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https://doi.org/10.1007/s10706-018-0544-5
ORIGINAL PAPER
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Geotech Geol Eng
also been found to be a successful technique (Hunter This paper presents, by comparison, the effect of fly
1988; Petry and Little 1992; Rollings et al. 1999; ash (FA) and rice husk ash (RHA) on some of the
Acosta et al. 2003; Hoyos et al. 2004; Phanikumar and index and engineering properties of a remoulded
Sharma 2004). Of the various additives used for expansive clay. Liquid limit (LL), plastic limit (PL),
stabilizing expansive soils, lime, fly ash (Chen 1988; plasticity index (PI) and free swell index (FSI) were
Rao 1984; Sankar 1989; Cokca 2001) and calcium the index properties studied at varying FA and RHA
chloride (Desai and Oza 1997) have shown promise as contents. And among the engineering properties,
they reduced the amount of heave and improved the compaction characteristics, hydraulic conductivity
strength characteristics. Lime exits in two forms such (k) and unconfined compressive strength (kPa) were
as quick lime (CaO) and hydrated lime (CaOH2). It is determined at varying FA and RHA contents.
quite effective in producing reactions such as floccu-
lation and cementation upon being added to clays.
Fly ash is extracted from the flue gases of a furnace 2 Experimental Investigation
fired with coal. The composition of fly ash varies with
the nature of the coal (Rollings and Rollings 1996). 2.1 Test Materials
Fly ash can be used for controlling expansion of
swelling soils because it is a pozzolanic material (Lee 2.1.1 Soil
et al. 2000; Shon et al. 2004). Because fly ash is a
pozzolanic material, it enhances the strength of The expansive soil used in this investigation had an
expansive clays (Joshi and Lohtia1997). Edil et al. FSI of 125%. Therefore, its degree of expansion may
(1987) found that fly ash could also be a potential be classified as ‘High’. Based on its plasticity char-
waste liner. An effective stabilizing agent, fly ash can acteristics, the soil can be classified as CH according
also be used as a base course material, a back fill to USCS. Table 1 shows some of the index and
material and an embankment material (Phanikumar engineering properties of the soil; Table 2 shows the
2000). Further, the use of fly ash in bulk quantities in chemical composition of the soil.
civil engineering infrastructure can ward off its
hazardous effects on environment (Malhotra and 2.1.2 Fly Ash (FA)
Mehta 1996; Dobrowolski 1998).
Rice-husk ash (RHA) is obtained from the burning The fly ash used in the experimental programme was
of rice husk, which is the by-product of rice milling. It collected from the National Thermal Power Corpora-
was estimated that 1000 kg of rice grain produced tion, Visakhapatnam, India. Table 1 shows some of
200 kg of rice husk. On burning rice husk, about 20% the index and engineering properties of the fly ash, and
or 40 kg would become RHA (Mehta 1986). RHA Table 2 shows its chemical composition. The OMC
contains a high amount of SiO2 in amorphous form and MDD of the fly ash were 21% and 12.8 kN/m3
(Mehta 1986; Gambhir 1995), which makes it poz- respectively.
zolanic according to ASTM C 168 (ASTM 1997).
Hence, RHA can be used in lime-pozzolana mixes and 2.1.3 Rice Husk Ash (RHA)
Portland cement replacement (Paya et al. 2001).
Pozzolana is a siliceous or siliceous and aluminous RHA used in this investigation was passed through
material by composition according to ASTM C 168 425 lm for convenient mixing with clay and com-
(ASTM 1997) and has no cementing property by itself. paction. As RHA particles have a high external surface
However, when pozzolana has high fineness, it can area, particles finer than 425 lm could result in non-
react with CaOH2 in the presence of water to provide uniform mixing. Hence, the RHA particle size was
cementing property. Further, research showed that limited to 425 lm in the blends. Some of the index and
RHA can be mixed with CaOH2 to produce a engineering properties of RHA are shown in Table 1.
cementing material. RHA can effectively stabilize Table 2 shows the chemical composition of RHA.
expansive soils either solely or mixed with lime
(Basha et al. 2003).
