5

6.7

MPa

6.9

7.1

7.3

7.5

103 psi

75
6.5

87

%
0.6

500

73

0.5

400

58

0.4

300

44

0.3

200

29

0.2

100

15

0.1

0.0

Yield strength

600

0
6.5

6.7

6.9

7.1

7.3

7.5

Hardness

6.7

6.9

7.1

7.3

7.5

7.3

7.5

Dimensional change

6.5

6.7

6.9

7.1

Sintered density (g/cm3)


%
12

Elongation
0.2% C

10

0.6% C

8
6
4
2
0
6.5

6.7

6.9

7.1

7.3

7.5

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11, P: 400, 600 and 800 MPa resp.
S: 1120 C (2050F), 30 min in Endogas. Dimensional change: Green to as sintered.

101

Iron and steel powders for sintered components

ASC100.29 + 4% Cu + C
103 psi

HV10

102

225

600

87

200

500

73

175

400

58

150

300

44

125

200

29

100

MPa

Tensile strength

700

100
6.3

6.5

MPa

6.7

6.9

7.1

7.3

15

103 psi

75
6.3

87

%
1.5

500

73

1.3

400

58

1.1

300

44

0.9

200

29

0.7

100

15

0.5

0.3

Yield strength

600

0
6.3

6.5

6.7

6.9

7.1

7.3

Hardness

6.5

6.7

6.9

7.1

7.3

7.1

7.3

Dimensional change

6.3

6.5

6.7

6.9

Sintered density (g/cm3)


%
6

Elongation
0.2% C

0.6% C

4
3
2
1
0
6.3

6.5

6.7

6.9

7.1

7.3

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11, P: 400, 600 and 800 MPa resp.
S: 1120 C (2050F), 30 min in Endogas. Dimensional change: Green to as sintered.

102

ASC100.29

ASC100.29 + 3% Ni
103 psi

HV10

400

58

150

350

51

125

300

44

100

250

36

75

200

29

50

150

22

25

MPa

100
6.5

Tensile strength

6.7

MPa

6.9

7.1

7.3

7.5

15

103 psi

Yield strength

0
6.5

44

%
-0.2

250

36

-0.3

200

29

-0.4

150

22

-0.5

100

15

-0.6

50

-0.7

-0.8
6.5

6.7

6.9

7.1

7.3

7.5

6.7

6.9

7.1

7.3

7.5

7.3

7.5

Dimensional change

300

0
6.5

Hardness

6.7

6.9

7.1

Sintered density (g/cm3)


%
25.0

Elongation
1120C (2050F)

22.5

1220C (2230F)

20.0
17.5
15.0
12.5
10.0

6.5

6.7

6.9

7.1

7.3

7.5

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11, P: 400, 600 and 800 MPa resp.
S: 1120 (2050F) and 1220C (2230F), 30 min in synthetic DA.
Dimensional change: Green to as sintered.

103

Iron and steel powders for sintered components

ASC100.29 + 2.5% Cu + 2.5% Ni


103 psi

HV10

87

150

500

73

125

400

58

100

300

44

75

200

29

50

100

15

25

MPa

Tensile strength

600

0
6.5

6.7

MPa

6.9

7.1

7.3

7.5

103 psi

6.5

%
0.6

250

36

0.5

200

29

0.4

150

22

0.3

100

15

0.2

50

0.1

0.0
6.5

0
6.5

6.7

6.9

7.1

7.3

7.5

6.7

6.9

7.1

7.3

7.5

7.3

7.5

Dimensional change

44

Yield strength

300

Hardness

6.7

6.9

7.1

Sintered density (g/cm3)


%
12

Elongation
1120C (2050F)

10

1220C (2230F)

8
6
4
2
0

6.5

6.7

6.9

7.1

7.3

7.5

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11, P: 400, 600 and 800 MPa resp.
S: 1120C (2050F) and 1220C (2230F), 30 min in synthetic DA.
Dimensional change: Green to as sintered.

104

ASC100.29

ASC100.29 + 2.5% Cu + 2.5% Ni + C


103 psi

HV10

102

225

600

87

200

500

73

175

400

58

150

300

44

125

200

29

100

MPa

Tensile strength

700

100
6.5

6.7

MPa

6.9

7.1

7.3

15
7.5

103 psi

75
6.5

87

%
0.8

500

73

0.7

400

58

0.6

300

44

0.5

200

29

0.4

100

15

0.3

Yield strength

600

6.5

6.7

6.9

7.1

7.3

0
7.5

Hardness

6.7

6.9

7.1

7.3

7.5

7.3

7.5

Dimensional change

0.2
6.5

6.7

6.9

7.1

Sintered density (g/cm3)


%
6

Elongation
0.2% C

0.6% C

4
3
2
1
0
6.5

6.7

6.9

7.1

7.3

7.5

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11, P: 400, 600 and 800 MPa resp.
S: 1120 C (2050F), 30 min in Endogas. Dimensional change: Green to as sintered.

105

Iron and steel powders for sintered components

ASC100.29 + 1.5% Cu + 0.15% Graphite, 20 minutes carburizing


Various densities
Centre

Surface

ASC100

Case har
MHV0.1
1000
800
600
400
200
0

Density 6.85 g/cm3 (500 MPa conventional compaction)

0.0

HV5
600
550
500
450
400
350
300
6.6

Density 7.15 g/cm (800 MPa conventional compaction)

3.0

Elongati

2.5
2.0
1.5
1.0
0.5
0.0
6.6

Density 7.30 g/cm3 (800 MPa warm compaction)

106

MANUFACT
conventiona
Carburizing
Dimensiona

ASC100.29

ASC100.29 + 1.5% Cu
Case hardening
MHV0.1

mm

Micro hardness profiles

1000

Thau

Case Depth

1.2

47

1.0

39

0.8

31

0.6

23

0.4

16

0.2

6.85 g/cm3

7.15

800

g/cm3

7.30 g/cm3

600
400
200

0.0

0
0.0

2.0

1.5

1.0

0.5

2.5

6.6

3.0

6.8

7.0

7.2

7.4

7.6

Distance from surface (mm)


HV5

MPa

Hardness

103 psi

Tensile and Yield strength

600

800

116

550

700

102

500

600

87

450

500

73

400

400

350

300

58
Tensile strength

44

Yield strength

29

200

300
6.6

6.8

7.0

% Elongation

7.2

7.4

Young's modulus

3.0

6.6

7.6

GPa 106 psi

200

29

0.6

180

26

0.5

2.0

160

23

0.4

1.5

140

20

0.3

1.0

120

17

0.2

0.5

100

15

0.1

80

12

0.0

Young's modulus

2.5

Elongation

0.0
6.6

6.8

7.0

7.2

Sintered density (g/cm3)

7.4

7.6

6.8

7.0

7.2

7.4

7.6

7.4

7.6

Dimensional change

Warm compaction
Conventional compaction

6.6

6.8

7.0

7.2

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube resp.; P: 500 - 800 MPa conventional
and warm compaction; S: 1120C (2050F), 20 min in 90/10 N2 /H2. Carburizing 920C (1690F),
20 min at 0.8% C-pot. Tempering 180C (355F), 60 min in air. Dimensional change:
Green to as hardened.

107

Iron and steel powders for sintered components

MANUFAC
20 min in
60 min in

108

ASC100.29

ASC100.29 + 1.5% Cu
Case hardening

MANUFACTURING CONDITIONS: 0.8% Amide wax; P: 650 MPa conventional compaction; S: 1120C (2050F),
20 min in 90/10 N2/H2. Carburizing 920C (1690F), various time at 0.8% C-pot. Tempering 180C (355F),
60 min in air. Dimensional change: Green to as hardened.

109

Iron and steel powders for sintered components

110

ASC100.29

111

Iron and steel powders for sintered components

112

MANUFACTU
20 min in 90
Tempering 1

ASC100.29

MANUFACTURING CONDITIONS: 0.8% Amide wax; P: 650 MPa conventional compaction; S: 1120C (2050F),
20 min in 90/10 N2/H2. Carburizing 920C (1690F), 20 min at 0.8% C-pot.
Tempering 180C (355F), 60 min in air. Dimensional change: Green to as hardened.

113

Iron and steel powders for sintered components

114

MANUFA
20 min
Temper

ASC100.29

MANUFACTURING CONDITIONS: 0.6% Lube; P: 650 MPa warm compaction; S: 1120C (2050F),
20 min in 90/10 N2/H2. Carburizing 920C (1690F), 20 min at 0.8% C-pot.
Tempering 180C (355F), 60 min in air. Dimensional change: Green to as hardened.

115

Iron and steel powders for sintered components

MANUFAC
(2050F),
Tempering

116

ASC100.29

MANUFACTURING CONDITIONS: 0.8% Amide wax; P: 550 - 700 MPa conventional compaction; S: 1120C
(2050F), 20 min in 90/10 N2/H2. Carburizing 920C (1690F), 20 min at 0.8% C-pot.
Tempering 180C (355F), 60 min in air. Dimensional change: Green to as hardened.

117

Iron and steel powders for sintered components

MANUF
20 min
60 min

118

ASC100.29

MANUFACTURING CONDITIONS: 0.6% Lube; P: 550 - 700 MPa warm compaction; S: 1120C (2050F),
20 min in 90/10 N2/H2. Carburizing 920C (1690F), 20 min at 0.8% C-pot. Tempering 180C (355F),
60 min in air. Dimensional change: Green to as hardened.

119

Iron and steel powders for sintered components

120

ABC100.30

ABC100.30

121

Iron and steel powders for sintered components

122

ABC100.30
g/cm

Apparent density versus mixing time

3.5

1. Zn-stearate

3.4

2. Kenolube P11

3.3

3.2

3. Amide wax

3.1
3.0
2.9
2.8

10

40

30

20

50

Spring back versus compacting pressure

0.4

0.6% Kenolube P11


0.3
0.2
0.1
0.0

400

300

g/cm

600

500

900

800

700

Green density versus compacting pressure

7.6

Lubricated die
0.8% Zn-st
0.6% Kenolube P11

7.4

7.2

7.0

6.8

6.6

400

300
25

30

600

500
35

40

45

50

900

800

700
55

60

Compacting pressure (MPa and tsi)

123

Iron and steel powders for sintered components

ABC100.30
103 psi

HV10

300

44

150

250

36

125

200

29

100

150

22

75

100

15

50

25

MPa

Tensile strength

50
0

6.6

6.8

MPa

7.0

7.2

7.4

7.6

103 psi
44

%
0.3

250

36

0.2

200

29

0.1

150

22

-0.0

100

15

-0.1

-0.2

-0.3

Yield strength

300

50
0

6.6

6.8

7.0

7.2

7.4

7.6

6.6

Hardness

6.8

7.0

7.2

6.6

6.8

7.0

7.2

Elongation
1120C (2050F)

27.5

1220C (2230F)

25.0
22.5
20.0
17.5
15.0

6.6

6.8

7.0

7.2

7.4

7.6

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.6% Kenolube P11, P: 392, 586 and 785 MPa resp.
S: 1120C (2050F) and 1220C (2230F), 30 min in syntethic DA.
Dimensional change: Green to as sintered.

124

7.6

7.4

7.6

Dimensional change

Sintered density (g/cm3)


%
30.0

7.4

ABC100.30

ABC100.30 + C
103 psi

HV10

58

150

350

51

125

300

44

100

250

36

75

200

29

50

150

22

25

15

MPa

Tensile strength

400

100

6.6

6.8

MPa

7.0

7.2

7.4

7.6

103 psi
44

%
0.3

250

36

0.2

200

29

0.1

150

22

-0.0

100

15

-0.1

-0.2

-0.3

Yield strength

300

50
0

6.6

6.8

7.0

7.2

7.4

7.6

6.6

Hardness

6.8

7.0

7.2

7.4

7.6

7.4

7.6

Dimensional change

6.6

6.8

7.0

7.2

Sintered density (g/cm3)


%
18

Elongation
0.2% C

15

0.6% C

12
9
6
3
0

6.6

6.8

7.0

7.2

7.4

7.6

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.6% Kenolube P11, P: 392, 586 and 785 MPa resp.
S: 1120C (2050F), 30 min in Endogas. Dimensional change: Green to as sintered.

125

Iron and steel powders for sintered components

ABC100.30 + 2% Cu + C
103 psi

HV10

102

225

600

87

200

500

73

175

400

58

150

300

44

125

200

29

100

15

75

103 psi
87

%
0.6

500

73

0.5

400

58

0.4

300

44

0.3

200

29

0.2

100

15

0.1

0.0

MPa

Tensile strength

700

100

6.6

6.8

MPa

7.2

7.4

Yield strength

600

0
6.6

7.0

6.8

7.0

7.2

7.4

7.6

7.6

6.6

Hardness

6.8

7.0

7.2

6.6

6.8

7.0

7.2

Elongation
0.2% C

10

0.6% C

8
6
4
2
0

6.6

6.8

7.0

7.2

7.4

7.6

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.6% Kenolube P11, P: 392, 586 and 785 MPa resp.
S: 1120 C (2050F), 30 min in Endogas. Dimensional change: Green to as sintered.

126

7.6

7.4

7.6

Dimensional change

Sintered density (g/cm3)


%
12

7.4

ABC100.30

ABC100.30 + 0.45% P + C
103 psi

HV10

102

225

600

87

200

500

73

175

400

58

150

300

44

125

200

29

100

MPa

Tensile strength

700

100
6.6

6.8

MPa

7.0

7.2

7.4

7.6

15

103 psi

75
6.6

87

%
0.5

500

73

0.4

400

58

0.3

300

44

0.2

200

29

0.1

100

15

-0.0

-0.1
6.6

Yield strength

600

0
6.6

6.8

7.0

7.2

7.4

7.6

Hardness

6.8

7.0

7.2

7.4

7.6

7.4

7.6

Dimensional change

6.8

7.0

7.2

Sintered density (g/cm3)


%
12

Elongation
0.2% C

10

0.5% C

8
6
4
2
0
6.6

6.8

7.0

7.2

7.4

7.6

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.6% Kenolube P11, P: 392, 586 and 785 MPa resp.
S: 1120C (2050F), 30 min in Endogas. Dimensional change: Green to as sintered.

127

Iron and steel powders for sintered components

ABC100.30 + 3% Ni
103 psi

HV10

58

150

350

51

125

300

44

100

250

36

75

200

29

50

150

22

25

15
7.6

MPa

Tensile and Yield strength

400

100
6.6

6.8

7.0

7.2

7.4

ft lb

6.6

103

%
-0.0

120

88

-0.1

100

74

-0.2

80

59

-0.3

60

44

-0.4

40

29

-0.5

Impact energy

140

20
6.6

6.8

7.0

7.2

7.4

14
7.6

-0.6
6.6

Hardness

7.0

6.8

7.2

6.8

7.0

7.2

Elongation
1120C (2050F)

22

1220C (2230F)

20

Tensile strength
Yield strength

18
16
14
12
6.6

6.8

7.0

7.2

7.4

7.6

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.6% Kenolube P11, P: 392, 586 and 785 MPa resp.
S: 1120C (2050F) and 1220C (2230F), 30 min in synthetic DA.
Dimensional change: Green to as sintered.

128

7.6

7.4

7.6

Dimensional change

Sintered density (g/cm3)


%
24

7.4

ABC100.30

ABC100.30 + Cu
103 psi

HV10

58

150

350

51

125

300

44

100

250

36

75

200

29

50

150

22

25

15

MPa

Tensile strength

400

100

MPa

103 psi
44

%
1.5

250

36

1.2

200

29

0.9

150

22

0.6

100

15

0.3

50

0.0

-0.3

Yield strength

300

Hardness

Dimensional change

Copper content (%)


%
24

Elongation

20
16
12
8
4
0

Copper content (%)

MANUFACTURING CONDITIONS: 0.6% Kenolube P11, P: 589 MPa (density 6.95 - 7.15 g/cm3)
S: 1120C (2050F), 30 min in synthetic DA. Dimensional change: Green to as sintered.

129

Iron and steel powders for sintered components

130

Phosphorous-alloyed Grades
PNC60
PASC60

131

Iron and steel powders for sintered components

132

PNC60

PNC60

133

Iron and steel powders for sintered components

134

PNC60

135

Iron and steel powders for sintered components

PNC60
103 psi

HV10

87

300

500

73

250

400

58

200

300

44

150

200

29

100

100

15

50

MPa

Tensile and Yield strength

600

6.4

6.6

6.8

7.0

7.2

0
7.4

6.4

75

-0.2

60

-0.4

45

-0.6

30

-0.8

15

-1.0

6.4

6.6

6.8

7.0

7.2

7.4

-1.2
6.4

6.8

6.6

%
-0.0

Impact energy

90

Hardness

7.0

7.2

7.4

7.2

7.4

Dimensional change

6.6

6.8

7.0

Sintered density (g/cm3)


%
18

Elongation
Endo

15

DA

12

Tensile strength
Yield strength

9
6
3
0

6.4

6.6

6.8

7.0

7.2

7.4

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11, P: 392, 589 and 785 MPa resp.
S: 1120C (2050F), 30 min in synthetic DA and endogas. Dimensional change: Green to as sintered.

136

PNC60

PNC60
103 psi

HV10

87

300

500

73

250

400

58

200

300

44

150

200

29

100

100

15

50

MPa

Tensile strength

600

0
840

920

MPa

1000

1080

1160

0
1240

103 psi

0
840

%
0.3

500

73

0.0

400

58

-0.3

300

44

-0.6

200

29

-0.9

100

15

-1.2

0
840

920

1000

1080

1160

0
1240

920

1000

1080

1160

1240

1160

1240

Dimensional change

87

Yield strength

600

Hardness

-1.5
840

920

1000

1080

Sintering temperature (C)


%
18

Elongation
Endo

15

DA

12
9
6
3
0
840

920

1000

1080

1160

1240

Sintering temperature (C)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11, P: 589 MPa. S: 30 minutes at
various temperatures in synthetic DA and Endogas. Dimensional change: Green to as sintered.

137

Iron and steel powders for sintered components

PNC60
103 Psi

HV10

87

300

500

73

250

400

58

200

300

44

150

200

29

100

100

15

50

MPa

Tensile strength

600

20

MPa

40

60

80

0
100

103 Psi

87

%
-0.2

500

73

-0.4

400

58

-0.6

300

44

-0.8

200

29

-1.0

100

15

-1.2

Yield strength

600

20

40

60

80

0
100

-1.4

Hardness

20

40

60

80

100

80

100

Dimensional change

20

40

60

Time at sintering temperature (min)


%
18

Elongation
Endo

15

DA

12
9
6
3
0

20

40

60

80

100

Time at sintering temperature (min)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11, P: 589 MPa. S: Various times
at 1120C (2050F) in synthetic DA and Endogas. Dimensional change: Green to as sintered.

138

PNC60

PNC60 + Cu
103 psi

HV10

87

300

500

73

250

400

58

200

300

44

150

200

29

100

100

15

50

MPa

Tensile strength

600

MPa

103 psi

87

%
-0.0

500

73

-0.2

400

58

-0.4

300

44

-0.6

200

29

-0.8

100

15

-1.0

-1.2

Yield strength

600

Hardness

Dimensional change

Copper content (%)


%
18

Elongation
Endo

15

DA

12
9
6
3
0

Copper content (%)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11 + various copper additions.
P: 589 MPa. S: 1120C (2050F), 30 min synthetic DA and Endogas. Dimensional change:
Green to as sintered.

139

Iron and steel powders for sintered components

PNC60 + Cu + C
103 psi

HV10

116

300

700

102

250

600

87

200

500

73

150

400

58

100

300

44

50

29
1.0

MPa

Tensile strength

800

200

0.0

0.2

MPa

0.4

0.6

0.8

103 psi

0.0

87

%
0.6

500

73

0.3

400

58

0.0

300

44

-0.3

200

29

-0.6

100

15

-0.9

Yield strength

600

0.0

0.2

0.4

0.6

0.8

0
1.0

Hardness

0.2

0.4

0.6

0.8

1.0

0.8

1.0

Dimensional change

-1.2
0.0

0.2

0.4

0.6

Carbon content (%)


%
18

Elongation
4% Cu

15

2% Cu
0% Cu

12
9
6
3
0

0.0

0.2

0.4

0.6

0.8

1.0

Carbon content (%)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11 + various graphite and copper
additions. P: 589 MPa. S: 1120C (2050F), 30 min synthetic DA and Endogas.
Dimensional change: Green to as sintered.

