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pores can comprise an appreciable component of trapped fluid in mature, organic-rich rocks.2 Destructive bulk analysis
of trapped organic and inorganic fluids
is accomplished via the Fluid Inclusion
Stratigraphy (FIS) technique.3 Samples
are crushed in a vacuum system, and
liberated fluids are analyzed via direct
quadrapole mass spectrometry for C1C13 petroleum species, and inorganic
volatiles (e.g., CO2, H2S, He). Mass spectra and depth profiles of critical species
Fig. 1. Static image from an interactive software program that allows mud gas
compositions, rock and fluid chemical data, electric logs and rock images to be viewed
and manipulated.
Fig. 2. Selected XRF and FIS data from a horizontal well within Cardium sandstone. Data
document a sweet spot which was found to have highest initial production.
164april 2013/WorldOil.com
Fig. 3. FIS, XRF and image data from a vertical well illustrating three zones.
EXAMPLES
Si
Al
FIS
Fe
Ca
Sr
CO2
C1
C4
C7
Zone 1
2,000
3,000
4,000
5,000
6,000
7,000
8,000
0
60,000
120,000
180,000
240,000
0
8,000
16,000
24,000
32,000
0
8,000
16,000
24,000
32,000
0
25,000
50,000
75,000
100,000
0
2,000
4,000
6,000
8,000
0
90,000
180,000
270,000
360,000
0
150
300
450
600
0
262,5000
525,0000
7875,000
10,500,000
0
500,000
1,000,000
1,500,000
2,000,000
0
30,000
60,000
90,000
120,000
0
1,250
2,500
3,750
5,000
9,000
Si
b)
Al
Fe
Ca
Sr
XRF
Si
Al
Fe
Ca
Sr
CO2
CO2
CH4
Parafins 57 AlkNaphtha
FIS
C1
C4
C7
2,000
3,000
4,000
5,000
6,000
Zone 2
7,000
8,000
0
60,000
120,000
180,000
240,000
0
8,000
16,000
24,000
32,000
0
8,000
16,000
24,000
32,000
0
25,000
50,000
75,000
100,000
0
2,000
4,000
6,000
8,000
0
90,000
180,000
270,000
360,000
0
150
300
450
600
0
262,5000
525,0000
7875,000
10,500,000
0
500,000
1,000,000
1,500,000
2,000,000
0
30,000
60,000
90,000
120,000
0
1,250
2,500
3,750
5,000
9,000
Si
c)
Al
Fe
Ca
Sr
XRF
Si
Al
Fe
Ca
Sr
CO2
CH4
CO2
C1
Parafins 57 AlkNaphtha
FIS
C4
C7
2,000
3,000
4,000
5,000
6,000
7,000
8,000
Zone 3
9,000
0
60,000
120,000
180,000
240,000
0
8,000
16,000
24,000
32,000
0
8,000
16,000
24,000
32,000
0
25,000
50,000
75,000
100,000
0
2,000
4,000
6,000
8,000
0
90,000
180,000
270,000
360,000
0
150
300
450
600
0
262,5000
525,0000
7875,000
10,500,000
0
500,000
1,000,000
1,500,000
2,000,000
0
30,000
60,000
90,000
120,000
0
1,250
2,500
3,750
5,000
XRF
a)
Si
Al
Fe
Ca
Sr
CO2
CH4
Parafins 57 AlkNaphtha
Fig. 4. Correlation of elemental sulfur response with gamma ray response suggests
variation in source potential, and correlates with visual organic matter in images and
thin section.
5,750
100
200
Gamma
400 500
300
Source rock
6,250
600
700
5,750
Sulfur
2,000 4,000 6,000 8,000 10,000 12,000 14,000 16,000
500
Bio
400
6,250
ge
nic
300
6,750
7,250
7,750
-Z
l Si
ria
100
t
res
Ter
0
7,750
8,250
8,250
8,750
8,750
9,250
9,250
-100
100
200
Zr
300
400
500
166april 2013/WorldOil.com
FIT_UmbrellaThird.indd 1
end
r tr
200
7,250
Mature oil-prone
organic matter
ca
SI, 10A 3
6,750
sili
3/11/13 10:45 PM
Printed in U.S.A.
Not to be distributed in electronic or printed form, or posted on a website, without express written permission of copyright holder.