Datos obtenidos:

[INT TIC: VINPAE208.D\data.ms] Time= Thu Oct 27 10:31:27 2016

Peak R.T. Area % relativo Pct Max Pct Total Height
1 9.808 798397875 5.8209155 17.79 5.821 39092783
2 9.848 667303847 4.86514234 14.87 4.865 31297996
3 16.407 60879836 0.44385937 1.36 0.444 390973
4 20.18 7911544 0.05768105 0.18 0.058 144715
5 21.532 13965856 0.1018215 0.31 0.102 126727
6 23.916 2950010671 21.5077762 65.74 21.508 34292330
7 25.091 22976384 0.16751496 0.51 0.168 425562
8 25.598 27407632 0.19982206 0.61 0.2 471878
9 27.498 4487066038 32.7140553 100 32.714 40361763
10 28.067 11972862 0.08729109 0.27 0.087 153674
11 28.516 4096440541 29.8661043 91.29 29.866 43440559
12 29.129 1152271 0.00840091 0.03 0.008 53458
13 29.946 355734715 2.59357118 7.93 2.594 6193289
14 30.578 156094085 1.13804221 3.48 1.138 2887147
15 31.554 6965143 0.05078108 0.16 0.051 113169
16 31.741 17603171 0.12834023 0.39 0.128 289431
17 33.695 22522619 0.16420668 0.5 0.164 389687
18 36.887 11613900 0.08467399 0.26 0.085 146094
total 13716018990 100
[INT VINPAE208.D\TST1A.CH]
Time= Thu Oct 27 10:31:28 2016
Peak R.T. Area % relativo Pct Max Pct Total Height
1 0.251 75638911 3.68679197 99.52 3.687 945815
2 1.751 75914401 3.7002199 99.88 3.7 946848
3 3.251 75991267 3.7039665 99.98 3.704 947117
4 4.751 76003085 3.70454254 100 3.705 946838
5 6.251 76003087 3.70454263 100 3.705 946813
6 7.751 76003089 3.70454273 100 3.705 946773
7 9.251 76003092 3.70454288 100 3.705 946814
8 10.751 76003084 3.70454249 100 3.705 946844
9 12.251 76003085 3.70454254 100 3.705 946868
10 13.751 76003087 3.70454263 100 3.705 946883
11 15.251 76003078 3.70454219 100 3.705 946888
12 16.751 76003085 3.70454254 100 3.705 946889
13 18.251 76003088 3.70454268 100 3.705 946889
14 19.751 76003085 3.70454254 100 3.705 946877
15 21.251 76003087 3.70454263 100 3.705 946856
16 22.751 76003088 3.70454268 100 3.705 946833
17 24.251 76003082 3.70454239 100 3.705 946808
18 25.751 76003086 3.70454258 100 3.705 946781
19 27.251 76003085 3.70454254 100 3.705 946819
20 28.751 76003083 3.70454244 100 3.705 946847
21 30.251 76003083 3.70454244 100 3.705 946871
22 31.751 76003087 3.70454263 100 3.705 946884
23 33.251 76003088 3.70454268 100 3.705 946889
24 34.751 76003089 3.70454273 100 3.705 946889
25 36.251 76003083 3.70454244 100 3.705 946888
26 37.751 76003086 3.70454258 100 3.705 946874
27 39.251 76003084 3.70454249 100 3.705 946852
total 2051618635 100

Control de informacion:

Sample Inlet: GC

Injection Source: GC ALS

Mass Spectrometer: Enabled

 6890 GC METHOD
Horno:
Initial temp: 140 °C (On) Maximum temp: 240 °C
Initial time: 5.00 min Equilibration time: 0.50 min
Ramps:
# Rate Final temp Final time
1 4.00 240 10.00
2 0.0(Off)
Post temp: 0 'C
Post time: 0.00 min
Run time: 40.00 min
FRONT INLET (HP PTV)

Mode: Split
Initial temp: 250 °C (On)
Initial time: 0.00 min
Ramps:
# Rate Final temp Final time
1 0.0(Off)
Pressure: 42.44 psi (On)
Split ratio: 50:1

Split flow: 65.0 mL/min

Total flow: 69.0 mL/min

Gas saver: On

Saver flow: 20.0 mL/min

Saver time: 2.00 min

Gas type: Helium

COLUMN 1 COLUMN 2
Capillary Column (not installed)
Model Number: SUPELCO SP2560
Stat phase> biscyanopropylsiloxane
Max temperature: 240 °C
Nominal length: 100.0 m
 Nominal diameter: 250.00 um
Nominal film thickness: 0.20 um
Mode: constant pressure
Pressure: 42.44 psi
Nominal initial flow: 1.3 mL/min
Average velocity: 24 cm/sec
Inlet: Front Inlet
Outlet: MSD
Outlet pressure: vacuum

BACK DETECTOR (FID) FRONT DETECTOR (NO DET)

Temperature: 250 'C (Off)
Hydrogen flow: 40.0 mL/min (Off)
Air flow: 450.0 mL/min (Off)
Mode: Constant makeup flow
Makeup flow: 45.0 mL/min (Off)
Makeup Gas Type: Nitrogen
Flame: Off
Electrometer: Off
Lit offset: 2.0
GC Injector
Front Injector: Cantidad:
Sample Washes 2
Sample Pumps 6
Injection Volume 1.00 microliters
Syringe Size 10.0 microliters
PreInj Solvent A Washes 3
PreInj Solvent B Washes 0
PostInj Solvent A Washes 3
PostInj Solvent B Washes 0
Viscosity Delay 0 seconds
Plunger Speed Fast
PreInjection Dwell 0.00 minutes
PostInjection Dwell 0.00 minutes
Back Injector:
No parameters specified
Column 1 Inventory Number AB002
Column 2 Inventory Number