140

PNC60

NC100.24 + 0.45% P
103 psi

HV10

87

300

500

73

250

400

58

200

300

44

150

200

29

100

100

15

50

MPa

Tensile and Yield strength

600

6.4

6.6

6.8

7.0

7.2

0
7.4

6.4

75

-0.1

60

-0.2

45

-0.3

30

-0.4

15

-0.5

6.4

6.6

6.8

7.0

7.2

7.4

-0.6
6.4

6.8

6.6

7.0

7.2

7.4

7.2

7.4

Dimensional change

%
-0.0

Impact energy

90

Hardness

6.8

6.6

7.0

Sintered density (g/cm3)


%
18

Elongation
Endo

15

DA

12

Tensile strength
Yield strength

9
6
3
0

6.4

6.6

6.8

7.0

7.2

7.4

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11, P: 392, 589 and 785 MPa resp.
S: 1120C (2050F), 30 min in synthetic DA and endogas. Dimensional change: Green to as sintered.

141

Iron and steel powders for sintered components

NC100.24 + 0.45% P
103 psi

HV10

87

300

500

73

250

400

58

200

300

44

150

200

29

100

100

15

50

MPa

Tensile strength

600

0
840

920

MPa

1000

1080

1160

0
1240

0.2

400

0.0

300

-0.2

200

-0.4

100

-0.6

920

1000

1080

1160

1240

1000

1080

1160

1240

1160

1240

Dimensional change

500

0
840

920

%
0.4

Yield strength

600

0
840

Hardness

-0.8
840

920

1000

1080

Sintering temperature (C)


%
18

Elongation
Endo

15

DA

12
9
6
3
0
840

920

1000

1080

1160

1240

Sintering temperature (C)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11, P: 589 MPa. S: 30 minutes at
various temperatures in synthetic DA and Endogas. Dimensional change: Green to as sintered.

142

PNC60

NC100.24 + 0.45% P
103 psi

HV10

87

300

500

73

250

400

58

200

300

44

150

200

29

100

100

15

50

MPa

Tensile strength

600

20

MPa

40

60

80

0
100

103 psi

87

%
-0.0

500

73

-0.1

400

58

-0.2

300

44

-0.3

200

29

-0.4

100

15

-0.5

Yield strength

600

20

40

60

80

0
100

-0.6

Hardness

20

40

60

80

100

80

100

Dimensional change

20

40

60

Time at sintering temperature (min)


%
18

Elongation
Endo

15

DA

12
9
6
3
0

20

40

60

80

100

Time at sintering temperature (min)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11, P: 589 MPa. S: Various times
at 1120C (2050F) in synthetic DA and Endogas. Dimensional change: Green to as sintered.

143

Iron and steel powders for sintered components

NC100.24 + 0.45% P + Cu
103 psi

HV10

87

300

500

73

250

400

58

200

300

44

150

200

29

100

100

15

50

MPa

Tensile strength

600

MPa

103 psi

87

%
0.4

500

73

0.2

400

58

0.0

300

44

-0.2

200

29

-0.4

100

15

-0.6

-0.8

Yield strength

600

Hardness

Dimensional change

Copper content (%)


%
18

Elongation
Endo

15

DA

12
9
6
3
0

Copper content (%)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11 + various copper additions.
P: 589 MPa. S: 1120C (2050F), 30 min synthetic DA and Endogas.
Dimensional change: Green to as sintered.

144

PNC60

NC100.24 + 0.45% P + Cu + C
103 psi

HV10

116

300

700

102

250

600

87

200

500

73

150

400

58

100

300

44

50

29
1.0

MPa

Tensile strength

800

200

0.0

0.2

MPa

0.4

0.6

0.8

103 psi

0.0

%
0.6

500

73

0.4

400

58

0.2

300

44

-0.0

200

29

-0.2

100

15

-0.4

0.0

0.2

0.4

0.6

0.8

0
1.0

0.2

0.4

0.6

0.8

1.0

0.8

1.0

Dimensional change

87

Yield strength

600

Hardness

-0.6
0.0

0.2

0.4

0.6

Carbon content (%)


%
12

Elongation
4% Cu

10

2% Cu
0% Cu

8
6
4
2
0

0.0

0.2

0.4

0.6

0.8

1.0

Carbon content (%)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11 + various graphite and copper
additions. P: 589 MPa. S: 1120C (2050F), 30 min synthetic DA and Endogas.
Dimensional change: Green to as sintered.

145

Iron and steel powders for sintered components

NC100.24 + 0.30% P
103 psi

HV10

87

300

500

73

250

400

58

200

300

44

150

200

29

100

100

15

50

MPa

Tensile and Yield strength

600

6.4

6.6

6.8

7.0

7.2

0
7.4

6.4

0.2

40

0.1

30

-0.0

20

-0.1

10

-0.2

6.4

6.6

6.8

7.0

7.2

7.4

7.0

7.2

7.4

7.2

7.4

Dimensional change

50

6.8

6.6

%
0.3

Impact energy

60

Hardness

-0.3
6.4

6.6

6.8

7.0

Sintered density (g/cm3)


%
12

Elongation
Endo

10

DA

Tensile strength
Yield strength

6
4
2
0

6.4

6.6

6.8

7.0

7.2

7.4

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11, P: 392, 589 and 785 MPa resp.
S: 1120C (2050F), 30 min in synthetic DA and endogas. Dimensional change: Green to as sintered.

146

PNC60

NC100.24 + 0.30% P
103 psi

HV10

87

300

500

73

250

400

58

200

300

44

150

200

29

100

100

15

50

MPa

Tensile strength

600

0
840

920

MPa

1000

1080

1160

0
1240

103 psi

0
840

87

%
0.2

500

73

0.1

400

58

0.0

300

44

-0.1

200

29

-0.2

100

15

-0.3

Yield strength

600

0
840

920

1000

1080

1160

0
1240

Hardness

920

1000

1080

1160

1240

1160

1240

Dimensional change

-0.4
840

920

1000

1080

Sintering temperature (C)


%
12

Elongation
Endo

10

DA

8
6
4
2
0
840

920

1000

1080

1160

1240

Sintering temperature (C)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11, P: 589 MPa. S: 30 minutes at
various temperatures in synthetic DA and Endogas. Dimensional change: Green to as sintered.

147

Iron and steel powders for sintered components

NC100.24 + 0.30% P
103 psi

HV10

87

300

500

73

250

400

58

200

300

44

150

200

29

100

100

15

50

MPa

Tensile strength

600

20

MPa

40

60

80

0
100

103 psi

87

%
0.3

500

73

0.2

400

58

0.1

300

44

-0.0

200

29

-0.1

100

15

-0.2

Yield strength

600

20

40

60

80

0
100

Hardness

20

40

60

80

100

80

100

Dimensional change

-0.3

20

40

60

Time at sintering temperature (min)


%
12

Elongation
Endo

10

DA

8
6
4
2
0

20

40

60

80

100

Time at sintering temperature (min)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11, P: 589 MPa. S: Various times
at 1120C (2050F) in synthetic DA and Endogas. Dimensional change: Green to as sintered.

148

PNC60

NC100.24 + 0.30% P + Cu
103 psi

HV10

87

300

500

73

250

400

58

200

300

44

150

200

29

100

100

15

50

MPa

Tensile strength

600

MPa

103 psi

87

%
0.3

500

73

0.2

400

58

0.1

300

44

-0.0

200

29

-0.1

100

15

-0.2

-0.3

Yield strength

600

Hardness

Dimensional change

Copper content (%)


%
18

Elongation
Endo

15

DA

12
9
6
3
0

Copper content (%)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11 + various copper additions.
P: 589 MPa. S: 1120C (2050F), 30 min synthetic DA and Endogas.
Dimensional change: Green to as sintered.

149

Iron and steel powders for sintered components

NC100.24 + 0.30% P + Cu + C
103 psi

HV10

800

116

300

700

102

250

600

87

200

500

73

150

400

58

100

300

44

50

29
1.0

MPa

200

0.0

Tensile strength

0.2

MPa

0.4

0.6

0.8

103 psi

0.0

87

%
0.6

500

73

0.4

400

58

0.2

300

44

-0.0

200

29

-0.2

100

15

-0.4

Yield strength

600

0.0

0.2

0.4

0.6

0.8

0
1.0

Hardness

0.2

0.4

0.6

0.8

1.0

0.8

1.0

Dimensional change

-0.6
0.0

0.2

0.4

0.6

Carbon content (%)


%
12

Elongation
4% Cu

10

2% Cu
0% Cu

8
6
4
2
0

0.0

0.2

0.4

0.6

0.8

1.0

Carbon content (%)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11 + various graphite and copper
additions. P: 589 MPa. S: 1120C (2050F), 30 min synthetic DA and Endogas.
Dimensional change: Green to as sintered.

150

PASC60

PASC60

151

Iron and steel powders for sintered components

152

PASC60

153

Iron and steel powders for sintered components

PASC60
103 psi

HV10

87

300

500

73

250

400

58

200

300

44

150

200

29

100

100

15

50

MPa

Tensile and Yield strength

600

6.6

6.8

7.0

7.2

7.4

0
7.6

6.6

75

-0.4

60

-0.5

45

-0.6

30

-0.7

15

-0.8

6.6

6.8

7.0

7.2

7.4

7.6

-0.9
6.6

7.0

6.8

%
-0.3

Impact energy

90

Hardness

7.2

7.4

7.6

7.4

7.6

Dimensional change

6.8

7.0

7.2

Sintered density (g/cm3)


%
18

Elongation
Endo

15

DA

12

Tensile strength
Yield strength

9
6
3
0

6.6

6.8

7.0

7.2

7.4

7.6

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11, P: 392, 589 and 785 MPa resp.
S: 1120C (2050F), 30 min in synthetic DA and endogas. Dimensional change: Green to as sintered.

154

PASC60

PASC60
103 psi

HV10

87

300

500

73

250

400

58

200

300

44

150

200

29

100

100

15

50

MPa

Tensile strength

600

0
840

920

MPa

1000

1080

1160

0
1240

103 psi

0
840

87

%
0.3

500

73

0.0

400

58

-0.3

300

44

-0.6

200

29

-0.9

100

15

-1.2

Yield strength

600

0
840

920

1000

1080

1160

0
1240

Hardness

920

1000

1080

1160

1240

1160

1240

Dimensional change

-1.5
840

920

1000

1080

Sintering temperature (C)


%
18

Elongation
Endo

15

DA

12
9
6
3
0
840

920

1000

1080

1160

1240

Sintering temperature (C)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11, P: 589 MPa. S: 30 minutes at
various temperatures in synthetic DA and Endogas. Dimensional change: Green to as sintered.

155

Iron and steel powders for sintered components

PASC60
103 psi

HV10

87

300

500

73

250

400

58

200

300

44

150

200

29

100

100

15

50

MPa

Tensile strength

600

20

MPa

40

60

80

0
100

103 psi

87

%
-0.0

500

73

-0.2

400

58

-0.4

300

44

-0.6

200

29

-0.8

100

15

-1.0

Yield strength

600

20

40

60

80

0
100

-1.2

Hardness

20

40

60

80

100

80

100

Dimensional change

20

40

60

Time at sintering temperature (min)


%
18

Elongation
Endo

15

DA

12
9
6
3
0

20

40

60

80

100

Time at sintering temperature (min)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11, P: 589 MPa. S: Various times
at 1120C (2050F) in synthetic DA and Endogas. Dimensional change: Green to as sintered.

156

PASC60

PASC60 + Cu
103 psi

HV10

87

300

500

73

250

400

58

200

300

44

150

200

29

100

100

15

50

MPa

Tensile strength

600

MPa

103 psi

87

%
0.2

500

73

-0.0

400

58

-0.2

300

44

-0.4

200

29

-0.6

100

15

-0.8

-1.0

Yield strength

600

Hardness

Dimensional change

Copper content (%)


%
18

Elongation
Endo

15

DA

12
9
6
3
0

Copper content (%)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11 + various copper additions.
P: 589 MPa. S: 1120C (2050F), 30 min synthetic DA and Endogas.
Dimensional change: Green to as sintered.

157

Iron and steel powders for sintered components

PASC60 + Cu + C
103 psi

HV10

116

300

700

102

250

600

87

200

500

73

150

400

58

100

300

44

50

29
1.0

MPa

Tensile strength

800

200

0.0

0.2

MPa

0.4

0.6

0.8

103 psi

0.0

87

%
0.9

500

73

0.6

400

58

0.3

300

44

-0.0

200

29

-0.3

100

15

-0.6

Yield strength

600

0.0

0.2

0.4

0.6

0.8

0
1.0

Hardness

0.2

0.4

0.6

0.8

1.0

0.8

1.0

Dimensional change

-0.9
0.0

0.2

0.4

0.6

Carbon content (%)


%
18

Elongation
4% Cu

15

2% Cu
0% Cu

12
9
6
3
0

0.0

0.2

0.4

0.6

0.8

1.0

Carbon content (%)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11 + various graphite and copper
additions. P: 589 MPa. S: 1120C (2050F), 30 min synthetic DA and Endogas.
Dimensional change: Green to as sintered.

158

PASC60

ASC100.29 + 0.45% P
103 psi

HV10

87

300

500

73

250

400

58

200

300

44

150

200

29

100

100

15

50

MPa

Tensile and Yield strength

600

6.6

6.8

7.0

7.2

7.4

0
7.6

6.6

75

-0.1

60

-0.2

45

-0.3

30

-0.4

15

-0.5

6.6

6.8

7.0

7.2

7.4

7.6

-0.6
6.6

7.0

6.8

%
-0.0

Impact energy

90

Hardness

7.2

7.4

7.6

7.4

7.6

Dimensional change

6.8

7.0

7.2

Sintered density (g/cm3)


%
18

Elongation
Endo

15

DA

12

Tensile strength
Yield strength

9
6
3
0

6.6

6.8

7.0

7.2

7.4

7.6

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11, P: 392, 589 and 785 MPa resp.
S: 1120C (2050F), 30 min in synthetic DA and endogas. Dimensional change: Green to as sintered.

159

Iron and steel powders for sintered components

ASC100.29 + 0.45% P
103 psi

HV10

87

300

500

73

250

400

58

200

300

44

150

200

29

100

100

15

50

MPa

Tensile strength

600

0
840

920

MPa

1000

1080

1160

0
1240

103 psi

0
840

87

%
0.3

500

73

0.1

400

58

-0.1

300

44

-0.3

200

29

-0.5

100

15

-0.7

Yield strength

600

0
840

920

1000

1080

1160

0
1240

Hardness

920

1000

1080

1160

1240

1160

1240

Dimensional change

-0.9
840

920

1000

1080

Sintering temperature (C)


%
18

Elongation
Endo

15

DA

12
9
6
3
0
840

920

1000

1080

1160

1240

Sintering temperature (C)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11, P: 589 MPa. S: 30 minutes at
various temperatures in synthetic DA and Endogas. Dimensional change: Green to as sintered.

160

PASC60

ASC100.29 + 0.45% P
103 psi

HV10

87

300

500

73

250

400

58

200

300

44

150

200

29

100

100

15

50

MPa

Tensile strength

600

20

MPa

40

60

80

0
100

103 psi

87

%
-0.0

500

73

-0.1

400

58

-0.2

300

44

-0.3

200

29

-0.4

100

15

-0.5

Yield strength

600

20

40

60

80

0
100

-0.6

Hardness

20

40

60

80

100

80

100

Dimensional change

20

40

60

Time at sintering temperature (min)


%
18

Elongation
Endo

15

DA

12
9
6
3
0

20

40

60

80

100

Time at sintering temperature (min)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11, P: 589 MPa. S: Various times
at 1120C (2050F) in synthetic DA and Endogas. Dimensional change: Green to as sintered.

161

Iron and steel powders for sintered components

ASC100.29 + 0.45% P + Cu
103 psi

HV10

87

300

500

73

250

400

58

200

300

44

150

200

29

100

100

15

50

MPa

Tensile strength

600

MPa

103 psi

87

%
0.3

500

73

0.1

400

58

-0.1

300

44

-0.3

200

29

-0.5

100

15

-0.7

-0.9

Yield strength

600

Hardness

Dimensional change

Copper content (%)


%
18

Elongation
Endo

15

DA

12
9
6
3
0

Copper content (%)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11 + various copper additions.
P: 589 MPa. S: 1120C (2050F), 30 min synthetic DA and Endogas.
Dimensional change: Green to as sintered.

162

PASC60

ASC100.29 + 0.45% P + Cu + C
103 psi

HV10

116

300

700

102

250

600

87

200

500

73

150

400

58

100

300

44

50

29
1.0

MPa

Tensile strength

800

200

0.0

0.2

MPa

0.4

0.6

0.8

103 psi

0.0

87

%
0.9

500

73

0.6

400

58

0.3

300

44

-0.0

200

29

-0.3

100

15

-0.6

Yield strength

600

0.0

0.2

0.4

0.6

0.8

0
1.0

Hardness

0.2

0.4

0.6

0.8

1.0

0.8

1.0

Dimensional change

-0.9
0.0

0.2

0.4

0.6

Carbon content (%)


%
18

Elongation
4% Cu

15

2% Cu
0% Cu

12
9
6
3
0

0.0

0.2

0.4

0.6

0.8

1.0

Carbon content (%)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11 + various graphite and copper
additions.P: 589 MPa. S: 1120C (2050F), 30 min synthetic DA and Endogas.
Dimensional change: Green to as sintered.

163

Iron and steel powders for sintered components

ASC100.29 + 0.30% P
103 psi

HV10

87

300

500

73

250

400

58

200

300

44

150

200

29

100

100

15

50

MPa

Tensile and Yield strength

600

6.6

6.8

7.0

7.2

7.4

0
7.6

6.6

0.2

60

0.1

45

-0.0

30

-0.1

15

-0.2

6.6

6.8

7.0

7.2

7.4

7.6

7.0

7.2

7.4

7.6

7.4

7.6

Dimensional change

75

6.8

%
0.3

Impact energy

90

Hardness

-0.3
6.6

6.8

7.0

7.2

Sintered density (g/cm3)


%
18

Elongation
Endo

15

DA

12

Tensile strength
Yield strength

9
6
3
0

6.6

6.8

7.0

7.2

7.4

7.6

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11, P: 392, 589 and 785 MPa resp.
S: 1120C (2050F), 30 min in synthetic DA and endogas. Dimensional change: Green to as sintered.

164

PASC60

ASC100.29 + 0.30% P
103 psi

HV10

87

300

500

73

250

400

58

200

300

44

150

200

29

100

100

15

50

MPa

Tensile strength

600

0
840

920

MPa

1000

1080

1160

0
1240

103 psi

0
840

87

%
0.3

500

73

0.2

400

58

0.1

300

44

-0.0

200

29

-0.1

100

15

-0.2

Yield strength

600

0
840

920

1000

1080

1160

0
1240

Hardness

920

1000

1080

1160

1240

1160

1240

Dimensional change

-0.3
840

920

1000

1080

Sintering temperature (C)


%
18

Elongation
Endo

15

DA

12
9
6
3
0
840

920

1000

1080

1160

1240

Sintering temperature (C)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11, P: 589 MPa. S: 30 minutes at
various temperatures in synthetic DA and Endogas. Dimensional change: Green to as sintered.

