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This standard has been approved for use lry agencies of the Department of Defense.
Copyr¡ght @ ASTM lnternational, 100 Bail Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
6.4 Hydrogen Embrittlement Relief: 6.10 Packaglng-Part(s) plated for the U.S. Government
6.4.1 Heat treatment appropriate for the tensile strength of and Military, including subcontracts, shall be packaged in
the electroplated part (see Specification 8850) shall be per- accordance with Practice D3951.
formed to reduce the risk of hydrogen embrittlement. In all 7. Test Methods
cases, the duration of the heat treatment shall commence from
the time at which the whole part attains the specified tempera- 7.I Separate Specimens-When the coated articles are of
ture. See 6.3.1.1 for important embrittlement relief information such a form as not to be readily adaptable to a test specified
regarding the selection of ER-0. When no embrittlement relief herein, when destructive tests would unreasonably reduce the
treatment is specified by the purchaser then Class ER-1 shall be
number or pieces in small lots, when the pieces are too
valuable to be destroyed, and when specified by the purchaser,
applied.
tests shall be made by the use of separate specimens plated
6.4.2 Begin the embrittlement relief heat-treatment as soon
as practical following the plating process but no longer than 1.5
concurrently with the articles represented. The separate speci-
mens shall be of a basis metal equivalent to that of the articles
h.
6.4.3 Parts or representative specimens shall be tested for represented. Equivalent basis metal includes chemical
composition, grade, condition, and finish of surface prior to
compliance in accordance with 7.5.
electroplating. The purchaser is responsible for providing these
6.5 Thickness-The thickness of the coating everywhere on specimens (see section 5.3). These specimens shall be intro-
the significant surface(s) shall conform to the requirements of duced into a lot before the cleaning operations preliminary to
the specified class as defined in Section 3 (see 7.2). electroplating and shall not be separated therefrom until after
Nors 2-The coating thickness requirements of this specification are a completion of electroplating. Conditions affecting the electro-
minimum requirement, that is, the coating thickness is required to equal or plating of specimens, including the spacing and positioning in
exceed the specified thickness everywhere on the significant surfaces (see respect to anodes and to other objects being electroplated, shall
4.1). Variation in the coating thickness from point to point on a coated correspond as nearly as practicable to those affecting the
article is an inherent characteristic of electroplating processes. Therefore,
the coating thickness must exceed the specified value at some point on the
significant surfaces of the articles represented. Unless a need
significant surfaces to ensure that the thickness equals or exceeds the can be demonstrated, separately prepared specimens shall not
specified value at all points. Hence, in most cases, the average coating be used in place of production items for nondestructive tests
thickness on an article will be greater than the specified value; how much and visual examination.
greater is largely determined by the shape of the article (see Practice
B507) and the characte¡istics of the electroplating process. In addition, the 1.2 Thickness-Measure the thickness of the chromium by
average coating thickness on articles will vary from article to article one of the following methods; other methods may be used if it
within a production lot. Therefore, if all of the articles within a production can be demonstrated that the uncerlainty of the method is less
lot are to meet the thickness requirement, the average coating thickness for
than l0 7o or unless direct physical measurement by mechani-
the production lot as a whole will be greater than the average necessary to
ensure that a single article meets the requirement. This may not apply to cal means of the final part dimension is specified.
parts that are ground after plating. 7.2.1 Microscopical---Test Method 8487 (this method is
destructive).
6.6 Adhesion-The coating shall be sufficiently adherent to
the basis metal to pass the adhesion test specified (see 7.3). 7.2.2 Magnefic-Test Method 8499.
These tests are, with the possible exception of the heat quench
7.2.3 Coulometric---Te.st Method 8504 (this method de-
test, all destructive and therefore, in most cases, should be stroys the coating in the test location).
performed on test panels.
aMessler, R. W., and Maller, R. R., "A New Inspection Process for Detecting
Nore 3-Adhesion may be influenced by the method of pretreating the Abusive Grinding Damage in Hard Ch¡omium Plated Pafls," Proceedings of the
base metal and the type of steel used as a basis metal. Helpful information Airlíne Plating Symposium, 1974, is a helpful discussion of the problems in
is given in Practices 8177, 8183, 8242, andB320. grinding.
l.3.l.l Bend Test-This method is destructive. agreed upon between the purchaser and the seller.
7.3.1.2 File Test-This method is destructive. 8. Sampling Requirements
7.3.1.3 Heat and Quench Zesr-This method may affect the
heat treatment of the basis metal. 8.1 The use of statistical process control in the coating
7.3.1.4 Push Test-This method is destructive. process is strongly recommended. Properly performed, this
7.3.2 These and other adhesion tests are described in Test will help ensure coated products of satisfactory quality and will
Methods B571 . The test selected should take into consideration reduce the amount of acceptance inspection required.
the size, shape, or thickness of the part. Adhesion tests may at 8.2 The sampling plan shall be Test Method 8602 unless
times fail to detect adhesion in the process of degradation; otherwise specified by the purchaser. Other sampling plans are
subsequent fabrication may reveal poor or inadequate adhesion contained in Guide 8697 and Method 8762.
that shall be cause for rejection. 8.3 Select a random sample of the size required by the test
7.4 Porosity-The coating shall pass one of the following method selected from the inspection lot (see 8.2). Inspect the
tests as specified by the purchaser: articles in the lot for conformance to the requirements of this
specification and classify the lot as conforming or not conform-
Nors 4-It is important to realize that the test duration specified for
each test must be used exactly for valid results. ing to each requirement in accordance with the criteria of the
sampling plans in the method selected.
