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Textiles and Light Industrial Science and Technology (TLIST) Volume 2 Issue 2, April 2013
Introduction
Textiles, especially those made of natural fibers, are an
excellent medium for the growth of microorganisms
when the basic requirements for their growth such as
nutrients, moisture, oxygen, and appropriate
temperature are present. The large surface area and
ability to retain moisture of textiles also assist the
growth of microorganisms on the fabric (Su et al., 2011)
which intern results in inflicting a range of unwanted
effects not only on the textile itself but also on the
wearer. These effects include the generation of
unpleasant odor, stains, discoloration in the fabric, a
reduction in the tensile strength of the fabric and an
78
Textiles and Light Industrial Science and Technology (TLIST) Volume 2 Issue 2, April 2013
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79
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Textiles and Light Industrial Science and Technology (TLIST) Volume 2 Issue 2, April 2013
Washing Fastness
Evaluation of colour fastness to washing was carried
out using ISO II methods (Trotmann, 1984). A solution
containing 5 g/L soap solution was used as the
washing liquor. The samples were treated for 45 min
at 500C using liquor to material ratio of 50:1 in rota
machine. After rinsing and drying, the change in
colour of the sample and staining on the undyed fabric
samples were evaluated on the respective standard
scales (rating 15, where 1 poor, 2 fair, 3 good, 4
very good and 5 excellent).
Rubbing Fastness
Evaluation of colour fastness to rubbing (dry and wet)
was carried out using crock-meter with 10 strokes of
rubbing.
Light Fastness
Dyed fabric was tested for colour fastness to light
according to ISO 105/B02 (ISO technical manual, 2006).
The light fastness was estimated using artificial
illumination with Xenon which is a light source, QSun Xenon Testing Chamber at black standard
temperature 65 0C with relative humidity of the air in
the testing chamber as 40% and daylight filter,
wavelength, k= 420 nm. The samples were compared
with the standard scale of blue wool reading (ratings,
18, where 1 poor, 2 fair, 3 moderate, 4 good, 5
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Textiles and Light Industrial Science and Technology (TLIST) Volume 2 Issue 2, April 2013
Dye Conc.
(%)
K/S
L*
a*
b*
2.8686
3.7455
4.0097
4.2397
66.085
65.77
62.028
60.888
1.844
1.433
3.439
3.566
22.632
21.748
23.052
22.208
10
15
20
Marigold
(%)
5
10
15
20
5
10
15
20
5
10
15
20
5
10
15
20
K/S
L*
a*
b*
5.5228
10.0529
11.8729
13.4266
6.4807
10.2255
10.9399
14.2789
6.9268
10.577
14.641
17.8174
7.3248
12.2046
13.2829
17.9598
66.503
66.442
67.955
60.742
54.323
57.923
60.551
68.874
66.975
58.389
61.319
58.786
53.109
57.255
58.661
58.955
4.355
2.726
2.494
4.682
7.55
6.135
5.577
2.044
4.445
4.69
4.491
4.622
3.367
5.261
5.324
4.931
40.756
38.444
40.142
43.456
39.602
43.042
43.867
39.643
40.6
40.499
43.981
43.592
33.784
41.354
43.309
43.635
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Marigold
(%)
5
10
K/S
L*
a*
b*
3.8059
59.989
3.815
22.823
3.9802
60.794
3.348
22.195
15
4.6245
66.897
1.721
22.338
20
5.2931
68.401
1.277
22.828
10
4.1157
58.313
2.647
18.26
10
10
5.4387
58.423
3.833
24.827
10
15
5.5844
56.737
3.789
23.531
10
20
6.1405
57.532
3.771
23.359
15
5.0177
56.43
4.14
23.707
15
10
5.7317
65.096
3.067
24.264
15
15
15
20
5.7487
6.5905
56.074
59.177
3.747
3.575
23.257
24.976
20
5.1231
54.98
4.213
22.963
20
10
5.6716
58.058
4.134
24.591
20
15
5.8756
59.135
3.528
24.259
20