165

Iron and steel powders for sintered components

ASC100.29 + 0.30% P
103 psi

HV10

87

300

500

73

250

400

58

200

300

44

150

200

29

100

100

15

50

MPa

Tensile strength

600

20

MPa

40

60

80

0
100

103 psi

87

%
0.3

500

73

0.2

400

58

0.1

300

44

-0.0

200

29

-0.1

100

15

-0.2

Yield strength

600

20

40

60

80

0
100

Hardness

20

40

60

80

100

80

100

Dimensional change

-0.3

20

40

60

Time at sintering temperature (min)


%
18

Elongation
Endo

15

DA

12
9
6
3
0

20

40

60

80

100

Time at sintering temperature (min)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11, P: 589 MPa. S: Various times
at 1120C (2050F) in synthetic DA and Endogas. Dimensional change: Green to as sintered.

166

PASC60

ASC100.29 + 0.30% P + Cu
103 psi

HV10

87

300

500

73

250

400

58

200

300

44

150

200

29

100

100

15

50

MPa

Tensile strength

600

MPa

103 psi

87

%
0.3

500

73

0.2

400

58

0.1

300

44

-0.0

200

29

-0.1

100

15

-0.2

-0.3

Yield strength

600

Hardness

Dimensional change

Copper content (%)


%
18

Elongation
Endo

15

DA

12
9
6
3
0

Copper content (%)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11 + various copper additions.
P: 589 MPa. S: 1120C (2050F), 30 min synthetic DA and Endogas. Dimensional change:
Green to as sintered.

167

Iron and steel powders for sintered components

ASC100.29 + 0.30% P + Cu + C
103 psi

HV10

116

300

700

102

250

600

87

200

500

73

150

400

58

100

300

44

50

29
1.0

MPa

Tensile strength

800

200

0.0

0.2

MPa

0.4

0.6

0.8

103 psi

0.0

87

%
0.6

500

73

0.4

400

58

0.2

300

44

-0.0

200

29

-0.2

100

15

-0.4

Yield strength

600

0.0

0.2

0.4

0.6

0.8

0
1.0

Hardness

0.2

0.4

0.6

0.8

1.0

0.8

1.0

Dimensional change

-0.6
0.0

0.2

0.4

0.6

Carbon content (%)


%
18

Elongation
4% Cu

15

2% Cu
0% Cu

12
9
6
3
0

0.0

0.2

0.4

0.6

0.8

1.0

Carbon content (%)

MANUFACTURING CONDITIONS: 0.8% Zn-st or 0.6% Kenolube P11 + various graphite and copper
additions. P: 589 MPa. S: 1120C (2050F), 30 min synthetic DA and Endogas.
Dimensional change: Green to as sintered.

168

Diffusion alloyed grades


Distaloy SA
Distaloy AB
Distaloy AE
Distaloy AF
Distaloy DC
Distaloy DH
Distaloy HP

169

Iron and steel powders for sintered components

170

Distaloy SA

Distaloy SA

Plain iron grades

171

Iron and steel powders for sintered components

Typical data, Distaloy SA

172

Distaloy SA
Springback

%
0.4

0.8% Zn-st
0.6 % Kenolube

0.3

Lubricated tool die

0.2
0.1
0.0
200

300

400

g/cm3

500

600

700

800

600

700

800

Green density

7.3
7.2
7.1
7.0
6.9
6.8
6.7
6.6
6.5
6.4
6.3
200

500

400

300

Green strength

MPa

psi

30

4350

25

3625

20

2900

15

2175

10

1450

725

0
200
15

400

300
20

25

30

600

500
35

40

45

800

700
50

55

Compacting pressure (MPa and tsi)

173

Iron and steel powders for sintered components

174

Distaloy SA
1090C (1995F)
1120C (2050F)
1150C (2100F)

Distaloy SA + 0.5% C
103 psi

HV10

131

300

750

109

250

80

600

87

200

70

450

65

150

60

44

100

50

22

50

MPa

Tensile and Yield strength

900

300
Tensile str.

150

HRB

Hardness

90

6.2

6.4

GPa

6.6

6.8

7.0

0
7.2

106 psi

40

HV10
HRB

Yield str

6.2

6.4

6.6

6.8

7.0

7.2

30

Ft lb

29.0

J
60

180

26.1

50

36.7

160

23.2

40

29.3

140

20.3

30

22.0

120

17.4

20

14.7

100

14.5

10

7.3

11.6
7.2

Young's modulus

200

80

6.2

6.4

6.6

6.8

7.0

6.2

0.2

0.1

0.0

-0.1

-0.2

6.2

6.4

6.6

6.8

Sintered density (g/cm3)

7.0

7.2

-0.3
6.2

6.6

6.8

44.0

7.0

7.2

7.0

7.2

0.0

Dimensional change

0.3

10

6.4

Elongation

%
12

Impact energy

6.4

6.6

6.8

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Amide wax; P: 300 - 700 MPa conventional compaction.
S: Various temperatures, 30 min in 90/10 N2/H2.
Dimensional change: Green to as sintered.

175

Iron and steel powders for sintered components

176

Distaloy SA

177

Iron and steel powders for sintered components

178

Distaloy AB

Distaloy AB

179

Iron and steel powders for sintered components

Typical data, Distaloy AB

180

Distaloy AB
Springback

%
0.4

0.8 % Amide-wax
0.8% Zn-st

0.3

0.6 % Kenolube
0.6% Lube + 0.45% Graphite, Warm compaction

0.2

Lubricated tool die

0.1
0.0

300

600

500

400

g/cm3

700

800

900

700

800

900

Green density

7.5
7.4
7.3
7.2
7.1
7.0
6.9
6.8
6.7
6.6
6.5
300

600

500

400

Green strength

MPa

psi

60

8700

50

7250

40

5800

30

4350

20

2900

10

1450

0
300
25

600

500

400
30

35

40

45

50

900

800

700
55

60

Compacting pressure (MPa and tsi)

181

Iron and steel powders for sintered components

182

Distaloy AB

183

Iron and steel powders for sintered components


1090C (1995F)
1120C (2050F)
1150C (2100F)

Distaloy AB + 0.5% C
103 psi

HV10

131

300

750

109

250

90

600

87

200

80

450

65

150

70

44

100

60

22

50

MPa

Tensile and Yield strength

900

300
Tensile str.

150

HRB

Hardness

100

6.6

6.8

7.0

7.2

7.4

0
7.6

50

HV10
HRB

Yield str

6.6

6.8

7.0

7.2

7.4

7.6

40

106 psi

29.0

60

180

26.1

50

36.7

160

23.2

40

29.3

140

20.3

30

22.0

120

17.4

20

14.7

100

14.5

10

7.3

11.6
7.6

GPa

Young's modulus

200

80

6.6

6.8

7.0

7.2

7.4

0.2

0.1

0.0

-0.1

-0.2

6.6

6.8

7.0

7.2

Sintered density (g/cm3)

6.8

7.4

7.6

-0.3

7.0

7.2

44.0

7.4

Conventional compaction
Warm compaction

6.6

6.8

7.0

7.2

7.4

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube respectively; P: 400 - 800 MPa
conventional and warm compaction, S: Various temperatures, 30 min in 90/10 N2/H2.
Dimensional change: Green to as sintered.

184

7.6

Dimensional change

0.3

10

6.6

Elongation

12

Ft lb

Impact energy

7.6

0.0

Distaloy AB

185

Iron and steel powders for sintered components

550 - 650 MPa

186

187

Iron and steel powders for sintered components

MANUFACTU
and warm c
20 min at 0
Dimensiona

188

Distaloy AB

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube resp.; P: 500 - 800 MPa conventional
and warm compaction; S: 1120C (2050F), 20 min in 90/10 N2/H2. Carburizing 920C (1690F),
20 min at 0.8% C-pot. Tempering 180C (355F), 60 min in air.
Dimensional change: Green to as hardened.

189

Iron and steel powders for sintered components

MANUFACT
20 min in 9
60 min in a

190

Distaloy AB

MANUFACTURING CONDITIONS: 0.8% Amide wax; P: 650 MPa conventional compaction; S: 1120C (2050F),
20 min in 90/10 N2/H2. Carburizing 920C (1690F), various time at 0.8% C-pot. Tempering 180C (355F),
60 min in air. Dimensional change: Green to as hardened.

191

Iron and steel powders for sintered components

192

Distaloy AB

193

Iron and steel powders for sintered components

0.1% graphite addition

0.2% graphite addition

194

Distaloy AB

0.1% graphite addition

195

Iron and steel powders for sintered components

0.1% graphite addition

0.2% graphite addition

196

Distaloy AB

0.1% graphite addition

197

Iron and steel powders for sintered components

198

Distaloy AE

Distaloy AE

199

Iron and steel powders for sintered components

Typical data, Distaloy AE

200

Distaloy AE
Springback

%
0.4

0.8 % Amide-wax
0.8% Zn-st

0.3

0.6 % Kenolube
0.6% Lube + 0.45% Graphite, Warm compaction

0.2

Lubricated tool die

0.1
0.0

500

400

300

g/cm3

600

700

800

900

700

800

900

Green density

7.5
7.4
7.3
7.2
7.1
7.0
6.9
6.8
6.7
6.6
6.5
600

500

400

300

Green strength

MPa

psi

60

8700

50

7250

40

5800

30

4350

20

2900

10

1450
0

0
300
25

600

500

400
30

35

40

45

700
50

900

800
55

60

Compacting pressure (MPa and tsi)

201

Iron and steel powders for sintered components

202

Distaloy AE

203

Iron and steel powders for sintered components




204

Distaloy AE

Distaloy AE + 0.5% C

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube respectively; P: 400 - 800 MPa
conventional and warm compaction, S: 1120C (2050F), various time in 90/10 N2/H2.
Dimensional change: Green to as sintered.

205

Iron and steel powders for sintered components

550 - 650 MPa

206

Distaloy AE

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube resp. P: 400 - 800 MPa conventional
and warm compaction, S: 1250C (2282F), 30 min in 90/10 N2/H2, convective cooling rate 2.5C/s.
Tempering 180C (355F), 60 min in air. Dimensional change: Green to as sintered.

207

Iron and steel powders for sintered components

Distaloy AE + C (sintered density 7.0 g/cm3)

208

Distaloy AE

Distaloy AE + 0.5% C

209

Iron and steel powders for sintered components

MANUFACTU
and warm co
20 min at 0.
Dimensional

210

Distaloy AE

Conventional compaction
Warm compaction

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube resp.; P: 500 - 800 MPa conventional
and warm compaction; S: 1120C (2050F), 20 min in 90/10 N2/H2. Carburizing 920C (1690F),
20 min at 0.8% C-pot. Tempering 180C (355F), 60 min in air.
Dimensional change: Green to as hardened.

211

Iron and steel powders for sintered components

MANUFACTU
20 min in 90
60 min in air

212

Distaloy AE

MANUFACTURING CONDITIONS: 0.8% Amide wax; P: 650 MPa conventional compaction; S: 1120C (2050F),
20 min in 90/10 N2/H2. Carburizing 920C (1690F), various time at 0.8% C-pot. Tempering 180C (355F),
60 min in air. Dimensional change: Green to as hardened.

213

Iron and steel powders for sintered components

214

Distaloy AE

215

Iron and steel powders for sintered components

216

Distaloy AE

0.1% graphite
0.2% graphite

217

Iron and steel powders for sintered components

218

Distaloy AE

0.1% graphite
0.2% graphite

219

Iron and steel powders for sintered components

220

Distaloy AF

Distaloy AF

221

Iron and steel powders for sintered components

Typical data, Distaloy AF

222

Distaloy AF
Springback

%
0.4

0.8 % Amide-wax
0.8% Zn-st

0.3

0.6 % Kenolube
0.6% Lube + 0.45% Graphite, Warm compaction

0.2

Lubricated tool die

0.1
0.0

300

500

400

g/cm3

600

700

800

900

700

800

900

Green density

7.5
7.4
7.3
7.2
7.1
7.0
6.9
6.8
6.7
6.6
6.5
600

500

400

300

Green strength

MPa

psi

60

8700

50

7250

40

5800

30

4350

20

2900

10

1450

0
300
25

600

500

400
30

35

40

45

700
50

900

800
55

60

Compacting pressure (MPa and tsi)

223

Iron and steel powders for sintered components

Conventional compaction

224

Distaloy AF

225

Iron and steel powders for sintered components

226

Distaloy AF

227

Iron and steel powders for sintered components

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube respectively; P: 550 - 650 MPa
conventional and warm compaction, S: 1120C (2050F), 30 min in 90/10 N2/H2.
Dimensional change: Green to as sintered.

228

Distaloy DC

Distaloy DC

229

Iron and steel powders for sintered components

Typical data, Distaloy DC

230

Distaloy DC
Springback

%
0.4

0.8 % Amide-wax
0.8% Zn-st

0.3

0.6 % Kenolube
0.6% Lube + 0.45% Graphite, Warm compaction

0.2

Lubricated tool die

0.1
0.0

300

600

500

400

g/cm3

700

800

900

700

800

900

Green density

7.5
7.4
7.3
7.2
7.1
7.0
6.9
6.8
6.7
6.6
6.5
300

600

500

400

Green strength

MPa

psi

60

8700

50

7250

40

5800

30

4350

20

2900

10

1450

0
300
25

600

500

400
30

35

40

45

700
50

900

800
55

60

Compacting pressure (MPa and tsi)

231

Iron and steel powders for sintered components

232

Distaloy DC

233

Iron and steel powders for sintered components

234

Distaloy DC

235

Iron and steel powders for sintered components

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube respectively; P: 550 - 650 MPa
conventional and warm compaction, S: 1120C (2050F), 30 min in 90/10 N2/H2.
Dimensional change: Green to as sintered.

236

237

Iron and steel powders for sintered components

238

MANUFACT
and warm c
20 min at 0
Dimensiona

Distaloy DC

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube resp.; P: 500 - 800 MPa conventional
and warm compaction; S: 1120C (2050F), 20 min in 90/10 N2/H2. Carburizing 920C (1690F),
20 min at 0.8% C-pot. Tempering 180C (355F), 60 min in air.
Dimensional change: Green to as hardened.

239

Iron and steel powders for sintered components

240

MANUFAC
20 min in
60 min in

Distaloy DC

MANUFACTURING CONDITIONS: 0.8% Amide wax; P: 650 MPa conventional compaction; S: 1120C (2050F),
20 min in 90/10 N2/H2. Carburizing 920C (1690F), various time at 0.8% C-pot. Tempering 180C (355F),
60 min in air. Dimensional change: Green to as hardened.

241

Iron and steel powders for sintered components

242

Distaloy DC

243

Iron and steel powders for sintered components

244

MANUFACT
20 min in 9
60 min in a

Distaloy DC

0.1% graphite addition

MANUFACTURING CONDITIONS: 0.8% Amide wax; P: 650 MPa conventional compaction; S: 1120C (2050F),
20 min in 90/10 N2/H2. Carburizing 920C (1690F), 20 min at 0.8% C-pot. Tempering 180C (355F),
60 min in air. Dimensional change: Green to as hardened.

245

Iron and steel powders for sintered components

246

MANUF
90/10
Dimens

Distaloy DC

MANUFACTURING CONDITIONS: 0.6% Lube; P: 650 MPa warm compaction; S: 1120C (2050F), 20 min in
90/10 N2/H2. Carburizing 920C (1690F), 20 min at 0.8% C-pot. Tempering 180C (355F), 60 min in air.
Dimensional change: Green to as hardened.

247

Iron and steel powders for sintered components

248

Distaloy DH

Distaloy DH

249

Iron and steel powders for sintered components

Typical data, Distaloy DH

250

Distaloy DH
Springback

%
0.4

0.8 % Amide-wax
0.8% Zn-st

0.3

0.6 % Kenolube
0.6% Lube + 0.45% Graphite, Warm compaction

0.2

Lubricated tool die

0.1
0.0

300

600

500

400

g/cm3

700

800

900

700

800

900

Green density

7.5
7.4
7.3
7.2
7.1
7.0
6.9
6.8
6.7
6.6
6.5
300

600

500

400

Green strength

MPa

psi

60

8700

50

7250

40

5800

30

4350

20

2900

10

1450

0
300
25

600

500

400
30

35

40

45

700
50

900

800
55

60

Compacting pressure (MPa and tsi)

251

Iron and steel powders for sintered components

252

Distaloy DH

253

Iron and steel powders for sintered components


1090C (1995F)
1120C (2050F)
1150C (2100F)

Distaloy DH + 0.5% C
10 3psi

HV10

131

300

750

109

250

90

600

87

200

80

450

65

150

70

300

44

100

60

22

50

MPa

Tensile and Yield strength

900

Tensile str.

150

HRB

Hardness

100

6.5

6.7

GPa

6.9

7.1

7.3

0
7.5

50

HV10
HRB

Yield str

6.5

6.7

6.9

7.1

7.3

7.5

40

10 psi

29.0

60

180

26.1

50

36.7

160

23.2

40

29.3

140

20.3

30

22.0

120

17.4

20

14.7

100

14.5

10

7.3

11.6
7.5

Young's modulus

200

80

6.5

6.7

6.9

7.1

7.3

0.5

0.4

0.3

0.2

0.1

6.5

6.7

6.9

7.1

Sintered density (g/cm3)

6.7

7.3

7.5

0.0

6.9

7.1

44.0

7.3

7.5

7.3

7.5

Dimensional change

0.6

6.5

Elongation

Ft lb

Impact energy

Conventional compaction
Warm compaction

6.5

6.7

6.9

7.1

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube respectively; P: 400 - 800 MPa
conventional and warm compaction, S: Various temperatures, 30 min in 90/10 N 2 /H2 .
Dimensional change: Green to as sintered.

254

0.0

Distaloy DH

255

Iron and steel powders for sintered components

256

257

Iron and steel powders for sintered components

258

Distaloy DH

Distaloy DH
Case hardening
MVH0.1

mm

Micro hardness profiles

1000
800
600
400

6.80 g/cm3
7.15 g/cm3

200
0

7.35 g/cm3

0.0

0.5

1.0

2.0

1.5

94

2.0

78

1.6

63

1.2

47

0.8

31

0.4

16

0.0

2.5

Thau

Case Depth

2.4

6.6

6.8

7.0

7.2

7.4

7.6

Distance from surface (mm)


HV5

MPa

Hardness

600

103 psi

Tensile and Yield strength

1100

160

550

1000

145

500

900

131

450

800

116

400

700
600

350
300

6.6

6.8

7.0

7.4

7.2

Young's modulus

Elongation

500

7.6

GPa 106psi

29 0.6

180

26 0.5

2.0

160

23 0.4

1.5

140

20 0.3

1.0

120

17 0.2

0.5

100

15 0.1

80

12 0.0

Young's modulus

2.5

0.0

Elongation

6.6

6.8

7.0

7.2

7.4

Sintered density (g/cm )


3

7.6

87

Yield strength

6.6

6.8

200

3.0

102
Tensile strength

7.0

7.2

7.4

7.6

73

Dimensional change
Conventional compaction
Warm compaction

6.6

6.8

7.0

7.2

7.4

7.6

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube resp.; P: 500 - 800 MPa conventional
and warm compaction; S: 1120C (2050F), 20 min in 90/10 N2/H2. Carburizing 920C (1690F),
20 min at 0.8% C-pot. Tempering 180C (355F), 60 min in air.
Dimensional change: Green to as hardened.

259

Iron and steel powders for sintered components

260

Distaloy DH

MANUFACTURING CONDITIONS: 0.8% Amide wax; P: 650 MPa conventional compaction; S: 1120C (2050F),
20 min in 90/10 N2/H2. Carburizing 920C (1690F), various time at 0.8% C-pot. Tempering 180C (355F),
60 min in air. Dimensional change: Green to as hardened.

261

Iron and steel powders for sintered components

262

Distaloy DH

263

Iron and steel powders for sintered components

MANUFAC
(2050F),
Tempering

264

Distaloy DH

MANUFACTURING CONDITIONS: 0.8% Amide wax; P: 650 MPa conventional compaction; S: 1120C
(2050F), 20 min in 90/10 N2/H2. Carburizing 920C (1690F), 20 min at 0.8% C-pot.
Tempering 180C (355F), 60 min in air. Dimensional change: Green to as hardened.