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Table 1 Index and engineering properties of soil, fly ash (FA) and rice husk ash (RHA)
Property Soil Fly ash Rice husk ash Standard designation
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2.3.2 Free Swell Index (FSI) respective OMC and MDD using cylindrical samples
(38 mm in diameter and 76 mm in length) by
Free swell index (FSI) was determined according to conducting unconfined compression tests. The effect
ASTM D5890-02. Oven-dried expansive clay passing of curing period was also studied by curing the
through 425 lm sieve was used for performing the FSI samples for 0, 7 and 28-days.
tests. The reference liquid used in the tests was
kerosene. Ten grams of oven-dried expansive clay 2.3.6 Swelling Pressure (ps)
passing 425 lm sieve were poured into two 100 ml
cylindrical jars containing kerosene and deionized The swelling pressure (ps) of the unblended soil and
water. The jars were made to stand for 24 h and then the soil blended with fly ash and RHA as per their
the volumes of the soil in the jars containing kerosene dosages was determined in a cylindrical mould at their
(Vk) and deionized water (Vw) were noted. Free swell respective OMC and MDD. The soil sample (or the
index (FSI) is defined as the ratio of difference in blend sample as the case may be) compacted in a
volumes of soil in water and kerosene to the volume of cylindrical mould which was soaked in water after
soil in kerosene expressed as a percentage (Holtz and compaction underwent swell, and as it swelled, the
Gibbs 1956). It is written as. vertical swelling pressure was measured with the help
Vw Vk of a proving ring. The soil used in the swelling
FSI ¼ 100 ð1Þ pressure tests was also passed through 4.75 mm sieve.
Vk
In the case of FSI tests on expansive clay blended
with fly ash and RHA, the oven-dry expansive clay 3 Discussion of Test Results
powder was replaced by the required amounts of fly
ash and RHA based on their dosages mentioned above, 3.1 General Observations
and FSI tests were performed on the blends as
explained above. A lot of research has been done and is being done on
chemically modified expansive clays with a view to
2.3.3 Proctor Compaction studying the physical and engineering properties of the
clay-chemical blends at both laboratory and field
Proctor compaction tests were performed according to scales. There are various chemicals the effect of which
ASTM 2000, D698a. The FA-clay blends and RHA- on clays in general emphasizing strength characteris-
clay blends for the compaction tests were prepared tics and on expansive clays in particular focusing on
based on the dosages of RHA and fly ash mentioned volume changes has been explored. So, a comparison
above using air-dried soil passing 4.75 mm sieve and drawing the attention of the scientific community to
replacing the soil with the respective dosages of the the depth and range of influence of different chemicals
additives by dry weight of the soil. on the above aspects is inevitable in such studies. By
way of comparison, this research sheds light on the
2.3.4 Hydraulic Conductivity (k) effect of fly ash (FA) and rice husk ash (RHA) on some
of the index and engineering properties of a remoulded
The hydraulic conductivity (k) of the unblended soil expansive clay. Both FA and RHA, as additives, have
and the soil blended with fly ash and RHA as per their a few striking similarities, a factor that necessitates an
dosages was determined at their respective OMC and attempt to compare the way they can influence some of
MDD according to the variable head permeameter the significant index and engineering properties of
method conforming to ASTM D2434. expansive clays. They both are very light materials
with a low specific gravity; and both are highly
2.3.5 Unconfined Compression Test siliceous materials, the amount of silica being higher
in RHA compared to FA. With a considerable
Undrained shear strength (ASTM 2000, D2166) of the potential for producing effects such as flocculation
unblended soil and the soil blended with fly ash and on clays, both FA and RHA, based on their dosages,
RHA based on their dosages was determined at their can result in reduced liquid limit (LL), plasticity index
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(PI) and free swell index (FSI), which are extremely PL increased by 16% when FA content increased from
important index properties of expansive clays. They 0 to 30%. Plasticity index (PI), which is a numerical
can also effectively influence compaction character- difference between LL and PL, also significantly
istics, hydraulic conductivity (k) and unconfined decreased when FA content increased. PI decreased
compressive strength (kPa) among the engineering from 55 to 10.5% when FA content increased from 0 to
properties of expansive clays. Hence, this comparative 30%, indicating negligible plasticity.