20
7.5429
64.339
2.523
23.862
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Textiles and Light Industrial Science and Technology (TLIST) Volume 2 Issue 2, April 2013
Marigold (%)
K/S
L*
a*
b*
3.1716
57.521
5.263
19.836
10
3.3931
56.043
6.303
18.757
15
3.7691
59.234
4.967
20.474
20
5.2415
52.322
3.279
13.519
10
3.5341
55.684
6.42
18.19
10
10
3.7573
57.479
6.211
19.698
10
15
3.9831
55.447
7.731
19.901
10
20
5.2722
57.642
6.808
20.923
15
3.6433
53.455
7.366
18.365
15
10
3.879
55.522
7.19
19.941
15
15
4.7567
60.272
5.984
21.011
15
20
5.3063
53.636
7.732
21.596
20
5.2149
59.647
7.065
22.212
20
10
5.2149
55.183
7.825
22.603
20
15
5.3063
58.16
7.06
21.309
20
20
6.0307
62.653
5.363
22.324
Marigold
20
Washing
2
Rubbing
3-4
Light
2
21.258
15
20
4-5
4-5
3.176
20.012
20
20
4-5
4-5
3.666
19.474
61.026
54.517
3.315
4.456
19.092
21.355
15
20
20
20
4-5
5.9055
53.447
4.116
20.306
15
20
4-5
4-5
4.2504
50.999
5.307
19.553
10
4.5406
53.81
4.309
20.984
20
20
4-5
15
15
5.6058
51.26
4.162
18.839
15
20
4-5
15
20
6.3601
53.206
4.362
20.44
20
20
4-5
20
4.5298
50.599
4.829
19.08
20
10
5.9158
52.435
4.814
20.199
20
15
6.401
54.839
4.348
21.749
20
20
6.5611
53.625
4.554
21.15
Amla
(%)
5
Marigold
(%)
5
K/S
L*
a*
b*
2.9932
59.741
3.697
18.686
10
4.0619
59.83
3.858
18.714
15
4.5883
64.118
3.319
20
4.7118
62.274
10
4.0555
61.247
10
10
10
15
4.2796
5.5623
10
20
15
15
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Mordant
Alum
Harda
TSC
Amla
Conc. (%)
Fastness Properties
Textiles and Light Industrial Science and Technology (TLIST) Volume 2 Issue 2, April 2013
Mordant
conc.
(%)
Marigold
conc.
20
62.25
60.80
20
45.05
44.75
20
20
90.30
86.75
20
63.98
62.58
20
20
90.20
87.25
20
62.20
61.75
20
20
89.75
87.10
20
60.80
60.10
20
20
88.65
86.25
Alum
Harda
TSC
Amla
Conclusions
Ecofriendly dyeing and antibacterial finishing of SPF
fabric was successfully carried out using natural
mordants and marigold dye. The dyed product
displayed good colour strength, although it was
distinctly lower than that in those obtained using
metal mordant like alum. The fastness properties were
however, comparable for both types of mordants. The
natural mordanted-dyed samples displayed broad
spectrum and durable antibacterial activity. The
marigold flower waste thus can be productively used
not only for dyeing of SPF fabric, but also to impart
antibacterial property. The replacement of metal
mordant by the newly found the natural mordents
TSC and Amla which individually contributes
towards antibacterial property, further showed
enhanced level in such property upon dyeing with
marigold. The concept of natural dyeing of SPF fabric
using natural mordant with an aim to produce gamut
of shades and at the same time the impartment of
antibacterial property seems to be indeed promising
one.
ACKNOWLEDGEMENT
Authors gratefully acknowledge University Grants
Commission (UGC- SAP) India for the research
fellowship.
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(%)
Bacterial Reduction
(%)
S.aureus
E. coli
Alum
Harda
TSC
Amla
Mordant
conc. (%)
20
20
20
20
Marigold
conc. (%)
20
20
20
20
No. of
Washes
Bacterial Reduction
(%)
S.aureus
E. coli
90.3
86.8
84.2
83.2
10
81.1
80.3
20
73.3
71.5
30
65.3
64.9
90.2
87.25
81.20
81.20
10
75.30
73.75
20
69.75
68.25
30
62.50
61.60
89.75
87.10
86.00
84.10
10
79.25
78.40
20
74.25
73.05
30
65.55
64.80
88.65
86.25
83.15
81.50
10
78.40
76.15
20
73.70
71.30
30
64.30
62.55
83
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Textiles and Light Industrial Science and Technology (TLIST) Volume 2 Issue 2, April 2013
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