265

Iron and steel powders for sintered components

266

MANUFACT
90/10 N2/H
Dimensiona

Distaloy DH

MANUFACTURING CONDITIONS: 0.6% Lube; P: 650 MPa warm compaction; S: 1120C (2050F), 20 min in
90/10 N2/H2. Carburizing 920C (1690F), 20 min at 0.8% C-pot. Tempering 180C (355F), 60 min in air.
Dimensional change: Green to as hardened.

267

Iron and steel powders for sintered components

268

Distaloy HP

Distaloy HP

269

Iron and steel powders for sintered components

Typical data, Distaloy HP

270

Distaloy HP
Springback

%
0.4

0.8 % Amide-wax
0.8% Zn-st

0.3

0.6 % Kenolube
0.6% Lube + 0.45% Graphite, Warm compaction

0.2

Lubricated tool die

0.1
0.0

300

600

500

400

g/cm3

700

800

900

700

800

900

Green density

7.5
7.4
7.3
7.2
7.1
7.0
6.9
6.8
6.7
6.6
6.5
400

300

600

500

Green strength

MPa

psi

60

8700

50

7250

40

5800

30

4350

20

2900

10

1450

0
300
25

600

500

400
30

35

40

45

700
50

900

800
55

60

Compacting pressure (MPa and tsi)

271

Iron and steel powders for sintered components

272

Distaloy HP

273

Iron and steel powders for sintered components


1090C (1995F)
1120C (2050F)
1150C (2100F)

Distaloy HP + 0.5% C
MPa

103 psi

Tensile and Yield strength

1400

HV10

HRB

Hardness

203

400

1200

174

350

90

1000

145

300

80

800

116

250

70

600

87

200

60

58

150

29
7.5

100

Tensile str.

400

100

200

6.5

6.7

6.9

7.1

7.3

50

HV10
HRB

Yield str

6.5

6.7

6.9

7.1

7.3

7.5

40

106 psi

29.0

60

180

26.1

50

36.7

160

23.2

40

29.3

140

20.3

30

22.0

120

17.4

20

14.7

100

14.5

10

7.3

11.6
7.5

GPa

Young's modulus

200

80

6.5

6.7

6.9

7.1

7.3

6.5

0.2

0.1

0.0

-0.1

-0.2

6.5

6.7

6.9

7.1

7.3

Sintered density (g/cm )


3

7.5

-0.3
6.5

6.9

7.1

44.0

7.3

7.5

7.3

7.5

Dimensional change

0.3

6.7

Elongation

Ft lb

Impact energy

Conventional compaction
Warm compaction

6.7

6.9

7.1

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube respectively; P: 400 - 800 MPa
conventional and warm compaction, S: Various temperatures, 30 min in 90/10 N2/H2.
Dimensional change: Green to as sintered.

274

0.0

Distaloy HP

275

Iron and steel powders for sintered components

P: 550 - 650 MPa

276

Distaloy HP

277

Iron and steel powders for sintered components




278

Distaloy HP

279

Iron and steel powders for sintered components

MANUFACTU
and warm c
20 min at 0
Dimensional

280

Distaloy HP

Conventional compaction
Warm compaction

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube resp.; P: 500 - 800 MPa conventional
and warm compaction; S: 1120C (2050F), 20 min in 90/10 N2/H2. Carburizing 920C (1690F),
20 min at 0.8% C-pot. Tempering 180C (355F), 60 min in air.
Dimensional change: Green to as hardened.

281

Iron and steel powders for sintered components

MANUFACTUR
20 min in 90/
60 min in air.

282

Distaloy HP

MANUFACTURING CONDITIONS: 0.8% Amide wax; P: 650 MPa conventional compaction; S: 1120C (2050F),
20 min in 90/10 N2/H2. Carburizing 920C (1690F), various time at 0.8% C-pot. Tempering 180C (355F),
60 min in air. Dimensional change: Green to as hardened.

283

Iron and steel powders for sintered components

284

Distaloy HP

285

Iron and steel powders for sintered components

286

MANUFACT
20 min in 9
60 min in a

Distaloy HP

Plain iron grades

MANUFACTURING CONDITIONS: 0.8% Amide wax; P: 650 MPa conventional compaction; S: 1120C (2050F),
20 min in 90/10 N2/H2. Carburizing 920C (1690F), 20 min at 0.8% C-pot. Tempering 180C (355F),
60 min in air. Dimensional change: Green to as hardened.

287

Iron and steel powders for sintered components

288

MANUFA
20 min in
Temperin

Distaloy HP

MANUFACTURING CONDITIONS: 0.6% Lube; P: 650 MPa warm compaction; S: 1120C (2050F),
20 min in 90/10 N2/H2. Carburizing 920C (1690F), 20 min at 0.8% C-pot.
Tempering 180C (355F), 60 min in air. Dimensional change: Green to as hardened.

289

Iron and steel powders for sintered components

290

Iron and steel powders for sintered components

Pre-alloyed grades
Astaloy 85 Mo
Astaloy Mo
Astaloy A
Astaloy B
Astaloy CrL
Astaloy CrM

291

Iron and steel powders for sintered components

292

Astaloy 85 Mo

Astaloy 85 Mo

293

Iron and steel powders for sintered components

294

Astaloy 85 Mo
Springback

%
0.4

0.8 % Amide-wax
0.8% Zn-st

0.3

0.6 % Kenolube
0.6% Lube, Warm compaction

0.2

Lubricated tool die

0.1
0.0

600

500

400

300

g/cm3

700

800

900

700

800

900

Green density

7.5
7.4
7.3
7.2
7.1
7.0
6.9
6.8
6.7
6.6
6.5
300

500

400

600

Green strength

MPa

psi

30

4350

25

3625

20

2900

15

2175

10

1450

725
0

0
300
25

600

500

400
30

35

40

45

700
50

900

800
55

60

Compacting pressure (MPa and tsi)

295

Iron and steel powders for sintered components

296

Astaloy 85 Mo
0% C
0.5% C
0.8% C

Astaloy 85 Mo + C
MPa
900

103 psi

Tensile and Yield strength

HV10

HRB

Hardness

131

300

109

250

600

87

200

70

450

65

150

60

300

44

100

50

150

22

50

40

Tensile str.

750

Yield str

6.6

6.8

7.0

7.2

7.4

0
7.6

90

HV10
HRB

6.6

6.8

80

7.0

7.2

7.4

7.6

30

106 psi

29.0

90

180

26.1

75

55.2

160

23.2

60

44.2

140

20.3

45

33.1

120

17.4

30

22.1

100

14.5

15

11.0

11.6
7.6

GPa

Young's modulus

200

80

6.6

6.8

7.0

7.2

7.4

6.6

0.1

12

0.0

-0.1

-0.2

-0.3

0
6.6

-0.4
6.6

7.0

7.2

Sintered density (g/cm3)

7.4

7.6

7.0

7.2

66.3

7.4

7.6

0.0

Dimensional change

0.2

15

6.8

6.8

Elongation

18

Ft lb

Impact energy

Conventional compaction
Warm compaction

6.8

7.0

7.2

7.4

7.6

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube respectively; P: 400 - 800 MPa
conventional and warm compaction, S: 1120C (2050F), 30 min in 90/10 N2/H2.
Dimensional change: Green to as sintered.

297

Iron and steel powders for sintered components


0% C
0.5% C
0.8% C

Astaloy 85 Mo + 1% Cu + C
MPa

103 psi

Tensile and Yield strength

900

HV10

HRB

Hardness

131

300

750

109

250

80

600

87

200

70

450

65

150

60

300

44

100

50

22

50

Tensile str.

150

90

0
6.6

6.8

7.0

7.2

7.4

7.6

40

HV10
HRB

Yield str

6.6

6.8

7.0

7.2

7.4

7.6

30

106 psi

29.0

90

180

26.1

75

55.2

160

23.2

60

44.2

140

20.3

45

33.1

120

17.4

30

22.1

100

14.5

15

11.0

80

11.6
7.6

GPa

Young's modulus

200

6.6

6.8

7.0

7.2

7.4

6.6

0.2

0.1

0.0

-0.1

-0.2

6.6

6.8

7.0

7.2

Sintered density (g/cm3)

7.4

7.6

-0.3
6.6

7.0

7.2

66.3

7.4

Conventional compaction
Warm compaction

6.8

7.0

7.2

7.4

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube respectively; P: 400 - 800 MPa
conventional and warm compaction, S: 1120C (2050F), 30 min in 90/10 N2/H2.
Dimensional change: Green to as sintered.

298

7.6

Dimensional change

0.3

10

6.8

Elongation

12

Ft lb

Impact energy

7.6

0.0

Astaloy 85 Mo
0% Cu
1% Cu
2% Cu

Astaloy 85 Mo + 0.5% C + Cu
103 psi

HV10

131

300

750

109

250

90

600

87

200

80

450

65

150

70

300

44

100

60

22

50

MPa

Tensile and Yield strength

900

Tensile str.

150

HRB

Hardness

100

6.6

6.8

7.0

7.2

7.4

7.6

50

HV10
HRB

Yield str

6.6

6.8

7.0

7.2

7.4

7.6

40

106 psi

29.0

60

180

26.1

50

36.7

160

23.2

40

29.3

140

20.3

30

22.0

120

17.4

20

14.7

100

14.5

10

7.3

11.6

GPa

Young's modulus

200

80

6.6

6.8

7.0

7.2

7.4

7.6

0.4

0.2

0.0

-0.2

-0.4

6.6

6.8

7.0

7.2

Sintered density (g/cm3)

6.8

7.4

7.6

-0.6

7.0

7.2

44.0

7.4

7.6

7.4

7.6

0.0

Dimensional change

0.6

6.6

Elongation

Ft lb

Impact energy

Conventional compaction
Warm compaction

6.6

6.8

7.0

7.2

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube respectively; P: 400 - 800 MPa
conventional and warm compaction, S: 1120C (2050F), 30 min in 90/10 N2/H2.
Dimensional change: Green to as sintered.

299

Iron and steel powders for sintered components


0% C
0.5% C
0.8% C

Astaloy 85 Mo + 2% Ni + C
103 psi

HV10

131

300

109

250

80

600

87

200

70

450

65

150

60

300

44

100

50

150

22

50

MPa

Tensile and Yield strength

900

Tensile str.

750

Yield str

6.6

6.8

7.0

7.2

7.4

7.6

HRB

Hardness

90

HV10
HRB

6.6

6.8

7.0

7.2

7.4

40
30
7.6

106 psi

29.0

90

180

26.1

75

55.2

160

23.2

60

44.2

140

20.3

45

33.1

120

17.4

30

22.1

100

14.5

15

11.0

11.6

GPa

Young's modulus

200

80

6.6

6.8

7.0

7.2

7.4

7.6

-0.1

12

-0.2

-0.3

-0.4

-0.5

6.6

6.8

7.0

7.2

Sintered density (g/cm3)

6.8

7.4

7.6

-0.6

7.0

7.2

66.3

7.4

Conventional compaction
Warm compaction

6.6

6.8

7.0

7.2

7.4

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube respectively; P: 400 - 800 MPa
conventional and warm compaction, S: 1120C (2050F), 30 min in 90/10 N2/H2.
Dimensional change: Green to as sintered.

300

0.0
7.6

Dimensional change

0.0

15

6.6

Elongation

18

Ft lb

Impact energy

7.6

Astaloy 85 Mo
0% C
0.5% C
0.8% C

Astaloy 85 Mo + 2% Cu + 2% Ni + C
103 psi

HV10

131

300

750

109

250

90

600

87

200

80

450

65

150

70

300

44

100

60

22

50

MPa

Tensile and Yield strength

900

Tensile str.

150

HRB

Hardness

100

6.6

6.8

7.0

7.2

7.4

0
7.6

50

HV10
HRB

Yield str

6.6

6.8

7.0

7.2

7.4

7.6

40

106 psi

29.0

60

180

26.1

50

36.7

160

23.2

40

29.3

140

20.3

30

22.0

120

17.4

20

14.7

100

14.5

10

7.3

11.6
7.6

GPa

Young's modulus

200

80

6.6

6.8

7.0

7.2

7.4

6.6

0.3

0.2

0.1

0.0

-0.1

6.6

6.8

7.0

7.2

7.4

Sintered density (g/cm )


3

7.6

-0.2
6.6

7.0

7.2

44.0

7.4

7.6

0.0

Dimensional change

0.4

10

6.8

Elongation

12

Ft lb

Impact energy

Conventional compaction
Warm compaction

6.8

7.0

7.2

7.4

7.6

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube respectively; P: 400 - 800 MPa
conventional and warm compaction, S: 1120C (2050F), 30 min in 90/10 N2/H2.
Dimensional change: Green to as sintered.

301

Iron and steel powders for sintered components

Astaloy 85 Mo + C
MPa
1000

Conventional compaction SD=7.0 g/cm3


Warm compaction SD=7.2 g/cm3

Tensile and Yield strength

103 psi

HV10

HRB

Hardness

145

300

850

123

250

80

700

102

200

70

550

80

150

60

58

100

50

36

50

15
0.8

400
Tensile str.

250
100

Yield str

0.0

0.2

0.4

0.6

90

40

HV10
HRB

0.0

0.2

0.4

0.6

0.8

30

106 psi

29.0

90

180

26.1

75

55.2

160

23.2

60

44.2

140

20.3

45

33.1

120

17.4

30

22.1

100

14.5

15

11.0

80

11.6
0.8

GPa

Young's modulus

200

0.0

0.2

0.4

0.6

0.0

0.1

0.0

-0.1

-0.2

-0.3

0.0

0.2

0.4

Combined carbon (%)

0.6

0.8

-0.4
0.0

0.4

66.3

0.6

0.8

0.6

0.8

Dimensional change

0.2

10

0.2

Elongation

12

Ft lb

Impact energy

0.2

0.4

Combined carbon (%)

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube respectively; P: 550 - 650 MPa
conventional and warm compaction, S: 1120C (2050F), 30 min in 90/10 N2/H2.
Dimensional change: Green to as sintered.

302

0.0

Astaloy 85 Mo
0.4% C
0.6% C
0.8% C

Astaloy 85 Mo + 2% Cu + C (cooling rate 2.5C/s)


Sinter hardening
MPa
1000

103 psi

Tensile and Yield strength

145

Tensile str.
Yield str

900

HV10

HRC

Hardness

600

45

HV10
HRC

131

500

800

116

400

35

700

102

300

30

600

87

200

25

500

73

100

20

58
7.4

400

6.4

6.6

6.8

7.0

7.2

6.4

6.6

40

6.8

7.0

7.2

7.4

15

106 psi

29.0

30

180

26.1

25

18.4

160

23.2

20

14.7

140

20.3

15

11.1

120

17.4

10

7.4

100

14.5

3.7

11.6
7.4

GPa

Young's modulus

200

80

6.4

6.6

6.8

7.0

7.2

0.5

2.0

0.4

1.5

0.3

1.0

0.2

0.5

0.1

6.4

6.6

6.8

7.0

Sintered density (g/cm3)

6.6

7.2

7.4

0.0

6.8

7.0

22.1

7.2

7.4

7.2

7.4

0.0

Dimensional change

0.6

2.5

0.0

6.4

Elongation

3.0

Ft lb

Impact energy

6.4

6.6

6.8

7.0

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 2% Cu-30 + 0.8% Amide wax and 0.6% Lube resp. P: 400 - 800 MPa
conventional and warm compaction, S: 1120C (2050F), 30 min in 80/20 N2/H2, convective cooling rate
2.5C/s. Tempering 180C (355F), 60 min in air. Dimensional change: Green to as sintered.

303

Iron and steel powders for sintered components

304

Astaloy 85 Mo
1 C/s
2.5 C/s
5 C/s

Astaloy 85 Mo + 2% Cu + 0.6% C
Sinter hardening
MPa

103 psi

Tensile and Yield strength

1000

HV10

HRC

Hardness

145

500

131

450

800

116

400

700

102

350

30

600

87

300

25

500

73

250

20

400

58
7.4

200

Tensile str.

900

6.6

6.8

7.0

7.2

40

HV10
HRC

Yield str

6.4

45

6.4

6.6

35

6.8

7.0

7.2

7.4

15

106 psi

29.0

30

180

26.1

25

18.4

160

23.2

20

14.7

140

20.3

15

11.1

120

17.4

10

7.4

100

14.5

3.7

11.6
7.4

GPa

Young's modulus

200

80

6.4

6.6

6.8

7.0

7.2

0.5

2.0

0.4

1.5

0.3

1.0

0.2

0.5

0.1

6.4

6.6

6.8

7.0

Sintered density (g/cm3)

6.6

7.2

7.4

0.0

6.8

7.0

22.1

7.2

7.4

7.2

7.4

0.0

Dimensional change

0.6

2.5

0.0

6.4

Elongation

3.0

Ft lb

Impact energy

6.4

6.6

6.8

7.0

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 2% Cu-30 + 0.8% Amide wax and 0.6% Lube resp. P: 400 - 800 MPa
conventional and warm compaction, S: 1120C (2050F), 30 min in 80/20 N2/H2, various convective cooling
rates. Tempering 180C (355F), 60 min in air. Dimensional change: Green to as sintered.

305

Iron and steel powders for sintered components

Astaloy 85 Mo + 1% Ni + 0.1% Graphite


20 minutes carburizing
Various densities
Centre

Astaloy

Case hard

Surface

MHV0.1
1000
800
600
400
200
0

Density 7.00 g/cm3 (500 MPa conventional compaction)

0.0

HV5
600
550
500
450
400
350
300
6.6

%
3.0

Density 7.30 g/cm3 (800 MPa conventional compaction)

Elongatio

2.5
2.0
1.5
1.0
0.5
0.0

Density 7.50 g/cm3 (800 MPa warm compaction)

306

6.6

MANUFACTU
and warm c
20 min at 0
Dimensiona

Astaloy 85 Mo

Astaloy 85 Mo + 1% Ni
Case hardening
MHV0.1

mm

Micro hardness profiles

1000

Thau

Case Depth

2.4

94

7.00 g/cm3
7.30 g/cm3

800

7.50 g/cm3

600
400
200
0

0.0

0.5

1.0

1.5

2.0

2.0

78

1.6

63

1.2

47

0.8

31

0.4

16

0.0

2.5

6.6

6.8

7.0

7.2

7.4

7.6

Distance from surface (mm)


HV5

MPa

Hardness

600

103 psi

Tensile and Yield strength

1100

160

550

1000

145

500

900

131

450

800

116

400

700
600

350
300
6.6

6.8

7.0

Elongation

7.2

7.4

Young's modulus

500
6.6

7.6

GPa 106psi
29

0.3

180

26

0.2

2.0

160

23

0.1

1.5

140

20

0.0

1.0

120

17 -0.1

0.5

100

15 -0.2

Young's modulus

2.5

0.0

Elongation

6.6

6.8

7.0

7.2

Sintered density (g/cm3)

7.4

80
7.6

12 -0.3

87

Yield strength

6.8

200

3.0

102
Tensile strength

7.0

7.2

7.4

7.6

7.4

7.6

73

Dimensional change
Conventional compaction
Warm compaction

6.6

6.8

7.0

7.2

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube resp.; P: 500 - 800 MPa conventional
and warm compaction; S: 1120C (2050F), 20 min in 90/10 N2/H2. Carburizing 920C (1690F),
20 min at 0.8% C-pot. Tempering 180C (355F), 60 min in air.
Dimensional change: Green to as hardened.

307

Iron and steel powders for sintered components

Astaloy 85 Mo +1% Ni + 0.1% Graphite


650 MPa conventional compaction (7.20 g/cm3)
Various carburizing time
Centre

Astaloy 85 M
Case hardning
Surface

MVH0.1

Micro

1000
800
600
400

7 minute

20 minu

200

40 minu

0
0.0

0.5

Distanc
HV5

7 minutes carburizing

600
550
500
450
400
350
300

10

Elongation

3.0

20 minutes carburizing

Young's

2.5

Elonga

2.0
1.5
1.0
0.5
0.0

40 minutes carburizing

308

10

MANUFACTURING C
20 min in 90/10 N2
Tempering 180C (

Astaloy 85 Mo

MANUFACTURING CONDITIONS: 0.8% Amide wax; P: 650 MPa conventional compaction; S: 1120C (2050F),
20 min in 90/10 N2/H2. Carburizing 920C (1690F), various time at 0.8% C-pot. Tempering 180C (355F),
60 min in air. Dimensional change: Green to as hardened.