study on the effect of FA and RHA—two very light, Figure 2 shows the variation of LL, PL and PI with
siliceous materials—on the behavior of expansive RHA content. LL decreased from 84 to 28% when
clays throws new light on and adds to what has been RHA content increased from 0 to 30%, indicating a
done so far. reduction of 64%. The reduction in LL by a huge
amount can be attributed more to the replacement of
3.2 Effect of Fly Ash (FA) and Rice Husk Ash expansive clay by RHA particles than to RHA causing
(RHA) on Index Properties flocculation, though it is pozzolanic. As RHA is of a
very low specific gravity (G = 0.7), more number of
Figure 1 shows the variation of liquid limit (LL), RHA particles replace the original expansive soil for a
plastic limit (PL) and plasticity index (PI) with fly ash given dosage. For the same reason, at 30% additive
content. LL decreased significantly with increase in fly content, LL decreased more in the case of RHA than
ash content. For example, LL decreased from 84 to FA. Flocculation caused by RHA increased PL by
44% when FA content increased from 0% to 30%, 21% when RHA increased from 0 to 30%. PI
showing a reduction of 48%. When expansive clay decreased from 55% to an extent that it was non-
particles are replaced by silt-sized fly ash particles, the plastic (NP).
water content required for rendering the blend fluidy Free swell index (FSI) is an important parameter in
(having liquid consistency) decreases. Hence, LL the case of expansive soils. Phanikumar (1997) and
decreases. Further, fly ash, being pozzolanic, induces Phanikumar (2006) suggested that FSI could be used
flocculation because of which the size of the blend as an index property of expansive soils because (1)
particles increases, which is also a reason for water swelling characteristics could be predicted by FSI (2)
content required for rendering the blend fluidy FSI is also determined on soil fraction passing 425 lm
decreasing. The figure also shows that PL increased sieve, and (3) FSI directly indicates the potential
slightly, which could also be attributed to flocculation. expansiveness of a clay. Figure 3 shows, by compar-
60
50
40
30
20
10
0
0 5 10 15 20 25 30 35
Fly ash content (%)
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Geotech Geol Eng
40
30
20
10
0
0 5 10 15 20 25 30 35
Rice husk ash content (%)
80
FSI (%)
60
40
20
0
0 5 10 15 20 25 30 35
Additive content (%)
ison, the variation of FSI with FA content and RHA both replacement of expansive clay particles by FA
content. FSI decreased from 125 to 35% when FA and RHA and also to flocculation they caused. Table 3
content increased from 0 to 30% indicating a reduction summarises the values of FSI, LL, PL and PI
of 72%; and FSI decreased from 125 to 20% when corresponding to varying quantities of fly ash and rice
RHA content increased from 0 to 30% indicating a husk ash.
reduction of 84%. The reduction in FSI with increase
in FA content and RHA content can be attributed to
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Table 3 Effect of fly ash Liquid limit, LL (%) Plastic limit, PL (%) Plasticity index, PI (%) FSI (%)
(FA) and rice husk ash
(RHA) on index properties Fly ash content (%)
0 84 29 55 125
5 79 30.5 49.5 118
10 74 31 43 100
15 68 31.5 36.5 85
20 62 32.5 29.5 70
25 54 33 21 50
30 44 33.5 10.5 35
Rice husk ash content (%)
0 84 29 55 125
5 80 30 50 108
10 73 31 42 92
15 66 32 34 75
20 52 34 18 60
25 40 35 5 45
30 28 NP NP 20
13
12
10 15 20 25 30 35
Water content (%)
3.3 Effect of Fly Ash (FA) and Rice Husk Ash towards left with increasing FA content. This means
(RHA) on Engineering Properties that the maximum dry density (MDD) and the
optimum moisture content (OMC) decreased with
3.3.1 Compaction Characteristics increase in fly ash content. As fly ash, a light weight
material, replaced the expansive clay in the blends, the
Figure 4 shows the Proctor compaction curves for the weight of the compacted cakes of FA-clay blends in
unblended soil and the soil blended with varying fly the Proctor mould decreased. Hence, the MDDs
ash contents (10, 20 and 30%). The data indicate that decreased. Further, the amount of water required to
the Proctor compaction curves shifted downwards and result in MDD (which is nothing but OMC) would be
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Geotech Geol Eng
less in FA-clay blends of higher FA contents because 3.3.2 Hydraulic Conductivity (k)
more number of clay particles (requiring larger
amount of water for MDDs) would be replaced by As already mentioned, hydraulic conductivity (k) of
fly ash. Hence, OMCs also decreased with increasing FA-clay blends and RHA-clay blends was determined
FA content. For example, the MDD was 15.5, 15.1, at the respective OMC and MDD of the blends.