7.4.1 Fenoxyl Test-Conduct in accordance with the proce-
dure described in Appendix Xl. Observe the results after 10 Nors 5-Test Method 8602 contains four sampling plans, three of
min. The part fails if more than the number of pores specified which are to be used with nondestructive test methods. The fourth plan is
used where the test method is destructive. The three plans for nondestruc-
by the purchaser per part or per unit area are found. tive tests ditrer in the quality level they require of the product; Test
7.4.2 Neutral Salt Spray-Conduct in accordance with Prac- Method 8602 requires use of the plan with the intermediate quality level,
tice B I 17. Observe results after I 6 h. The part fails if more than unless the purchaser specifies otherwise. It is recommended that the
the number of pores specified by the purchaser per part or per purchaser compare the plans with his/her needs and state which plan is to
unit area are found. be used. If the plans in Test Method B602 do not serve those needs,
additional ones are given in Guide 8697. Both Test Method 8602 and
7.4.3 Copper Sulfate ksl-Immerse the coated part in a Guide B697 list references where additional information on sampling
15-g/L solution of copper sulfate (CuSO 5HrO) for 2 min. inspection and additional plans are given.
Inspect for copper spots that indicate pores. The part fails if Nore 6-When both destructive and nondestructive tests exist for the
more tha¡ the number of pores specified by the purchaser per measurement of a characteristic, the purchaser needs to state which is to
be used so that the proper sampling plan is selected. Whether or not a test
part or per unit area are found.
is desüuctive may not always be clear. A test may destroy the coating but
7.5 Hydrogen Embrittlemenf-Representative sample parts in a noncritical area, or, although it may destroy the coating, the part can
or test specimens (see 7.5.1) plated concurrently with the parts, be reclaimed by stripping and recoating. The purchaser needs to state
whether or not the test is to be considered destructive or nondestructive.
shall be subjected to a sustained load test. In the case of parts,
The decision is important because the plans for destructive tests are
the samples shall be subjected for 200 h to a sustained tensile significantly less able to discriminate between acceptable and unaccept-
load equal to ll5 Vo of the maximum design load for which the able lots. This is because fewer pafts are tested in destructive plans.
part was designed as specified by the purchaser. test If 8.4 An inspection lot shall be defined as a collection of
specimens are employed, they shall be subjected for 200 h to a ofthe same kind, that have been produced
coated parts that are
load equal to 75 Vo of the ultimate tensile strength of the alloy to the same specification, that have been coated by a single
employed. Any fractures or signs of cracks shall be cause for producer at the one time or approximately the same time under
reiection. essentially the same conditions, and that are submitted for
7.5.1 Separate specimens for embrittlement relief testing acceptance or rejection as a group.
shall be round notched specimens of the alloy being plated or
a metallurgically equivalent alternative specified by the pur- 8.5 All specimens used in the sampling plan shall be made
chaser. The specimens shall be prepared with the axis of the of the same basis material in the same metallurgical conditions
specimen perpendicular to the short traverse grain direction as the articles being plated to this specification.
and shall conform to Fig. 8 of Test Methods E8 and shall have 8.6 All specimens shall be provided by the purchaser unless
a 60 V-notch, the bottom of which shall have a radius of otherwise agreed upon by the producer.
curvature of 0.254 -r 0.0127 mm and the area of which shall be
approximately equal to half the area of the specimen's reduced 9. Keywords
section. 9.1 chromium plating standard; steel
(Nonmandatory Information)
Xl. FERROXYLTEST
X1.1 Scope---This method reveals discontinuities, such as remain undisturbed. (Do not apply the solution if its tempera-
pores, in coatings of chromium on iron or steel. ture is below 60'C.) Place the test specimen in a horizontal
position allowing it to cool to between 2l and 27"C. Begin
Xl.2 Material---The test solution is prepared by dissolving timing the 1O-min test period from the time the agar solution is
10 g of agar, l0 g of sodium chloride (NaCl), and I g of on the test specimen. At the end of the test period examine the
potassium ferricyanide (K Fe(CN)) in 1 L of warm distilled or coating or remove the filter paper and examine the aside that
deionized water. was in contact with the specimen. Blue spots indicate basis
metal corrosion or porosity.
X1.3 Procedure-Clean and degrease the surface to be
tested with methyl alcohol or other suitable solvent (avoid Xl.4 Report:
inhalation of fumes). Slowly warm the test solution to 93"C to Xl.4.l Report the following information:
liquify (a borosilicate glass double boiler arrangement is X1.4.1.1 Area of the surface tested,
suggested). Apply the warmed test solution to the speiimen by XI.4.1.2 Total number and diameter of all spots visible to
one of the following methods: (1) dip the specimen in the the unaided eye, and
solution, (2) pour the solution over the specimen, or (3) dip a X1.4.1.3 The highest number of spots visible at one time
piece of filter paper into the solution, allow the excess to drain through a template placed on the surface with a 25 by 25-mm
off, and then apply the wet paper to the test area and allow to opening.
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coPYRtGHTq.
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