309

Iron and steel powders for sintered components

Astaloy 85 Mo +1% Ni + 0.1% Graphite


650 MPa warm compaction (7.40 g/cm3)
Various carburizing time
Centre

Astaloy

Case har

Surface

MVH0.1
1000
800
600
400
200
0
0.0

HV5

7 minutes carburizing

600
550
500
450
400
350
300

%
3.0

20 minutes carburizing

Elongat

2.5
2.0
1.5
1.0
0.5
0.0

40 minutes carburizing

310

MANUFACT
90/10 N2/
Dimension

Astaloy 85 Mo

Astaloy 85 Mo + 1% Ni
Case hardening
MVH0.1

mm

Micro hardness profiles

1000

Thau

Case Depth

1.2

47

7 minutes carburizing
20 minutes carburizing

800

40 minutes carburizing

600
400
200
0
0.0

0.5

1.0

1.5

2.0

1.0

39

0.8

31

0.6

23

0.4

16

0.2

0.0

2.5

10

20

30

40

50

Distance from surface (mm)


HV5

MPa

Hardness

600

103 psi

Tensile and Yield strength

1100

159.5

550

1000

145.0

500

900

130.5

450

800

116.0

400

700

350
300

%
3.0

600

10

20

30

40

Young's modulus

Elongation

500

50

GPa 106psi

29 0.3

180

28 0.2

2.0

160

26 0.1

1.5

140

25 0.0

1.0

120

23 -0.1

0.5

100

22 -0.2

80

20 -0.3

Young's modulus

2.5

Elongation

10

20

30

Carburizing time (min)

40

50

87.0

Yield strength

10

200

0.0

101.5
Tensile strength

20

30

40

50

40

50

72.5

Dimensional change

10

20

30

Carburizing time (min)

MANUFACTURING CONDITIONS: 0.6% Lube; P: 650 MPa warm compaction; S: 1120C (2050F), 20 min in
90/10 N2/H2. Carburizing 920C (1690F), various time at 0.8% C-pot. Tempering 180C (355F), 60 min in air.
Dimensional change: Green to as hardened.

311

Iron and steel powders for sintered components

Astaloy 85 Mo + 1% Ni
650 MPa conventional compaction (7.20 g/cm3), 20 minutes carburizing
Various graphite additions
Surface
Centre

Astalo

Case ha
MVH0.1
1000
800
600
400
200
0

0.0

HV5

No graphite addition

600
550
500
450
400
350
300
0.0

%
3.0

0.1% graphite addition

Elong

2.5
2.0
1.5
1.0
0.5
0.0

0.2% graphite addition

312

0.0

MANUFAC
in 90/10
Dimensio

Astaloy 85 Mo

MANUFACTURING CONDITIONS: 0.8% Amide wax; P: 650 MPa conventional compaction; S: 1120C (2050F),
20 min in 90/10 N2/H2. Carburizing 920C (1690F), 20 min at 0.8% C-pot. Tempering 180C (355F),
60 min in air. Dimensional change: Green to as hardened.

313

Iron and steel powders for sintered components

Astaloy 85 Mo + 1% Ni
650 MPa warm compaction (7.40 g/cm3), 20 minutes carburizing
Various graphite additions
Surface
Centre

Astaloy

Case har
MVH0.1
1000
800
600
400
200
0

0.0

HV5

No graphite addition

600
550
500
450
400
350
300
0.0

%
3.0

0.1% graphite addition

Elongat

2.5
2.0
1.5
1.0
0.5
0.0

0.0

MANUFACT
90/10 N2/
Dimensiona
0.2% graphite addition

314

Astaloy 85 Mo

Astaloy 85 Mo + 1% Ni
Case hardening
MVH0.1

mm

Micro hardness profiles

1000

No graphite addition

800

0.1% graphite addition


0.2% graphite addition

600
400
200
0

0.0

1.0

0.5

2.0

1.5

47

1.0

39

0.8

31

0.6

23

0.4

16

0.2

0.0

2.5

Thau

Case Depth

1.2

0.0

0.1

0.2

0
0.3

Distance from surface (mm)


HV5

MPa

Hardness

600

1100

Tensile and Yield strength

103 psi
160

550

1000

145

500

900

131

450

800

116

400

700
600

350
300
0.0

%
3.0

0.1

0.2

Young's modulus

Elongation

500
0.0

0.3

GPa 106psi

200

29

0.3

190

26

0.2

2.0

180

23

0.1

1.5

170

20

0.0

1.0

160

17

-0.1

0.5

150

15

-0.2

140
0.3

12

-0.3

Young's modulus

2.5

0.0

Elongation

0.0

0.1

0.2

Graphite addition (%)

102
Tensile strength

87

Yield strength

0.1

0.2

73
0.3

Dimensional change

0.0

0.1

0.2

0.3

Graphite addition (%)

MANUFACTURING CONDITIONS: 0.6% Lube; P: 650 MPa warm compaction; S: 1120C (2050F), 20 min in
90/10 N2/H2. Carburizing 920C (1690F), 20 min at 0.8% C-pot. Tempering 180C (355F), 60 min in air.
Dimensional change: Green to as hardened.

315

Iron and steel powders for sintered components

Astaloy 85 Mo + 0.1% Graphite


650 MPa conventional compaction (7.20 g/cm3), 20 minutes carburizing
Various nickel additions
Surface
Centre

Astalo

Case ha
MVH0.1
1000
800
600
400
200
0

No Nickel addition

0.0

HV5
600
550
500
450
400
350
300

1% Nickel addition

3.0

Elonga

2.5
2.0
1.5
1.0
0.5
0.0

2% Nickel addition

316

MANUFAC
20 min in
60 min in

Astaloy 85 Mo

Astaloy 85 Mo + Ni
Case hardening
MVH0.1

mm

Micro hardness profiles

1000

No Ni addition

800

1% Ni addition
2% Ni addition

600
400
200
0

0.0

0.5

1.0

1.5

2.0

47

1.0

39

0.8

31

0.6

23

0.4

16

0.2

0.0

2.5

Thau

Case Depth

1.2

Distance from surface (mm)


HV5

MPa

Hardness

600

Tensile and Yield strength

1100

103 psi
160

550

1000

145

500

900

131

450

800

116

400

700

350
300

600

Young's modulus

Elongation

500

0.3

180

26

0.2

2.0

160

23

0.1

1.5

140

20

0.0

1.0

120

17 -0.1

0.5

100

15 -0.2

80

12 -0.3

Young's modulus

2.5

0.0

Elongation

Nickel addition (%)

29

87

Yield strength

GPa 10 psi %
200

3.0

102
Tensile strength

73

Dimensional change

Nickel addition (%)

MANUFACTURING CONDITIONS: 0.8% Amide wax; P: 650 MPa conventional compaction; S: 1120C (2050F),
20 min in 90/10 N2/H2. Carburizing 920C (1690F), 20 min at 0.8% C-pot. Tempering 180C (355F),
60 min in air. Dimensional change: Green to as hardened.

317

Iron and steel powders for sintered components

Astaloy 85 Mo + 0.1% Graphite


650 MPa warm compaction (7.40 g/cm3), 20 minutes carburizing
Various nickel additions
Surface
Centre

Astalo

Case ha
MHV0.1
1000
800
600
400
200
0

No Nickel addition

0.0

HV5
600
550
500
450
400
350
300

1% Nickel addition

3.0

Elong

2.5
2.0
1.5
1.0
0.5
0.0

2% Nickel addition

318

MANUFAC
20 min in
Temperin

Astaloy 85 Mo

Astaloy 85 Mo + Ni
Case hardening
MHV0.1

mm

Micro hardness profiles

1000

Thau

Case Depth

1.2

47

No Ni addition
1% Ni addition

800

2% Ni addition

600
400
200
0

0.0

0.5

1.0

1.5

2.0

1.0

39

0.8

31

0.6

23

0.4

16

0.2

0.0

2.5

Distance from surface (mm)


HV5

MPa

Hardness

600

Tensile and Yield strength

1100

103 psi
160

550

1000

145

500

900

131

450

800

116

400

700

350
300

600

Young's modulus

Elongation

500

GPa 106psi
29

0.3

190

28

0.2

2.0

180

26

0.1

1.5

170

25

0.0

1.0

160

23 -0.1

0.5

150

22 -0.2

140

20 -0.3

Young's modulus

2.5

0.0

Elongation

Nickel addition (%)

87

Yield strength

200

3.0

102
Tensile strength

73

Dimensional change

Nickel addition (%)

MANUFACTURING CONDITIONS: 0.6% Lube; P: 650 MPa warm compaction; S: 1120C (2050F),
20 min in 90/10 N2/H2. Carburizing 920C (1690F), 20 min at 0.8% C-pot.
Tempering 180C (355F), 60 min in air. Dimensional change: Green to as hardened.

319

Iron and steel powders for sintered components

320

Astaloy Mo

Astaloy Mo

321

Iron and steel powders for sintered components

322

Astaloy Mo
Springback

%
0.4

0.8 % Amide-wax
0.8% Zn-st

0.3

0.6 % Kenolube
0.6% Lube, Warm compaction

0.2

Lubricated tool die

0.1
0.0

400

300

600

500

g/cm3

700

800

900

700

800

900

Green density

7.5
7.4
7.3
7.2
7.1
7.0
6.9
6.8
6.7
6.6
6.5
300

400

600

500

Green strength

MPa

psi

30

4350

25

3625

20

2900

15

2175

10

1450

725
0

0
400

300
25

30

600

500
35

40

45

700
50

900

800
55

60

Compacting pressure (MPa and tsi)

323

Iron and steel powders for sintered components

Astaloy Mo
Sintered density
g/cm3

g/cm3

Conventional compaction

7.3
7.2

7.4

7.1

7.3

7.0

7.2
0% C

6.9

6.7
350

0.5% C

7.0

0.8% C
0.5% C + 2% Cu

450

550

650

750

850

6.9
350

Compacting pressure (MPa)


g/cm3
7.6

7.5

7.4

7.4

7.3

7.3

7.0
350

550

650

750

7.6

650

750

850

7.0
350

450

550

650

750

P2 (MPa)

Double pressing - 0.5% C - P1: 600 MPa

7.5
7.4
7.3
7.2

S1: 750C
S1: 800C
S1: 850C

7.1
7.0
350

450

550

650

750

850

P2 (MPa)

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube respectively; P: 400 - 800 MPa
conventional, double and warm compaction, S: 1120C (2050F), 30 min in 90/10 N2/H2.

324

850

0% C
0.5% C
0.8% C

7.1

P2 (MPa)
g/cm3

550

7.2

P1: 400 MPa


P1: 600 MPa
P1: 800 MPa

450

450

g/cm3 Double pressing - P1: 600 MPa - S1: 800C


7.6

7.5

7.1

0.8% C
0.5% C + 2% Cu

Compacting pressure (MPa)

Double pressing - 0.5% C - S1: 800C

7.2

0% C

7.1

0.5% C

6.8

Warm Compaction

7.5

850

Astaloy Mo
0% C
0.5% C
0.8% C

Astaloy Mo + C
103 psi

HV10

131

300

109

250

80

600

87

200

70

450

65

150

60

300

44

100

50

150

22

50

MPa

Tensile and Yield strength

900

Tensile str.

750

0
6.5

Yield str

6.7

6.9

7.1

7.3

7.5

HRB

Hardness

90

40

HV10
HRB

6.5

6.7

6.9

7.1

7.3

30
7.5

106 psi

29.0

90

180

26.1

75

55.2

160

23.2

60

44.2

140

20.3

45

33.1

120

17.4

30

22.1

100

14.5

15

11.0

11.6
7.5

GPa

Young's modulus

200

80

6.5

6.7

6.9

7.1

7.3

0.2

12

0.1

0.0

-0.1

-0.2

6.7

6.9

7.1

Sintered density (g/cm3)

6.7

7.3

7.5

-0.3

6.9

7.1

66.3

7.3

7.5

7.3

7.5

0.0

Dimensional change

0.3

15

0
6.5

6.5

Elongation

18

Ft lb

Impact energy

Conventional compaction
Warm compaction

6.5

6.7

6.9

7.1

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube respectively; P: 400 - 800 MPa
conventional and warm compaction, S: 1120C (2050F), 30 min in 90/10 N2/H2.
Dimensional change: Green to as sintered.

325

Iron and steel powders for sintered components


1090C (1995F)
1120C (2050F)
1150C (2100F)

Astaloy Mo+ 0.5% C


MPa

103 psi

Tensile and Yield strength

900

HV10

HRB

Hardness

131

300

750

109

250

80

600

87

200

70

450

65

150

60

44

100

50

22

50

300
Tensile str.

150

90

6.5

6.7

6.9

7.1

7.3

0
7.5

40

HV10
HRB

Yield str

6.5

6.7

6.9

7.1

7.3

7.5

30

106 psi

29.0

60

180

26.1

50

36.7

160

23.2

40

29.3

140

20.3

30

22.0

120

17.4

20

14.7

100

14.5

10

7.3

11.6
7.5

GPa

Young's modulus

200

80

6.5

6.7

6.9

7.1

7.3

6.5

0.2

0.1

0.0

-0.1

-0.2

6.5

6.7

6.9

7.1

Sintered density (g/cm3)

7.3

7.5

-0.3
6.5

6.9

7.1

44.0

7.3

7.5

7.3

7.5

Dimensional change

0.3

6.7

Elongation

Ft lb

Impact energy

Conventional compaction
Warm compaction

6.7

6.9

7.1

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube respectively; P: 400 - 800 MPa
conventional and warm compaction, S: Various temperatures, 30 min in 90/10 N2/H2.
Dimensional change: Green to as sintered.

326

0.0

Astaloy Mo
15 minutes
30 minutes
45 minutes

Astaloy Mo + 0.5% C
MPa

103 psi

Tensile and Yield strength

HV10

HRB

Hardness

90

131

300

750

109

250

80

600

87

200

70

450

65

150

60

44

100

50

22

50

900

300
Tensile str.

150
0

0
6.5

6.7

6.9

7.1

7.3

Young's modulus

7.5

40

HV10
HRB

Yield str

6.5

6.7

6.9

7.1

7.3

7.5

30

106 psi

200

29.0

60

180

26.1

50

36.7

160

23.2

40

29.3

140

20.3

30

22.0

120

17.4

20

14.7

100

14.5

10

7.3

11.6
7.5

GPa

80

6.5

6.7

6.9

7.1

7.3

6.5

0.2

0.1

0.0

-0.1

-0.2

6.5

6.7

6.9

7.1

Sintered density (g/cm3)

7.3

7.5

-0.3
6.5

6.9

7.1

44.0

7.3

7.5

7.3

7.5

0.0

Dimensional change

0.3

6.7

Elongation

Ft lb

Impact energy

Conventional compaction
Warm compaction

6.7

6.9

7.1

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube respectively; P: 400 - 800 MPa
conventional and warm compaction, S: 1120C (2050F), various time in 90/10 N2/H2.
Dimensional change: Green to as sintered.

327

Iron and steel powders for sintered components


0% C
0.5% C
0.8% C

Astaloy Mo + 1% Cu + C
103 psi

HV10

131

300

109

250

80

600

87

200

70

450

65

150

60

300

44

100

50

150

22

50

MPa

Tensile and Yield strength

900
750

6.5

Tensile str.
Yield str

6.7

6.9

7.1

7.3

7.5

HRB

Hardness

90

40

HV10
HRB

6.5

6.7

6.9

7.1

7.3

7.5

30

106 psi

29.0

90

180

26.1

75

55.2

160

23.2

60

44.2

140

20.3

45

33.1

120

17.4

30

22.1

100

14.5

15

11.0

11.6
7.5

GPa

Young's modulus

200

80

6.5

6.7

6.9

7.1

7.3

0.2

0.1

0.0

-0.1

-0.2

6.5

6.7

6.9

7.1

Sintered density (g/cm3)

6.7

7.3

7.5

-0.3

6.9

7.1

66.3

7.3

Conventional compaction
Warm compaction

6.5

6.7

6.9

7.1

7.3

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube respectively; P: 400 - 800 MPa
conventional and warm compaction, S: 1120C (2050F), 30 min in 90/10 N2/H2.
Dimensional change: Green to as sintered.

328

7.5

Dimensional change

0.3

10

6.5

Elongation

12

Ft lb

Impact energy

7.5

0.0

Astaloy Mo
0% Cu
1% Cu
2% Cu

Astaloy Mo + 0.5%C + Cu
103 psi

HV10

131

300

750

109

250

90

600

87

200

80

450

65

150

70

300

44

100

60

22

50

MPa

Tensile and Yield strength

900

Tensile str.

150

HRB

Hardness

100

0
6.5

0
6.7

6.9

7.1

7.3

7.5

50

HV10
HRB

Yield str

0
6.5

40
6.7

6.9

7.1

7.3

7.5

10 psi

29.0

60

180

26.1

50

36.7

160

23.2

40

29.3

140

20.3

30

22.0

120

17.4

20

14.7

100

14.5

10

7.3

GPa

Young's modulus

200

80
6.5

6.7

6.9

7.1

7.3

11.6
7.5

0.2

0.1

0.0

-0.1

-0.2

6.7

6.9

7.1

Sintered density (g/cm3)

7.3

7.5

-0.3

6.9

7.1

44.0

7.3

7.5

0.0

Dimensional change

0.3

0
6.5

6.7

Elongation

0
6.5

Ft lb

Impact energy

Conventional compaction
Warm compaction

6.5

6.7

6.9

7.1

7.3

7.5

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube respectively; P: 400 - 800 MPa
conventional and warm compaction, S: 1120C (2050F), 30 min in 90/10 N 2 /H 2 .
Dimensional change: Green to as sintered.

329

Iron and steel powders for sintered components

Astaloy Mo + C
MPa

Conventional compaction SD=7.0 g/cm3


Warm compaction SD=7.2 g/cm3

Tensile and Yield strength

103 psi

HV10

HRB

Hardness

90

131

300

750

109

250

80

600

87

200

70

450

65

150

60

44

100

50

22

50

900

300
Tensile str.

150
0

Yield str

0.0

0.2

0.4

0.6

0.8

40

HV10
HRB

0.0

0.2

0.4

0.6

0.8

30

106 psi

29.0

90

180

26.1

75

55.2

160

23.2

60

44.2

140

20.3

45

33.1

120

17.4

30

22.1

100

14.5

15

11.0

11.6
0.8

GPa

Young's modulus

200

80

0.0

0.2

0.4

0.6

0.0

0.2

0.1

0.0

-0.1

-0.2

0.2

0.4

Combined carbon (%)

0.6

0.8

-0.3
0.0

0.4

66.3

0.6

0.8

0.6

0.8

Dimensional change

0.3

10

0
0.0

0.2

Elongation

12

Ft lb

Impact energy

0.2

0.4

Combined carbon (%)

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube respectively; P: 550 - 650 MPa
conventional and warm compaction, S: 1120C (2050F), 30 min in 90/10 N2/H2.
Dimensional change: Green to as sintered.

330

0.0

Astaloy Mo

331

Iron and steel powders for sintered components


1 C/s
2.5 C/s
5 C/s

Astaloy Mo + 2% Cu + C (sintered density 7.0 g/cm3)


Sinter hardening
103 psi

HV10

203

500

1200

174

450

1000

145

400

35

800

116

350

30

87

300

25

58

250

20

MPa
1400

Tensile and Yield strength

600

HRC

Hardness

45
40

HV10
HRC

Tensile str.