14.5 and 13.9 kN/m3 for the FA contents of 0, 10, 20 Figure 6 shows, by comparison, the variation of
and 30% respectively. Similarly, the OMC was 25, hydraulic conductivity with FA content and RHA
24.2, 23.6 and 23% respectively for the FA contents of content. The hydraulic conductivity of both FA-clay
0, 10, 20 and 30%. blends and RHA-clay blends increased with increase
Figure 5 shows the Proctor compaction curves for in additive content. However, for a given additive
the unblended soil and the soil blended with varying content, the hydraulic conductivity of RHA-clay
RHA contents (10, 20 and 30%). Proctor compaction blends was higher than that of FA-clay blends. The
curves shifted downwards and towards right with hydraulic conductivity of FA-clay blends increased
increasing RHA content, which means that the MDD with increase in FA content because the MDD of the
decreased but the OMC increased with increasing blends decreased with increased FA content (see
RHA content. As RHA, a very light material, replaced Fig. 4). As MDD decreased with FA content, the void
the expansive clay in the blends, the weights of the ratio (e) or void space of the compacted blends
compacted cakes of RHA-clay blends in the Proctor increased. Hence, the hydraulic conductivity
mould decreased. Hence, the MDDs decreased. More- increased with FA content. The hydraulic conductivity
over, RHA absorbs water and increases the water- of RHA-clay blends also increased with increase in
voids ratio in the RHA-clay blends. This phenomenon RHA content because of the reasons mentioned above
becomes more predominant at higher RHA contents. (see Fig. 5). However, the higher hydraulic conduc-
Hence, the OMCs increased with increasing RHA tivity of RHA-clay blends compared to that of FA-clay
content. For example, the MDD was 15.5, 14.7, 14 and blends for a given additive content can be attributed to
13.2 kN/m3 for the RHA contents of 0, 10, 20 and 30% their MDDs being lower than the MDDs of FA-clay
respectively. Similarly, the OMC was 25, 26.2, 27.8 blends (see Figs. 4 and 5) and also to the higher water
and 29.4% respectively for the RHA contents of 0, 10, void ratios at higher RHA contents as indicated by
20 and 30%. increasing OMCs (see Fig. 5). For example, the
hydraulic conductivity of FA-clay blends increased
from 4.6 9 10-7 to 1.8 9 10-6 cm/s and that of
20% RHA
14
30% RHA
13
12
11
10 15 20 25 30 35 40
Water content (%)
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RHA
4.00E-06
k (cm/sec)
3.00E-06
2.00E-06
1.00E-06
0.00E+00
0 5 10 15 20 25 30 35 40
Additive content (%)
RHA-clay blends increased from 4.6 9 10-7 to reduction in MDD with increasing FA content and
5.5 9 10-6 cm/s when the additive content increased RHA content (see Figs. 4 and 5). However, UCS
from 0 to 30%. increased with increase in FA content when the curing
period increased to 7 and 28-days. Further, for a given
3.3.3 Unconfined Compressive Strength additive content, the UCS for 28-days was higher than
that for 7-days. This can be attributed to increased
Figures 7 and 8 respectively show the variation of pozzolanic reaction with increasing additive content
UCS with fly ash content and RHA content for the and curing period. It may, however, be observed that,
curing periods of 0, 7 and 28-days. At 0-days curing, for a given additive content, the UCS for FA-clay
UCS decreased slightly with increasing FA content blends was higher than that for RHA-clay blends.
and RHA content. This can be attributed to the
7-days
400
strength (kPa)
28-days
300
200
100
0
0 5 10 15 20 25 30 35 40
Fly ash content (%)
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Unconfined compressive
300
7-days
strength (kPa)
250
28-days
200
150
100
50
0
0 5 10 15 20 25 30 35 40
Rice husk ash content (%)
Fly ash
100
Swelling pressure (kPa)
80
RHA
60
40
20
0
0 10 20 30 40 50
Additive (%)
3.3.4 Swelling Pressure 30%. This can be attributed to reduced MDDs of both
the types of blends with increasing additive content.
Figure 9 shows, by comparison, the variation of Table 4 summarises the values of OMC, MDD,
swelling pressure (kPa) with FA content and RHA swelling pressure (ps), hydraulic conductivity (k) un-
content. The swelling pressure of both FA-clay blends confined compressing strength (for different curing
and RHA-clay blends decreased significantly with FA periods) corresponding to varying quantities of fly ash
and RHA contents. For example, the swelling pressure and rice husk ash. Table 4 summarises the engineering
decreased from 120 to 20 kPa and 120 to 30 kPa properties of the expansive clay corresponding to
respectively for FA-clay blends and RHA-clay blends varying quantities of fly ash and rice husk ash.
when the FA and RHA contents increased from 0 to
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