DISEO FACTORIAL PARA TRES VARIABLES (K=3)

Niveles
VARIABLES
Inferior Superior
Z1: Grado de Molienda (% - 200M) 70 100
Z2: Tiempo de Cianuracin (Horas) 24 72
Z3: Cianuro de Sodio (PPM) 500 1000

MATRIZ DE DISEO EXPERIMENTAL (K=3)

ESCALA CODIFICADA ESCALA NATURAL

N X1 X2 X3 Z1 Z2
1 -1 -1 -1 70 24
2 1 -1 -1 100 24
3 -1 1 -1 70 72
4 1 1 -1 100 72
5 -1 -1 1 70 24
6 1 -1 1 100 24
7 -1 1 1 70 72
8 1 1 1 100 72
9 0 0 0 85 48
10 0 0 0 85 48
11 0 0 0 85 48

MATRIZ DE VARIABLES INDEPENDIENTES CODIFICADO

N X0 X1 X2 X3 X1*X2
1 1 -1 -1 -1 1
2 1 1 -1 -1 -1
3 1 -1 1 -1 -1
4 1 1 1 -1 1
5 1 -1 -1 1 1
6 1 1 -1 1 -1
7 1 -1 1 1 -1
8 1 1 1 1 1
9 0 0 0 0 0
10 0 0 0 0 0
11 0 0 0 0 0

CALCULO DE EFECTOS

X0 X1 X2 X3 X1*X2 X1*X3
656.5 -0.90 4.1 4.7 -1.7 0.9
-0.23 1.03 1.18 -0.43 0.22
0.10 2.10 2.76 0.36 0.10

ALGORITMO F. YATES
 METODO DE ALGORITMO DE YATES EFECTOS

1 81.50 162.70 325.90 656.50 164.13

X1 81.20 163.20 330.60 -0.90 -0.23
X2 81.90 163.50 -0.90 4.10 1.03
X1*X2 81.30 167.10 0.00 -1.70 -0.43
X3 81.40 -0.30 0.50 4.70 1.18
X1*X3 82.10 -0.60 3.60 0.90 0.22
X2 X3
*
83.90 0.70 -0.30 3.10 0.78
X1*X2*X3 83.20 -0.70 -1.40 -1.10 -0.27
Efectos

ANALISIS DE LA VARIANZA (ANAVA)

El clculo de la suma de cuadrados del error (SSE) se define por:

SSE= _(i=1)^n0(Yi-
Y0)2
Yi: Replicas en el punto central del diseo.
Y0: Promedio de todas las Replicas.
n0: Nmero de replicas en el centro del diseo.

La suma de los cuadrados para la curvatura esta dado por:

SSCurvatura = Nn0(Yi
-Y0) N+n0
Yi: Promedio de los puntos exteriores del diseo.

DETERMINACION DE SIGNIFICANCIA DE LAS VARIABLES

METODO DE W.G.COCHRAN
Fuente de SSEfectos Grados de Media de
F
Variacion Libertad Cuad.
X1 X1 0.101 1 0.101 1.08
X2 X2 2.101 1 2.101 22.51
X3 X3 2.761 1 2.761 29.58
X1*X2 X1*X2 0.361 1 0.361 3.87
X1*X3 X1*X3 0.101 1 0.101 1.08
X2*X3 X2*X3 1.201 1 1.201 12.87
X1*X2*X3 X1*X2*X3 0.151 1 0.151 1.62
SSCurvatura Curvatura 1.082 1 1.082 11.59
SSE Error 0.187 2 0.093
Total 8.047 10

MODELO MATEMATICO A ESCALA CODIFICADO

[B] = ([X]T[X])-1 * ([X]T[Y])

 [B] = ([X]T[X])-1 * ([X]T[Y])
([X]T[X])-1 = 1 / N
Coeficiente Codificado = [DIAGONAL] * ([X]T[Y])
N : Numero de Pruebas = 8

[DIAGONAL] ([X]T[X])-1
0.125 0 0 0 0 0
0 0.125 0 0 0 0
0 0 0.125 0 0 0
0 0 0 0.125 0 0
0 0 0 0 0.125 0
0 0 0 0 0 0.125
0 0 0 0 0 0
0 0 0 0 0 0

X0 X1 X2 X3 X1*X2 X1*X3
82.06 -0.11 0.51 -0.21 0.59 0.11

Y = 82.06 -0.11X1 + 0.51X2 - 0.21X3 + 0.59 X1 X2 +0.11X1 X3 + 0.39X

 Numero de Pruebas 8
Numero de Pruebas Centrales 3
Total de Pruebas 11 85
48
N=2k 8 8 750

ESCALA NATURAL Y
Z3 % Extrac. Au
500 81.5
500 81.2
500 81.9
500 81.3
1000 81.4
1000 82.1
1000 83.9
1000 83.2
750 83.1
750 82.5
750 82.7

X1*X3 X2*X3 X1*X2*X3 Y(Obs) X1

1 1 -1 81.50 -81.5
-1 1 1 81.20 81.2
1 -1 1 81.90 -81.9
-1 -1 -1 81.30 81.3
-1 -1 1 81.40 -81.4
1 -1 -1 82.10 82.1
-1 1 -1 83.90 -83.9
1 1 1 83.20 82.06 83.2
0 0 0 83.10 -0.9
0 0 0 82.50
0 0 0 82.70
82.77