400
200
0.35

Yield str

0.45

0.55

0.65

0.75

29
0.85

200
0.35

0.45

0.55

0.65

0.75

15
0.85

106 psi

29.0

30

180

26.1

25

18.4

160

23.2

20

14.7

140

20.3

15

11.1

120

17.4

10

7.4

100

14.5

3.7

GPa

Young's modulus

200

80
0.35

0.45

0.55

0.65

0.75

11.6
0.85

0.5

2.0

0.4

1.5

0.3

1.0

0.2

0.5

0.1

0.45

0.55

0.65

Combined carbon (%)

0.75

0.85

0.0
0.35

0.55

0.65

22.1

0.75

0.0
0.85

0.75

0.85

Dimensional change

0.6

2.5

0.0
0.35

0.45

Elongation

3.0

0
0.35

Ft lb

Impact energy

0.45

0.55

0.65

Combined carbon (%)

MANUFACTURING CONDITIONS: 2% Cu-30 + 0.8% Amide wax, P: 550 - 650 MPa conventional compaction,
S: 1120C (2050F), 30 min in 80/20 N2/H2, various convective cooling rates.
Tempering 180C (355F), 60 min in air. Dimensional change: Green to as sintered.

332

Astaloy Mo
1 C/s
2.5 C/s
5 C/s

Astaloy Mo + 2% Cu + 0.6% C
Sinter hardening
103 psi

HV10

203

500

1200

174

450

1000

145

400

35

800

116

350

30

87

300

25

58

250

20

MPa

Tensile and Yield strength

1400

600
Tensile str.

400
200
6.4

Yield str

6.6

6.8

7.0

7.2

29
7.4

200
6.4

HRC

Hardness

45
40

HV10
HRC

6.6

6.8

7.0

7.2

15
7.4

106 psi

29.0

30

180

26.1

25

18.4

160

23.2

20

14.7

140

20.3

15

11.1

120

17.4

10

7.4

100

14.5

3.7

11.6
7.4

GPa

Young's modulus

200

80

6.4

6.6

6.8

7.0

7.2

0.5

2.0

0.4

1.5

0.3

1.0

0.2

0.5

0.1

6.4

6.6

6.8

7.0

Sintered density (g/cm3)

6.6

7.2

7.4

0.0

6.8

7.0

22.1

7.2

0.0
7.4

7.2

7.4

Dimensional change

0.6

2.5

0.0

6.4

Elongation

3.0

Ft lb

Impact energy

6.4

6.6

6.8

7.0

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 2% Cu-30 + 0.8% Amide wax and 0.6% Lube resp. P: 400 - 800 MPa
conventional and warm compaction, S: 1120C (2050F), 30 min in 80/20 N2/H2, various convective cooling
rates. Tempering 180C (355F), 60 min in air. Dimensional change: Green to as sintered.

333

Iron and steel powders for sintered components

Astaloy Mo + 0.1% Graphite


20 minutes carburizing
Various densities
Centre

Astaloy M

Case harde

Surface

MVH0.1
1000
800
600
400
200
0

0.0

0.5

D
HV5

Density 7.00 g/cm3 (500 MPa conventional compaction)

600
550
500
450
400
350
300

%
3.0

Density 7.25 g/cm3 (800 MPa conventional compaction)

6.6

6.8

Elongation

2.5
2.0
1.5
1.0
0.5
0.0

Density 7.45 g/cm3 (800 MPa warm compaction)

334

6.6

6.8

MANUFACTUR
and warm com
20 min at 0.8
Dimensional c

Astaloy Mo

Astaloy Mo
Case hardening
MVH0.1

mm

Micro hardness profiles

1000

7.00 g/cm3
7.25 g/cm3

800

7.45 g/cm3

600
400
200
0

0.0

0.5

1.0

1.5

2.0

47

1.0

39

0.8

31

0.6

23

0.4

16

0.2

0.0

2.5

Thau

Case Depth

1.2

6.6

6.8

7.0

7.2

7.4

7.6

Distance from surface (mm)


HV5

MPa

Hardness

600

1100

103psi

Tensile and Yield strength

160

550

1000

145

500

900

131

450

800

116

400

700

350
300

%
3.0

102
Tensile strength

600

6.6

6.8

7.0

Elongation

7.2

7.4

Young's modulus

500

7.6

GPa 106psi

6.6

6.8

200

29

0.3

180

26

0.2

2.0

160

23

0.1

1.5

140

20

0.0

1.0

120

17 -0.1

0.5

100

15 -0.2

80

12 -0.3

7.0

0.0

Elongation

6.6

6.8

7.0

7.2

7.4

Sintered density (g/cm )


3

7.6

7.2

7.4

7.6

73

Dimensional change

Young's modulus

2.5

87

Yield strength

Conventional compaction
Warm compaction

6.6

6.8

7.0

7.2

7.4

7.6

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube resp.; P: 500 - 800 MPa conventional
and warm compaction; S: 1120C (2050F), 20 min in 90/10 N2/H2. Carburizing 920C (1690F),
20 min at 0.8% C-pot. Tempering 180C (355F), 60 min in air.
Dimensional change: Green to as hardened.

335

Iron and steel powders for sintered components

Astaloy Mo + 0.1% Graphite


650 MPa conventional compaction (7.15 g/cm3)
Various carburizing time
Centre

Astaloy

Case hard
Surface

MVH0.1
1000
800
600
400
200
0

0.0

HV5

7 minutes carburizing

600
550
500
450
400
350
300

%
3.0

20 minutes carburizing

Elongatio

2.5
2.0
1.5
1.0
0.5
0.0

40 minutes carburizing

336

MANUFACT
20 min in 9
Tempering

Astaloy Mo

MANUFACTURING CONDITIONS: 0.8% Amide wax; P: 650 MPa conventional compaction; S: 1120C (2050F),
20 min in 90/10 N2/H2. Carburizing 920C (1690F), various time at 0.8% C-pot. Tempering 180C (355F),
60 min in air. Dimensional change: Green to as hardened.

337

Iron and steel powders for sintered components

Astaloy Mo + 0.1% Graphite


650 MPa warm compaction (7.35 g/cm3)
Various carburizing time
Centre

Astalo
Surface

Case ha
MVH0.1
1000
800
600
400
200
0

7 minutes carburizing

0.0

HV5
600
550
500
450
400
350
300

20 minutes carburizing

3.0

Elong

2.5
2.0
1.5
1.0
0.5
0.0

40 minutes carburizing

338

MANUFA
20 min in
Temperin

Astaloy Mo

Astaloy Mo
Case hardening
MVH0.1

mm

Micro hardness profiles

1000

Thau

Case Depth

1.2

47

7 minutes carburizing
20 minutes carburizing

800

40 minutes carburizing

600
400
200
0

0.0

0.5

1.0

1.5

2.0

1.0

39

0.8

31

0.6

23

0.4

16

0.2

0.0

2.5

10

20

30

40

50

Distance from surface (mm)


HV5

MPa

Hardness

600

103 psi

Tensile and Yield strength

1100

160

550

1000

145

500

900

131

450

800

116

400

700

350
300

%
3.0

102
Tensile strength

600

10

20

30

40

Young's modulus

Elongation

500

50

10

GPa 106psi %
200

29

0.3

180

26

0.2

2.0

160

23

0.1

1.5

140

20

0.0

1.0

120

17 -0.1

0.5

100

15 -0.2

80

12 -0.3

87

Yield strength

20

30

40

50

40

50

73

Dimensional change

Young's modulus

2.5

0.0

Elongation

10

20

30

Carburizing time (min)

40

50

10

20

30

Carburizing time (min)

MANUFACTURING CONDITIONS: 0.6% Lube; P: 650 MPa warm compaction; S: 1120C (2050F),
20 min in 90/10 N2/H2. Carburizing 920C (1690F), various time at 0.8% C-pot.
Tempering 180C (355F), 60 min in air. Dimensional change: Green to as hardened.

339

Iron and steel powders for sintered components

Astaloy Mo
650 MPa conventional compaction (7.15 g/cm3), 20 minutes carburizing
Various graphite additions
Surface
Centre

Astaloy M

Case hard
MVH0.1
1000
800
600
400
200
0

No graphite addition

0.0

HV5
600
550
500
450
400
350
300
0.0

0.1% graphite addition

3.0

Elongation

2.5
2.0
1.5
1.0
0.5
0.0

0.2% graphite addition

340

0.0

MANUFACTU
(2050F), 20
Tempering 1

Astaloy Mo

0.1% graphite
0.2% graphite

MANUFACTURING CONDITIONS: 0.8% Amide wax; P: 650 MPa conventional compaction; S: 1120C (2050F),
20 min in 90/10 N2/H2. Carburizing 920C (1690F), 20 min at 0.8% C-pot. Tempering 180C (355F),
60 min in air. Dimensional change: Green to as hardened.

341

Iron and steel powders for sintered components

Astaloy Mo
650 MPa warm compaction (7.35 g/cm3), 20 minutes carburizing
Various graphite additions
Surface
Centre

Astaloy

Case har
MVH0.1
1000
800
600
400
200
0

No graphite addition

0.0

HV5
600
550
500
450
400
350
300
0.0

0.1% graphite addition

3.0

Elongati

2.5
2.0
1.5
1.0
0.5
0.0
0.0

0.2% graphite addition

342

MANUFACT
90/10 N2/
Dimensiona

Astaloy Mo

Astaloy Mo
Case hardening
MVH0.1

Micro hardness profiles

1000

No graphite addition
0.1% graphite

800

Thau

Case Depth

mm
1.2

47

1.0

39

0.8

31

0.6

23

0.4

16

0.2

0.2% graphite

600
400
200
0

0.0

1.0

0.5

2.0

1.5

0.0

2.5

0.0

0.2

0.1

0
0.3

Distance from surface (mm)


HV5

MPa

Hardness

600

1100

Tensile and Yield strength

103 psi
160

550

1000

145

500

900

131

450

800

116

400

700

350

600

300
0.0

500
0.0

%
3.0

0.1

0.2

Young's modulus

Elongation

0.3

GPa 106psi %
200

29 0.3

180

28 0.2

2.0

160

26 0.1

1.5

140

25 0.0

1.0

120

23 -0.1

0.5

100

22 -0.2

102
Tensile strength
Yield strength

0.1

0.2

87
73
0.3

Dimensional change

Young's modulus

2.5

0.0
0.0

Elongation

0.1

0.2

Graphite addition (%)

80
0.3

20 -0.3

0.0

0.1

0.2

0.3

Graphite addition (%)

MANUFACTURING CONDITIONS: 0.6% Lube; P: 650 MPa warm compaction; S: 1120C (2050F), 20 min in
90/10 N2/H2. Carburizing 920C (1690F), 20 min at 0.8% C-pot. Tempering 180C (355F), 60 min in air.
Dimensional change: Green to as hardened.

343

Iron and steel powders for sintered components

344

Astaloy A

Astaloy A

345

Iron and steel powders for sintered components

346

Astaloy A
Springback

%
0.4

0.8 % Amide-wax
0.8% Zn-st

0.3

0.6 % Kenolube
0.6% Lube, Warm compaction

0.2

Lubricated tool die

0.1
0.0

400

300

600

500

g/cm3

700

800

900

700

800

900

Green density

7.5
7.4
7.3
7.2
7.1
7.0
6.9
6.8
6.7
6.6
6.5
300

400

600

500

Green strength

MPa

psi

30

4350

25

3625

20

2900

15

2175

10

1450

725
0

0
400

300
25

30

600

500
35

40

45

700
50

900

800
55

60

Compacting pressure (MPa and tsi)

347

Iron and steel powders for sintered components

Astaloy A
Sintered density
g/cm3
7.40
7.25

g/cm3

Conventional compaction

Warm Compaction

7.40

0% C
0.4% C

7.25

0.8% C

7.10

7.10

0.5% C + 2% Cu

6.95

6.95

6.80

6.80

6.65

6.65

0% C

6.50
350

450

550

650

750

850

6.50
350

Compacting pressure (MPa)


g/cm3
7.6

7.4

7.4

7.3

7.3

7.2

550

650

7.2
P1: 400 MPa
P1: 600 MPa
P1: 800 MPa

7.1

450

550

650

750

750

850

7.0
350

450

550

650

750

P2 (MPa)

Double pressing - 0.4% C - P1: 600 MPa


S1: 750C
S1: 800C
S1: 850C

7.5
7.4
7.3
7.2
7.1
7.0
350

450

550

650

750

850

P2 (MPa)

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube respectively; P: 400 - 800 MPa
conventional, double and warm compaction, S: 1120C (2050F), 30 min in 90/10 N2/H2.

348

850

0% C
0.4% C
0.8% C

7.1

P2 (MPa)

7.6

450

g/cm3 Double pressing - P1: 600 MPa - S1: 800C


7.6

Double pressing - 0.4% C - S1: 800C

7.5

g/cm3

0.8% C
0,5% C + 2% Cu

Compacting pressure (MPa)

7.5

7.0
350

0.4% C

850

Astaloy A
0% C
0.4% C
0.8% C

Astaloy A + C
103 psi

HV10

131

300

109

250

85

600

87

200

70

450

65

150

55

300

44

100

40

150

22

50

MPa

Tensile and Yield strength

900
750

6.4

Tensile str.
Yield str

6.6

6.8

7.0

7.2

0
7.4

HRB

Hardness

100

25

HV10
HRB

6.4

6.6

6.8

7.0

7.2

10
7.4

106 psi

29.0

90

180

26.1

75

55.2

160

23.2

60

44.2

140

20.3

45

33.1

120

17.4

30

22.1

100

14.5

15

11.0

11.6
7.4

GPa

Young's modulus

200

80

6.4

6.6

6.8

7.0

7.2

6.4

-0.1

12

-0.2

-0.3

-0.4

-0.5

6.4

6.6

6.8

7.0

Sintered density (g/cm3)

7.2

7.4

-0.6
6.4

6.8

7.0

66.3

7.2

7.4

0.0

Dimensional change

0.0

15

6.6

Elongation

18

Ft lb

Impact energy

Conventional compaction
Warm compaction

6.6

6.8

7.0

7.2

7.4

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube respectively; P: 400 - 800 MPa
conventional and warm compaction, S: 1120C (2050F), 30 min in 90/10 N2/H2.
Dimensional change: Green to as sintered.

349

Iron and steel powders for sintered components


15 minutes
30 minutes
45 minutes

Astaloy A + 0.4% C
MPa

103 psi

Tensile and Yield strength

900

HV10

HRB

Hardness

131

300

750

109

250

85

600

87

200

70

450

65

150

55

44

100

40

22

50

300
Tensile str.

150

100

6.4

6.6

6.8

7.0

7.2

0
7.4

25

HV10
HRB

Yield str

6.4

6.6

6.8

7.0

7.2

7.4

10

106 psi

29.0

60

180

26.1

50

36.7

160

23.2

40

29.3

140

20.3

30

22.0

120

17.4

20

14.7

100

14.5

10

7.3

11.6

GPa

Young's modulus

200

80
6.4

6.6

6.8

7.0

7.2

7.4

6.4

-0.1

-0.2

-0.3

-0.4

-0.5

6.4

6.6

6.8

7.0

Sintered density (g/cm3)

7.2

7.4

-0.6
6.4

6.8

7.0

44.0

7.2

Conventional compaction
Warm compaction

6.6

6.8

7.0

7.2

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube respectively; P: 400 - 800 MPa
conventional and warm compaction, S: 1120C (2050F), various time in 90/10 N2/H2.
Dimensional change: Green to as sintered.

350

7.4

Dimensional change

0.0

6.6

Elongation

Ft lb

Impact energy

7.4

0.0

Astaloy A
0% C
0.4% C
0.8% C

Astaloy A + 1% Cu + C
103 psi

HV10

131

300

750

109

250

85

600

87

200

70

450

65

150

55

300

44

100

40

22

50

MPa

Tensile and Yield strength

900

150
0

Tensile str.
Yield str

6.4

6.6

6.8

7.0

7.2

7.4

HRB

Hardness

100

25

HV10
HRB

6.4

6.6

6.8

7.0

7.2

7.4

10

106 psi

29.0

60

180

26.1

50

36.9

160

23.2

40

29.5

140

20.3

30

22.1

120

17.4

20

14.7

100

14.5

10

7.4

11.6

GPa

Young's modulus

200

80

6.4

6.6

6.8

7.0

7.2

7.4

0.2

0.1

0.0

-0.1

-0.2

6.4

6.6

6.8

7.0

Sintered density (g/cm3)

6.6

7.2

7.4

-0.3

6.8

7.0

44.2

7.2

7.4

7.2

7.4

0.0

Dimensional change

0.3

10

6.4

Elongation

12

Ft lb

Impact energy

Conventional compaction
Warm compaction

6.4

6.6

6.8

7.0

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube respectively; P: 400 - 800 MPa
conventional and warm compaction, S: 1120C (2050F), 30 min in 90/10 N2/H2.
Dimensional change: Green to as sintered.

351

Iron and steel powders for sintered components


0% Cu
1% Cu
2% Cu

Astaloy A + Cu + 0.4% C
103 psi

HV10

131

300

750

109

250

85

600

87

200

70

450

65

150

55

44

100

40

22

50

MPa

Tensile and Yield strength

900

300
Tensile str.

150

HRB

Hardness

100

6.4

6.6

6.8

7.0

7.2

7.4

25

HV10
HRB

Yield str

6.4

6.6

6.8

7.0

7.2

7.4

10

106 psi

29.0

60

180

26.1

50

36.9

160

23.2

40

29.5

140

20.3

30

22.1

120

17.4

20

14.7

100

14.5

10

7.4

11.6
7.4

GPa

Young's modulus

200

80

6.4

6.6

6.8

7.0

7.2

0.8

0.4

0.0

-0.4

-0.8

6.4

6.6

6.8

7.0

Sintered density (g/cm3)

6.6

7.2

7.4

-1.2

6.8

7.0

44.2

7.2

Conventional compaction
Warm compaction

6.4

6.6

6.8

7.0

7.2

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube respectively; P: 400 - 800 MPa
conventional and warm compaction, S: 1120C (2050F), 30 min in 90/10 N2/H2.
Dimensional change: Green to as sintered.

352

7.4

Dimensional change

1.2

6.4

Elongation

Ft lb

Impact energy

7.4

0.0

Astaloy A

Astaloy A + C

Conventional compaction SD=6.9 g/cm3


Warm compaction SD=7.1 g/cm3

103 psi

HV10

131

300

750

109

250

80

600

87

200

70

450

65

150

60

44

100

50

22

50

MPa
900

Tensile and Yield strength

300
Tensile str.

150
0

Yield str

0.0

0.2

0.4

0.6

0.8

HRB

Hardness

90

40

HV10
HRB

0.0

0.2

0.4

0.6

0.8

30

106 psi

29.0

90

180

26.1

75

55.2

160

23.2

60

44.2

140

20.3

45

33.1

120

17.4

30

22.1

100

14.5

15

11.0

11.6
0.8

GPa

Young's modulus

200

80

0.0

0.2

0.4

0.6

0.0

0.1

0.0

-0.1

-0.2

-0.3

0.0

0.2

0.4

Combined carbon (%)

0.6

0.8

-0.4
0.0

0.4

66.3

0.6

0.8

0.6

0.8

0.0

Dimensional change

0.2

10

0.2

Elongation

12

Ft lb

Impact energy

0.2

0.4

Combined carbon (%)

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube respectively; P: 550 - 650 MPa
conventional and warm compaction, S: 1120C (2050F), 30 min in 90/10 N2/H2.
Dimensional change: Green to as sintered.

353

Iron and steel powders for sintered components


0.4% C
0.6% C
0.8% C

Astaloy A + 2% Cu + C (cooling rate 2.5C/s)


Sinter hardening
MPa

103 psi

Tensile and Yield strength

1000

145

Tensile str.

900

HV10

HRC

Hardness

600

45

HV10
HRC

131

500

800

116

400

35

700

102

300

30

600

87

200

25

500

73

100

20

58

400

Yield str

6.4

6.6

6.8

7.2

7.0

7.4

6.4

6.6

40

6.8

7.0

7.2

7.4

15

106 psi

29

30

180

26

25

18.4

160

23

20

14.7

140

20

15

11.1

120

17

10

7.4

100

15

3.7

12

GPa

Young's modulus

200

80

6.4

6.6

6.8

7.0

7.2

7.4

0.5

2.0

0.4

1.5

0.3

1.0

0.2

0.5

0.1

6.4

6.6

6.8

6.6

7.0

7.2

Sintered density (g/cm )


3

7.4

0.0

6.8

7.0

22.1

7.2

7.4

7.2

7.4

0.0

Dimensional change

0.6

2.5

0.0

6.4

Elongation

3.0

Ft lb

Impact energy

6.4

6.6

6.8

7.0

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 2% Cu-30 + 0.8% Amide wax and 0.6% Lube resp. P: 400 - 800 MPa
conventional and warm compaction, S: 1120C (2050F), 30 min in 80/20 N2/H2, convective cooling rate
2.5C/s. Tempering 180C (355F), 60 min in air. Dimensional change: Green to as sintered.

354

Astaloy A
1 C/s
2.5 C/s
5 C/s

Astaloy A + 2% Cu + C (sintered density 7.0 g/cm3)


Sinter hardening
MPa
1000

103 psi

Tensile and Yield strength

HV10

HRC

Hardness

145

450

900

131

400

40

800

116

350

35

700

102

300

30

87

250

25

73

200

600

Tensile str.
Yield str

500
400
0.35

0.45

0.55

0.65

0.75

58
0.85

150
0.35

45

HV10
HRC

0.45

0.55

0.65

0.75

20
15
0.85

106 psi

29.0

30

180

26.1

25

18.4

160

23.2

20

14.7

140

20.3

15

11.1

120

17.4

10

7.4

100

14.5

3.7

GPa

Young's modulus

200

80
0.35

0.45

0.55

0.65

0.75

11.6
0.85

0.5

2.0

0.4

1.5

0.3

1.0

0.2

0.5

0.1

0.45

0.55

0.65

Combined carbon (%)

0.75

0.85

0.0
0.35

0.55

0.65

22.1

0.75

0.0
0.85

0.75

0.85

Dimensional change

0.6

2.5

0.0
0.35

0.45

Elongation

3.0

0
0.35

Ft lb

Impact energy

0.45

0.55

0.65

Combined carbon (%)

MANUFACTURING CONDITIONS: 2% Cu-30 + 0.8% Amide wax, P: 650 - 750 MPa


conventional compaction, S: 1120C (2050F), 30 min in 80/20 N2/H2, various convective cooling
rates. Tempering 180C (355F), 60 min in air. Dimensional change: Green to as sintered.

355

Iron and steel powders for sintered components

Astaloy A + 2% Cu + 0.6% C

1 C/s
2.5 C/s
5 C/s

Sinter hardening
3

10 psi

HV10

160

500

1000

145

450

40

900

131

400

35

800

116

350

30

102

300

25

87

250

MPa

Tensile and Yield strength

1100

700
Tensile str.

600

Yield str

500
6.4

6.6

6.8

7.0

7.2

73
7.4

HRC

Hardness

45

HV10
HRC

200
6.4

6.6

6.8

7.0

7.2

20
15
7.4

Ft lb

10 psi

29.0

30

180

26.1

25

18.4

160

23.2

20

14.7

140

20.3

15

11.1

120

17.4

10

7.4

100

14.5

3.7

11.6
7.4

GPa

Young's modulus

200

80

6.4

6.6

6.8

7.0

7.2

0.5

2.0

0.4

1.5

0.3

1.0

0.2

0.5

0.1

6.4

6.6

6.8

6.6

7.0

7.2

Sintered density (g/cm )


3

7.4

0.0

6.8

7.0

22.1

7.2

7.4

7.2

7.4

Dimensional change

0.6

2.5

0.0

6.4

Elongation

3.0

Impact energy

6.4

6.6

6.8

7.0

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 2%Cu-30 + 0.8% Amide wax and 0.6% Lube resp. P: 400 - 800 MPa
conventional and warm compaction, S: 1120C in 80/20 N2/H2, various convective cooling rates.
Tempering 180C (355F), 60 min in air. Dimensional change: Green to as sintered.

356

0.0

Astaloy B

Astaloy B

357

Iron and steel powders for sintered components

358

Astaloy B
Springback

%
0.4

0.8 % Amide-wax
0.8% Zn-st

0.3

0.6 % Kenolube
0.6% Lube, Warm compaction

0.2

Lubricated tool die

0.1
0.0

400

300

500

g/cm

600

700

800

900

700

800

900

Green density

7.5
7.4
7.3
7.2
7.1
7.0
6.9
6.8
6.7
6.6
6.5
400

300

500

600

Green strength

MPa

psi

30

4350

25

3625

20

2900

15

2175

10

1450

725

0
400

300
25

500

30

35

600
40

45

800

700
50

55

900
60

Compacting pressure (MPa and tsi)

359

Iron and steel powders for sintered components

Astaloy B
Sintered density
g/cm3

g/cm3

Conventional compaction

7.40
7.25

7.25

7.10

7.10

6.95

6.95
0% C

0% C

6.80

6.80

0.4% C

6.65
6.50
350

0.5% C + 2% Cu

450

550

650

7.6

750

850

6.50
350

7.4

7.4

7.3

7.3

550

650

750

7.6

750

0% C
0.4% C
0.8% C

850

7.0
350

450

550

650

750

P2 (MPa)

Double pressing - 0.4% C - P1: 600 MPa


S1: 750C
S1: 800C
S1: 850C

7.5
7.4
7.3
7.2
7.1
7.0
350

450

550

650

750

850

P2 (MPa)

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube respectively; P: 400 - 800 MPa
conventional, double and warm compaction, S: 1120C (2050F), 30 min in 90/10 N2/H2.

360

850

7.1

P2 (MPa)
g/cm3

650

7.2

P1: 400 MPa


P1: 600 MPa
P1: 800 MPa

450

550

7.6
7.5

7.0
350

450

g/cm3 Double pressing - P1: 600 MPa - S1: 800C

7.5

7.1

0.8% C
0.5% C + 2% Cu

Compacting pressure (MPa)

Double pressing - 0.4% C - S1: 800C

7.2

0.4% C

6.65

0.8% C

Compacting pressure (MPa)


g/cm3

Warm Compaction

7.40

850

Astaloy B
15 minutes
30 minutes
45 minutes

Astaloy B + 0.4% C
MPa

103 psi

Tensile and Yield strength

900

HV10

HRB

Hardness

131

300

750

109

250

85

600

87

200

70

450

65

150

55

44

100

40

22

50

300
Tensile str.

150

100

6.5

6.7

6.9

7.1

7.3

7.5

25

HV10
HRB

Yield str

6.5

6.7

6.9

7.1

7.3

7.5

10

106 psi

29.0

60

180

26.1

50

36.7

160

23.2

40

29.3

140

20.3

30

22.0

120

17.4

20

14.7

100

14.5

10

7.3

11.6

GPa

Young's modulus

200

80

6.5

6.7

6.9

7.1

7.3

7.5

6.5

-0.1

-0.2

-0.3

-0.4

-0.5

6.5

6.7

6.9

7.1

Sintered density (g/cm3)

7.3

7.5

-0.6
6.5

6.9

7.1

44.0

7.3

7.5

0.0

Dimensional change

0.0

6.7

Elongation

Ft lb

Impact energy

Conventional compaction
Warm compaction

6.7

6.9

7.1

7.3

7.5

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube respectively; P: 400 - 800 MPa
conventional and warm compaction, S: 1120C (2050F), various time in 90/10 N2/H2.
Dimensional change: Green to as sintered.

361

Iron and steel powders for sintered components

362

Astaloy B
0% C
0.4% C
0.8% C

Astaloy B + 1% Cu + C
103 psi

HV10

131

300

109

250

85

600

87

200

70

450

65

150

55

300

44

100

40

150

22

50

MPa

Tensile and Yield strength

900
750

6.5

Tensile str.
Yield str.

6.7

6.9

7.1

7.3

0
7.5

HRB

Hardness

100

25

HV10
HRB

6.5

6.7

6.9

7.1

7.3

10
7.5

106 psi

29.0

90

180

26.1

75

55.2

160

23.2

60

44.2

140

20.3

45

33.1

120

17.4

30

22.1

100

14.5

15

11.0

11.6
7.5

GPa

Young's modulus

200

80

6.5

6.7

6.9

7.1

7.3

0.2

12

0.1

0.0

-0.1

-0.2

6.5

6.7

6.9

7.1

Sintered density

(g/cm3)

6.7

7.3

7.5

-0.3

6.9

7.1

66.3

7.3

7.5

7.3

7.5

0.0

Dimensional change

0.3

15

6.5

Elongation

18

Ft lb

Impact energy

Conventional compaction
Warm compaction

6.5

6.7

6.9

7.1

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube respectively; P: 400 - 800 MPa
conventional and warm compaction, S: 1120C (2050F), 30 min in 90/10 N2/H2.
Dimensional change: Green to as sintered.

363

Iron and steel powders for sintered components


0% Cu
1% Cu
2% Cu

Astaloy B + Cu + 0.4% C
MPa

103 psi

Tensile and Yield strength

900

HV10

HRB

Hardness

131

300

750

109

250

85

600

87

200

70

450

65

150

55

300

44

100

40

22

50

Tensile str.

150

100

6.5

6.7

6.9

7.1

7.3

0
7.5

25

HV10
HRB

Yield str

6.5

6.7

6.9

7.1

7.3

7.5

10

106 psi

29.0

60

180

26.1

50

36.7

160

23.2

40

29.3

140

20.3

30

22.0

120

17.4

20

14.7

100

14.5

10

7.3

11.6
7.5

GPa

Young's modulus

200

80

6.5

6.7

6.9

7.1

7.3

6.5

0.8

0.4

0.0

-0.4

-0.8

6.5

6.7

6.9

7.1

Sintered density

(g/cm3)

7.3

7.5

-1.2
6.5

6.9

7.1

44.0

7.3

Conventional compaction
Warm compaction

6.7

6.9

7.1

7.3

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube respectively; P: 400 - 800 MPa
conventional and warm compaction, S: 1120C (2050F), 30 min in 90/10 N2/H2.
Dimensional change: Green to as sintered.

364

7.5

Dimensional change

1.2

6.7

Elongation

Ft lb

Impact energy

7.5

0.0

Astaloy B

Astaloy B + C

Conventional compaction SD=7.0 g/cm3


Warm compaction SD=7.1 g/cm3

103 psi

HV10

131

300

750

109

250

80

600

87

200

70

450

65

150

60

44

100

50

22

50

MPa
900

Tensile and Yield strength

300
Tensile str.

150
0

Yield str

0.0

0.2

0.4

0.6

0.8

HRB

Hardness

90

HV10
HRB

0.0

0.2

0.4

0.6

40
30
0.8

106 psi

29.0

90

180

26.1

75

55.2

160

23.2

60

44.2

140

20.3

45

33.1

120

17.4

30

22.1

100

14.5

15

11.0

80

11.6

GPa

Young's modulus

200

0.0

0.2

0.4

0.6

0.8

0.2

0.1

0.0

-0.1

-0.2

0.0

0.2

0.4

Combined carbon (%)

0.2

0.6

0.8

-0.3

0.4

66.3

0.6

0.0
0.8

0.6

0.8

Dimensional change

0.3

10

0.0

Elongation

12

Ft lb

Impact energy

0.0

0.2

0.4

Combined carbon (%)

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube respectively; P: 550 - 650 MPa
conventional and warm compaction, S: 1120C (2050F), 30 min in 90/10 N2/H2.
Dimensional change: Green to as sintered.

365

Iron and steel powders for sintered components


0.3% C
0.5% C
0.7% C

Astaloy B + 2% Cu + C (cooling rate 2.5C/s)


Sinter hardening
103 psi

HV10

145

600

123

500

700

102

400

35

550

80

300

30

400

58

200

25

250

36

100

20

15
7.4

MPa
1000

Tensile str.
Yield str

850

100

Tensile and Yield strength

6.4

6.6

6.8

7.0

7.2

6.4

HRC

Hardness

45

HV10
HRC

6.6

40

6.8

7.0

7.2

15
7.4

106 psi

29.0

30

180

26.1

25

18.4

160

23.2

20

14.7

140

20.3

15

11.1

120

17.4

10

7.4

100

14.5

3.7

80

11.6
7.4

GPa

Young's modulus

200

6.4

6.6

6.8

7.0

7.2

0.5

2.0

0.4

1.5

0.3

1.0

0.2

0.5

0.1

6.4

6.6

6.8

7.0

Sintered density (g/cm3)

6.6

7.2

7.4

0.0

6.8

7.0

22.1

7.2

0.0
7.4

7.2

7.4

Dimensional change

0.6

2.5

0.0

6.4

Elongation

3.0

Ft lb

Impact energy

6.4

6.6

6.8

7.0

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 2% Cu-30 + 0.8% Amide wax and 0.6% Lube resp. P: 400 - 800 MPa
conventional and warm compaction, S: 1120C (2050F), 30 min in 80/20 N2/H2, convective cooling rate
2.5C/s. Tempering 180C (355F), 60 min in air. Dimensional change: Green to as sintered.

366

Astaloy B
1 C/s
2.5 C/s
5 C/s

Astaloy B + 2% Cu + C (sintered density 7.0 g/cm3)


Sinter hardening
MPa
1000

Tensile and Yield strength


Tensile str.

103 psi

HV10

145

450

HRC

Hardness

45

HV10
HRC

40

131

400

800

116

350

35

700

102

300

30

600

87

250

25

500

73

200

20

900

400
0.25

Yield str

0.35

0.45

0.55

0.65

58
0.75

150
0.25

0.35

0.45

0.55

0.65

15
0.75

106 psi

29.0

30

180

26.1

25

18.4

160

23.2

20

14.7

140

20.3

15

11.1

120

17.4

10

7.4

100

14.5

3.7

GPa

Young's modulus

200

80
0.25

0.35

0.45

0.55

0.65

11.6
0.75

0.5

2.0

0.4

1.5

0.3

1.0

0.2

0.5

0.1

0.35

0.45

0.55

Combined carbon (%)

0.65

0.75

0.0
0.25

0.45

0.55

22.1

0.65

0.0
0.75

0.65

0.75

Dimensional change

0.6

2.5

0.0
0.25

0.35

Elongation

3.0

0
0.25

Ft lb

Impact energy

0.35

0.45

0.55

Combined carbon (%)

MANUFACTURING CONDITIONS: 2% Cu-30 + 0.8% Amide wax, P: 600 - 700 MPa


conventional compaction, S: 1120C (2050F), 30 min in 80/20 N2/H2, various convective cooling
rates. Tempering 180C (355F), 60 min in air. Dimensional change: Green to as sintered.

367

Iron and steel powders for sintered components

368

Astaloy CrL

Astaloy CrL

369

Iron and steel powders for sintered components

370

Astaloy CrL
Springback

%
0.4

0.8 % Amide-wax
0.8% Zn-st

0.3

0.6 % Kenolube
0.6% Lube, Warm compaction

0.2

Lubricated tool die

0.1
0.0

600

500

400

300

g/cm3

700

800

900

700

800

900

Green density

7.5
7.4
7.3
7.2
7.1
7.0
6.9
6.8
6.7
6.6
6.5
300

600

500

400

Green strength

MPa

psi

60

8700

50

7250

40

5800

30

4350

20

2900

10

1450
0

25

600

500

400

300

30

35

40

45

700
50

900

800
55

60

Compacting pressure (MPa and tsi)

371

Iron and steel powders for sintered components


0% C
0.4% C
0.8% C

Astaloy CrL + C
MPa
1000

103 psi

Tensile and Yield strength

HV10

HRB

Hardness

145

300

123

250

700

102

200

70

550

80

150

55

400

58

100

40

250

36

50

25

15

Tensile str.
Yield str

850

100

6.4

6.6

6.8

7.0

7.2

7.4

100

HV10
HRB

6.4

6.6

85

6.8

7.0

7.2

7.4

10

106 psi

29.0

60

180

26.1

50

36.9

160

23.2

40

29.5

140

20.3

30

22.1

120

17.4

20

14.7

100

14.5

10

7.4

80

11.6

GPa

Young's modulus

200

6.4

6.6

6.8

7.0

7.2

7.4

6.4

0.0

-0.1

-0.2

-0.3

-0.4

6.4

6.6

6.8

7.0

Sintered density (g/cm3)

7.2

7.4

-0.5
6.4

6.8

7.0

44.2

7.2

Conventional compaction
Warm compaction

6.6

6.8

7.0

7.2

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube respectively; P: 400 - 800 MPa
conventional and warm compaction, S: 1120C (2050F), 30 min in 90/10 N2/H2.
Dimensional change: Green to as sintered.

372

7.4

Dimensional change

0.1

10

6.6

Elongation

12

Ft lb

Impact energy

7.4

0.0

Astaloy CrL
15 minutes
30 minutes
45 minutes

Astaloy CrL + 0.5% C


MPa

103 psi

Tensile and Yield strength

1000

HV10

HRB

Hardness

145

400

850

123

350

90

700

102

300

80

550

80

250

70

58

200

60

36

150

15

100

400
Tensile str.

250
100

Yield str

6.4

6.6

6.8

7.0

7.2

7.4

100

50

HV10
HRB

6.4

6.6

6.8

7.0

7.2

7.4

40

106 psi

29.0

60

180

26.1

50

36.7

160

23.2

40

29.3

140

20.3

30

22.0

120

17.4

20

14.7

100

14.5

10

7.3

80

11.6
7.4

GPa

Young's modulus

200

6.4

6.6

6.8

7.0

7.2

6.4

0.0

-0.1

-0.2

-0.3

-0.4

6.4

6.6

6.8

7.0

Sintered density (g/cm3)

7.2

7.4

-0.5
6.4

6.8

7.0

44.0

7.2

7.4

0.0

Dimensional change

0.1

6.6

Elongation

Ft lb

Impact energy

Conventional compaction
Warm compaction

6.6

6.8

7.0

7.2

7.4

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube respectively; P: 400 - 800 MPa
conventional and warm compaction, S: 1120C (2050F), various time in 90/10 N2/H2.
Dimensional change: Green to as sintered.

373

Iron and steel powders for sintered components

Astaloy CrL + C

6.90 g/cm3 (conventional compaction)


7.15 g/cm3 (warm compaction)

103 psi

HV10

145

400

850

123

350

90

700

102

300

80

550

80

250

70

58

200

60

36

150

15

100
0.0

MPa
1000

Tensile and Yield strength

400
Tensile str.

250

HRB

Hardness

100

100

0.0

0.2

0.4

0.6

0.8

50

HV10
HRB

Yield str

0.2

0.4

0.6

40
0.8

106 psi

29.0

60

180

26.1

50

36.9

160

23.2

40

29.5

140

20.3

30

22.1

120

17.4

20

14.7

100

14.5

10

7.4

11.6

GPa

Young's modulus

200

80

0.0

0.2

0.4

0.6

0.8

0.0

-0.1

-0.2

-0.3

-0.4

0.0

0.2

0.4

Combined carbon (%)

0.2

0.6

0.8

-0.5

0.4

44.2

0.6

0.0
0.8

0.6

0.8

Dimensional change

0.1

10

0.0

Elongation

12

Ft lb

Impact energy

0.0

0.2

0.4

Combined carbon (%)

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube respectively; P: 550 - 650 MPa
conventional and warm compaction, S: 1120C (2050F), 30 min in 90/10 N2/H2.
Dimensional change: Green to as sintered.