X2*X3 X1*X2*X3
3.1 -1.1
0.78 -0.27 Exi
1.20 0.15 SS Efectos
 SS EFECTOS SS EFECTOS
(4TA COLUMNA) (5TA COLUMNA)
53874.03 3367.13
0.10 0.01
2.10 0.13 LEER NOTA
0.36 0.02
2.76 0.17
0.10 0.01
1.20 0.08
0.15 0.01
SS Efectos

Yi 82.06
Y0 82.77
SSE 0.187
SSCurvatura 1.082

RIABLES

Significancia

No
Si
Si
No
No
No
No
No

F al 95% 18.51

X])-1 * ([X]T[Y])
X])-1 * ([X]T[Y])
X])-1 = 1 / N
NAL] * ([X]T[Y])

)-1 [X]T[Y]
0 0 656.50
0 0 -0.90
0 0 4.10
0 0 -1.70
0 0 4.70
0 0 0.90
0.125 0 3.10
0 0.125 -1.10

X2*X3 X1*X2*X3
0.39 -0.14

.11X1 X3 + 0.39X2 X3 - 0.14X1 X2 X13

 X2 X3 X1*X2 X1*X3 X2*X3 X1*X2*X3
-81.5 -81.5 81.5 81.5 81.5 -81.5
-81.2 -81.2 -81.2 -81.2 81.2 81.2
81.9 -81.9 -81.9 81.9 -81.9 81.9
81.3 -81.3 81.3 -81.3 -81.3 -81.3
-81.4 81.4 81.4 -81.4 -81.4 81.4
-82.1 82.1 -82.1 82.1 -82.1 -82.1
83.9 83.9 -83.9 -83.9 83.9 -83.9
83.2 83.2 83.2 83.2 83.2 83.2
4.1 4.7 -1.7 0.9 3.1 -1.1
 NIVEL Centro de diseo
VARIABLES
inferior superior Z
Z1: Xantato z-11 (g/TM) 50 100 75
Z2: pH de la Pulpa 7 10 8.5

DISEO HEXAGONAL
CODIFICADO NATURAL
N
X1 X2 Z1
1 1 0 100.0
2 0.5 0.866 87.5
3 -0.5 0.866 62.5
4 -1 0 50.0
5 -0.5 -0.866 62.5
6 0.5 -0.866 87.5
7 0 0 75.0
8 0 0 75.0
1 0 0 75.0

CODIFICADO

MATRIZ [X]
N
Xo X1 X2
1 1 1.000 0.000
2 1 0.500 0.866
3 1 -0.500 0.866
4 1 -1.000 0.000
5 1 -0.500 -0.866
6 1 0.500 -0.866
7 1 0.000 0.000
8 1 0.000 0.000
9 1 0.000 0.000

TRANSPUESTA [
1 1 1
1 0.5 -0.5
0 0.866 0.866
1 0.250 0.250
0 0.750 0.750
0 0.433 -0.433

PRODUCTO DE LAS MATRICES ([X]^T)*[X]

9 0 0
0 3 0
0 0 2.999824
 3 0 0
2.999824 0 0
0 0 0

INVERSA DE LA MATRIZ (([X]^T)*[X])^-1 MATRIZ DE CORRE

0.333333 0.0 0.0
0.0 0.333333 0.0
0.0 0.0 0.333353
-0.333333 0.0 0.0
-0.333353 0.0 0.0
0.0 0.0 0.0

PRODUCTO ([X]^T)*[Y]
781.90
4.15
1.30
260.83
262.26
0.22

( ([X]^T) * [X] )^-1 * ([X]^T) * [Y]

86.27
1.38
0.43
0.43
1.40
0.29

MODELO MATEMATICO CO
Y = 86.27 1.38 X1
 DISEO HEXAGONAL

Radio de diseo
Z
25
1.5

AL
NATURAL
Y
Z2
8.50 87.7
9.80 89
9.80 86.6
8.50 85.7
7.20 86.1
7.20 88
8.50 86.6
8.50 86
8.50 86.2

DIFICADO

MATRIZ [X] VECTOR [Y]

X1^2 X2^2 X1X2 Y
1.00 0.00 0.00 87.7
0.25 0.75 0.43 89
0.25 0.75 -0.43 86.6
1.00 0.00 0.00 85.7
0.25 0.75 0.43 86.1
0.25 0.75 -0.43 88
0.00 0.00 0.00 86.6
0.00 0.00 0.00 86
0.00 0.00 0.00 86.2

TRANSPUESTA [X]^T
1 1 1 1 1 1
-1 -0.5 0.5 0 0 0
0 -0.866 -0.866 0 0 0
1 0.250 0.250 0 0 0
0 0.750 0.750 0 0 0
0 0.433 -0.433 0 0 0

TO DE LAS MATRICES ([X]^T)*[X]

3 2.999824 0
0 0 0
0 0 0
 2.25 0.749956 0
0.749956 2.249736008 0
0 0 0.749956

IZ (([X]^T)*[X])^-1 MATRIZ DE CORRELACION

-0.333333 -0.333353 0.0
0.0 0.0 0.0
0.0 0.0 0.0
0.833333 0.166676 0.0
0.166676 0.833431 0.0
0.0 0.0 1.333412

MODELO MATEMATICO CODIFICADO

0.43 X2 0.43 X1^2 1.40 X2^2 0.29
X1*X2