374

Astaloy CrL
0.4% C
0.6% C
0.8% C

Astaloy CrL + C (cooling rate 2.5C/s)


High temperature sintering
103 psi

HV10

232

600

203

500

1200

174

400

35

1000

145

300

30

800

116

200

25

600

87

100

20

58
7.5

MPa
1600
1400

400
6.5

Tensile and Yield strength


Tensile str.
Yield str

6.7

6.9

7.1

7.3

6.5

HRC

Hardness

45

HV10
HRC

6.7

40

6.9

7.1

7.3

15
7.5

106 psi

29.0

60

180

26.1

50

36.9

160

23.2

40

29.5

140

20.3

30

22.1

120

17.4

20

14.7

100

14.5

10

7.4

11.6
7.5

GPa

Young's modulus

200

80

6.5

6.7

6.9

7.1

7.3

6.5

-0.2

-0.4

-0.6

-0.8

-1.0

6.5

6.7

6.9

7.1

Sintered density (g/cm3)

7.3

7.5

-1.2
6.5

6.9

7.1

44.2

7.3

0.0
7.5

7.3

7.5

Dimensional change

0.0

6.7

Elongation

Ft lb

Impact energy

6.7

6.9

7.1

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube resp. P: 400 - 800 MPa conventional
and warm compaction, S: 1250C (2282F), 30 min in 90/10 N2/H2, convective cooling rate 2.5C/s.
Tempering 180C (355F), 60 min in air. Dimensional change: Green to as sintered.

375

Iron and steel powders for sintered components


1 C/s
2.5 C/s
5 C/s

Astaloy CrL + C (sintered density 7.0 g/cm3)


High temperature sintering
MPa

Tensile and Yield strength

1200

103 psi

HV10

203

600

Tensile str.

1050

HRC

Hardness

60

HV10
HRC

176

500

900

150

400

40

750

123

300

30

600

97

200

20

450

70

100

10

300

44
1.0

Yield str

0.0

0.2

0.4

0.6

0.8

0.0

0.2

50

0.4

0.6

0.8

0
1.0

106 psi

29.0

60

180

26.1

50

36.9

160

23.2

40

29.5

140

20.3

30

22.1

120

17.4

20

14.7

100

14.5

10

7.4

11.6
1.0

GPa

Young's modulus

200

80

0.0

0.2

0.4

0.6

0.8

-0.2

-0.4

-0.6

-0.8

-1.0

0.0

0.2

0.4

0.6

Combined carbon (%)

0.2

0.8

1.0

-1.2

0.4

0.6

44.2

0.8

0.0
1.0

0.8

1.0

Dimensional change

0.0

0.0

Elongation

%
6

Ft lb

Impact energy

0.0

0.2

0.4

0.6

Combined carbon (%)

MANUFACTURING CONDITIONS: 0.8% Amide wax, P: 500 - 600 MPa conventional compaction,
S: 1250C (2282F), 30 min in 90/10 N2/H2, various convective cooling rates.
Tempering 180C (355F), 60 min in air. Dimensional change: Green to as sintered.

376

Astaloy CrL


3)

3)

377

Iron and steel powders for sintered components


0.4% C
0.6% C
0.8% C

Astaloy CrL + 2% Cu + C (cooling rate 2.5C/s)


Sinter hardening
MPa

Tensile and Yield strength

1100

103 psi

HV10

160

600

HRC

Hardness

50

HV10
HRC

45

145

500

131

400

40

800

116

300

35

700

102

200

30

600

87

100

25

73

1000

Tensile str.
Yield str

900

500

6.4

6.6

6.8

7.0

7.2

7.4

6.4

6.6

6.8

7.0

7.2

20
7.4

106 psi

29.0

30

180

26.1

25

18.4

160

23.2

20

14.7

140

20.3

15

11.1

120

17.4

10

7.4

100

14.5

3.7

11.6
7.4

GPa

Young's modulus

200

80

6.4

6.6

6.8

7.0

7.2

0.5

2.0

0.4

1.5

0.3

1.0

0.2

0.5

0.1

6.4

6.6

6.8

7.0

Sintered density (g/cm3)

6.6

7.2

7.4

0.0

6.8

7.0

22.1

7.2

0.0
7.4

7.2

7.4

Dimensional change

0.6

2.5

0.0

6.4

Elongation

3.0

Ft lb

Impact energy

6.4

6.6

6.8

7.0

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 2% Cu -30 + 0.8% Amide wax and 0.6% Lube resp. P: 400 - 800 MPa
conventional and warm compaction, S: 1120C (2050F), 30 min in 80/20 N2/H2, convective cooling rate
2.5C/s. Tempering 180C (355F), 60 min in air. Dimensional change: Green to as sintered.

378

Astaloy CrL
1 C/s
2.5 C/s
5 C/s

Astaloy CrL + 2% Cu + C (sintered density 7.0 g/cm3)


Sinter hardening
MPa

103 psi

Tensile and Yield strength

HV10

HRC

Hardness

50

160

450

1000

145

400

45

900

131

350

40

800

116

300

35

102

250

30

87

200

1100

700
Tensile str.

600
500
0.35

Yield str

0.45

0.55

0.65

0.75

73
0.85

150
0.35

HV10
HRC

0.45

0.55

0.65

0.75

25
20
0.85

106 psi

29.0

30

180

26.1

25

18.4

160

23.2

20

14.7

140

20.3

15

11.1

120

17.4

10

7.4

100

14.5

3.7

GPa

Young's modulus

200

80
0.35

0.45

0.55

0.65

0.75

11.6
0.85

0.5

2.0

0.4

1.5

0.3

1.0

0.2

0.5

0.1

0.45

0.55

0.65

Combined carbon (%)

0.75

0.85

0.0
0.35

0.55

0.65

22.1

0.75

0.0
0.85

0.75

0.85

Dimensional change

0.6

2.5

0.0
0.35

0.45

Elongation

3.0

0
0.35

Ft lb

Impact energy

0.45

0.55

0.65

Combined carbon (%)

MANUFACTURING CONDITIONS: 2% Cu -30 + 0.8% Amide wax, P: 600 - 700 MPa


conventional compaction, S: 1120C (2050F), 30 min in 80/20 N2/H2, various convective cooling
rates. Tempering 180C (355F), 60 min in air. Dimensional change: Green to as sintered.

379

Iron and steel powders for sintered components


1 C/s
2.5 C/s
5 C/s

Astaloy CrL + 2% Cu + 0.6% C


Sinter hardening
103 psi

HV10

174

500

160

450

45

145

400

40

900

131

350

35

800

116

300

30

700

102

250

87

200
6.4

MPa

Tensile and Yield strength

1200
1100

Tensile str.
Yield str

1000

600

6.4

6.6

6.8

7.0

7.2

7.4

HRC

Hardness

50

25

HV10
HRC

6.6

6.8

7.0

7.2

20
7.4

106 psi

29.0

30

180

26.1

25

18.4

160

23.2

20

14.7

140

20.3

15

11.1

120

17.4

10

7.4

100

14.5

3.7

11.6
7.4

GPa

Young's modulus

200

80

6.4

6.6

6.8

7.0

7.2

0.5

2.0

0.4

1.5

0.3

1.0

0.2

0.5

0.1

6.4

6.6

6.8

7.0

Sintered density (g/cm3)

6.6

7.2

7.4

0.0

6.8

7.0

22.1

7.2

0.0
7.4

7.2

7.4

Dimensional change

0.6

2.5

0.0

6.4

Elongation

3.0

Ft lb

Impact energy

6.4

6.6

6.8

7.0

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 2% Cu - 30 + 0.8% Amide wax and 0.6% Lube resp. P: 400 - 800 MPa
conventional and warm compaction, S: 1120C (2050F), 30 min in 80/20 N2/H2, various convective cooling
rates. Tempering 180C (355F), 60 min in air. Dimensional change: Green to as sintered.

380

Astaloy CrM

Astaloy CrM

381

Iron and steel powders for sintered components

382

Astaloy CrM
Springback

%
0.4

0.8 % Amide-wax
0.8% Zn-st

0.3

0.6 % Kenolube
0.6% Lube + 0.35% Graphite, Warm compaction

0.2

Lubricated tool die

0.1
0.0

300

600

500

400

g/cm3

700

800

900

700

800

900

Green density

7.4
7.3
7.2
7.1
7.0
6.9
6.8
6.7
6.6
6.5
6.4
300

500

400

600

Green strength

MPa

psi

60

8700

50

7250

40

5800

30

4350

20

2900

10

1450
0

0
300
25

600

500

400
30

35

40

45

700
50

900

800
55

60

Compacting pressure (MPa and tsi)

383

Iron and steel powders for sintered components


0.2 % C
0.4% C
0.6% C

Astaloy CrM + C
MPa

103 psi

Tensile and Yield strength

1500

HV10

HRC

Hardness

218

600

181

500

1000

145

400

40

750

109

300

30

500

73

200

20

250

36

100

10

Tensile str.

1250

Yield str

6.4

6.6

6.8

7.0

7.2

7.4

60

HV10
HRC

6.4

6.6

50

6.8

7.0

7.2

7.4

106 psi

29.0

60

180

26.1

50

36.9

160

23.2

40

29.5

140

20.3

30

22.1

120

17.4

20

14.7

100

14.5

10

7.4

80

11.6

GPa

Young's modulus

200

6.4

6.6

6.8

7.0

7.2

7.4

6.4

-0.1

2.0

-0.2

1.5

-0.3

1.0

-0.4

0.5

-0.5

6.4

6.6

6.8

7.0

Sintered density (g/cm3)

7.2

7.4

-0.6
6.4

6.8

7.0

44.2

7.2

Conventional compaction
Warm compaction

6.6

6.8

7.0

7.2

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube respectively; P: 400 - 800 MPa
conventional and warm compaction, S: 1120C (2050F), 30 min in 90/10 N2/H2.
Dimensional change: Green to as sintered.

384

7.4

Dimensional change

0.0

2.5

0.0

6.6

Elongation

3.0

Ft lb

Impact energy

7.4

0.0

Astaloy CrM
1090C (1995F)
1120C (2050F)
1150C (2100F)

Astaloy CrM + 0.4% C


103 psi

HV10

218

400

1250

181

350

50

1000

145

300

40

750

109

250

30

73

200

20

36

150

MPa

Tensile and Yield strength

1500

500
Tensile str.

250
0

Yield str

6.4

6.6

6.8

7.0

7.2

0
7.4

100
6.4

HRC

Hardness

60

10

HV10
HRC

6.6

6.8

7.0

7.2

7.4

106 psi

29.0

60

180

26.1

50

36.9

160

23.2

40

29.5

140

20.3

30

22.1

120

17.4

20

14.7

100

14.5

10

7.4

GPa

Young's modulus

200

80

6.4

6.6

6.8

7.0

7.2

11.6
7.4

0
6.4

-0.1

2.0

-0.2

1.5

-0.3

1.0

-0.4

0.5

-0.5

6.4

6.6

6.8

7.0

Sintered density (g/cm3)

7.2

7.4

-0.6

6.8

7.0

44.2

7.2

7.4

0.0

Dimensional change

0.0

2.5

0.0

6.6

Elongation

3.0

Ft lb

Impact energy

Conventional compaction
Warm compaction

6.4

6.6

6.8

7.0

7.2

7.4

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube respectively; P: 400 - 800 MPa
conventional and warm compaction, S: Various temperatures, 30 min in 90/10 N2/H2.
Dimensional change: Green to as sintered.

385

Iron and steel powders for sintered components


15 minutes
30 minutes
45 minutes

Astaloy CrM + 0.4% C


103 psi

HV10

218

400

1250

181

350

50

1000

145

300

40

750

109

250

30

73

200

20

36

150

MPa

Tensile and Yield strength

1500

500
Tensile str.

250

HRC

Hardness

60

6.4

6.6

6.8

7.0

7.2

0
7.4

100
6.4

10

HV10
HRC

Yield str

6.6

6.8

7.0

7.2

7.4

106 psi

29.0

60

180

26.1

50

36.9

160

23.2

40

29.5

140

20.3

30

22.1

120

17.4

20

14.7

100

14.5

10

7.4

11.6
7.4

GPa

Young's modulus

200

80

6.4

6.6

6.8

7.0

7.2

-0.1

2.0

-0.2

1.5

-0.3

1.0

-0.4

0.5

-0.5

6.4

6.6

6.8

7.0

Sintered density (g/cm3)

6.6

7.2

7.4

-0.6

6.8

7.0

44.2

7.2

Conventional compaction
Warm compaction

6.4

6.6

6.8

7.0

7.2

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube respectively; P: 400 - 800 MPa
conventional and warm compaction, S: 1120C (2050F), various time in 90/10 N2/H2.
Dimensional change: Green to as sintered.

386

7.4

Dimensional change

0.0

2.5

0.0

6.4

Elongation

3.0

Ft lb

Impact energy

7.4

0.0

Astaloy CrM

Astaloy CrM + C
MPa
1500

Conventional compaction SD=6.9 g/cm3


Warm compaction SD=7.1 g/cm3

Tensile and Yield strength

103 psi

HV10

HRC

Hardness

218

600

181

500

50

1000

145

400

40

750

109

300

30

500

73

200

20

250

36

100

1250

0.0

Tensile str.
Yield str

0.2

0.4

0.6

0
0.8

60

10

HV10
HRC

0.0

0.2

0.4

0.6

0.8

106 psi

29.0

60

180

26.1

50

36.8

160

23.2

40

29.5

140

20.3

30

22.1

120

17.4

20

14.7

100

14.5

10

7.4

80

11.6
0.8

GPa

Young's modulus

200

0.0

0.2

0.4

0.6

0.0

-0.1

2.0

-0.2

1.5

-0.3

1.0

-0.4

0.5

-0.5

0.0

0.2

0.4

Combined carbon (%)

0.6

0.8

-0.6
0.0

0.4

44.2

0.6

0.8

0.6

0.8

0.0

Dimensional change

0.0

2.5

0.0

0.2

Elongation

3.0

Ft lb

Impact energy

0.2

0.4

Combined carbon (%)

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube respectively; P: 550 - 650 MPa
conventional and warm compaction, S: 1120C (2050F), 30 min in 90/10 N2/H2.
Dimensional change: Green to as sintered.

387

Iron and steel powders for sintered components


0.3% C
0.4% C
0.5% C

Astaloy CrM + C (cooling rate 2.5C/s)


High temperature sintering
103 psi

HV10

232

600

203

500

1200

174

400

40

1000

145

300

35

800

116

200

30

600

87

100

25

58

MPa

Tensile and Yield strength

1600

Tensile str.
Yield str

1400

400

6.5

6.7

6.9

7.1

7.3

7.5

6.5

HRC

Hardness

50

HV10
HRC

6.7

45

6.9

7.1

7.3

20
7.5

106 psi

29.0

60

180

26.1

50

36.9

160

23.2

40

29.5

140

20.3

30

22.1

120

17.4

20

14.7

100

14.5

10

7.4

11.6
7.5

GPa

Young's modulus

200

80

6.5

6.7

6.9

7.1

7.3

-0.2

-0.4

-0.6

-0.8

-1.0

6.5

6.7

6.9

7.1

Sintered density (g/cm3)

6.7

7.3

7.5

-1.2

6.9

7.1

44.2

7.3

0.0
7.5

7.3

7.5

Dimensional change

0.0

6.5

Elongation

Ft lb

Impact energy

6.5

6.7

6.9

7.1

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube resp. P: 400 - 800 MPa conventional
and warm compaction, S: 1250C (2282F), 30 min in 90/10 N2/H2, convective cooling rate 2.5 C/s.
Tempering 180C (355F), 60 min in air. Dimensional change: Green to as sintered.

388

Astaloy CrM
1 C/s
2.5 C/s
5 C/s

Astaloy CrM + C (sintered density 7.0 g/cm3)


High temperature sintering
MPa
1300

Tensile and Yield strength

103 psi

HV10

203

500

Tensile str.

HRC

Hardness

50

HV10
HRC

45

176

450

1100

150

400

40

1000

123

350

35

900

97

300

30

800

70

250

25

1200

700
0.15

Yield str

0.25

0.35

0.45

0.55

44
0.65

200
0.15

0.25

0.35

0.45

0.55

20
0.65

106 psi

29.0

60

180

26.1

50

36.9

160

23.2

40

29.5

140

20.3

30

22.1

120

17.4

20

14.7

100

14.5

10

7.4

GPa

Young's modulus

200

80
0.15

0.25

0.35

0.45

0.55

0
0.15

11.6
0.65

0.0

-0.2

-0.4

-0.6

-0.8

-1.0

0
0.15

0.25

0.35

0.45

Combined carbon (%)

0.25

Elongation

0.55

0.65

-1.2
0.15

Ft lb

Impact energy

0.35

0.45

44.2

0.55

0.0
0.65

0.55

0.65

Dimensional change

0.25

0.35

0.45

Combined carbon (%)

MANUFACTURING CONDITIONS: 0.8% Amide wax, P: 550 - 650 MPa conventional compaction,
S: 1250C (2282F), 30 min in 90/10 N2/H2, various convective cooling rates.
Tempering 180C (355F), 60 min in air. Dimensional change: Green to as sintered.

389

Iron and steel powders for sintered components


1 C/s
2.5 C/s
5 C/s

Astaloy CrM + 0.4% C


High temperature sintering
MPa
1600

103 psi

Tensile and Yield strength

232

HV10

HRC

Hardness

550

45

HV10
HRC

40

1400

203

500

1200

174

450

35

1000

145

400

30

116

350

25

87

300

20

58

250

800
Tensile str.

600
400
6.5

Yield str

6.7

6.9

7.1

7.3

7.5

6.5

6.7

6.9

7.1

7.3

15
7.5

106 psi

29.0

60

180

26.1

50

36.9

160

23.2

40

29.5

140

20.3

30

22.1

120

17.4

20

14.7

100

14.5

10

7.4

11.6
7.5

GPa

Young's modulus

200

80

6.5

6.7

6.9

7.1

7.3

-0.2

2.0

-0.4

1.5

-0.6

1.0

-0.8

0.5

-1.0

6.5

6.7

6.9

7.1

Sintered density (g/cm3)

6.7

7.3

7.5

-1.2

6.9

7.1

44.2

7.3

0.0
7.5

7.3

7.5

Dimensional change

0.0

2.5

0.0

6.5

Elongation

3.0

Ft lb

Impact energy

6.5

6.7

6.9

7.1

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube resp. P: 400 - 800 MPa conventional
and warm compaction, S: 1250C (2282F), 30 min in 90/10 N2/H2, various convective cooling rates.
Tempering 180C (355F), 60 min in air. Dimensional change: Green to as sintered.

390

Astaloy CrM
0.3% C
0.4% C
0.5% C

Astaloy CrM + C (cooling rate 2.5C/s)


Sinter hardening
MPa
1500

Tensile and Yield strength

103 psi

HV10

218

600

Tensile str.
Yield str

1300

HRC

Hardness

45

HV10
HRC

189

500

1100

160

400

35

900

131

300

30

700

102

200

25

500

73

100

20

44

300

6.4

6.6

6.8

7.0

7.2

7.4

6.4

6.6

40

6.8

7.0

7.2

15
7.4

106 psi

29.0

30

180

26.1

25

18.4

160

23.2

20

14.7

140

20.3

15

11.1

120

17.4

10

7.4

100

14.5

3.7

11.6
7.4

Young's modulus

GPa
200

80

6.4

6.6

%
3.0

6.8

7.0

7.2

2.5

0.2

2.0

0.1

1.5

0.0

1.0

-0.1

0.5

-0.2

0.0

6.4

6.6

6.8

7.0

Sintered density (g/cm3)

6.4

6.6

%
0.3

Elongation

7.2

7.4

-0.3

Ft lb

Impact energy

6.8

7.0

22.1

7.2

0.0
7.4

7.2

7.4

Dimensional change

6.4

6.6

6.8

7.0

Sintered density (g/cm3)

MANUFACTURING CONDITIONS: 0.8% Amide wax and 0.6% Lube resp. P: 400 - 800 MPa
conventional and warm compaction, S: 1120C (2050F), 30 min in 80/20 N2/H2, convective cooling rate
2.5C/s. Tempering 180C (355F), 60 min in air. Dimensional change: Green to as sintered.

391

Iron and steel powders for sintered components

MANUFACTURING CONDITIONS: 0.8% Amide wax, P: 600 - 700 MPa conventional compaction,
S: 1120C (2050F), 30 min in 80/20 N2/H2, various convective cooling rates.
Tempering 180C (355F), 60 min in air. Dimensional change: Green to as sintered.

392

Astaloy CrM

393

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