C184-E013B

OCI/PTV-2010
Shimadzu
Sample Injection Unit for On-Column Analysis

Residual Pesticide Analysis System

Shimadzu Gas Chromatograph GC-2010 Series

One System Meets Versatile Analysis Requirements for Residual Pesticides in Food
Features
The management and quality T h ree select ive det ect ors can be inst alled
checks of ingredients are critical
factors in ensuring food safety. Select detectors suitable for target pesticide components. Available detectors include an ECD for
The Food Sanitation Law chlorinated pesticides, FTD for nitric and organophosphorus pesticides and FPD for sulfuric and
stipulates methods for analyzing organophosphorus pesticides. It is also possible to mount an ECD, FTD and FPD at the same time.

residual pesticides in foods for

individual agricultural, livestock
and fishery products, as well as
for individual pesticide
components.
Detector temperatures conform to official methods
Some pesticides' components are designated to be analyzed at the maximum detector
temperature of 300°C as specified by the Food Sanitation Law. The GC-2010's FPD and FTD
are designed with heat resistance that meets this requirement (FPD: 350°C and FTD: 450°C).

The Shimadzu gas chromatograph

GC-2010 Series, provided with a
wide range of options for sample
injection units and detectors,
enables accurate and quick
analysis of target pesticide
On-column analysis for thermally labile components
Use the on-column analysis sample injection unit for the analysis of pesticide
components, such as DEP (trichlorfon) and endrin, which easily decompose with heat
processing. It is also possible to use a capillary column with a small internal diameter
without the press-tight connector.

components in accordance with

regulations.
D u al analysis for mult i- sample analysis
Two samples can be analyzed in parallel by configuring a dual injection system
incorporating two sample injection units and two detectors.
 Analysis example of 0.1ppm nitric pesticide using FTD Analysis example of 0.1ppm phosphorus pesticide using FPD

Salithion
Chinomethionat
Pendimethalin
Thiobencarb Diethofencarb

Chlorpyrifos Malathion
Dichlorvos
Isoprocarb

Pyridaphenthion
Diazinon
Methyl Parathion
Esprocarb
Chlorpropham

Fenitrothion

Isoxathion
Prothiofos
Dimethoate

EPN
Pretilachlor

Mepronil
Analysis conditions Analysis conditions
Column: 5% diphenyl, 95% dimethyl polysiloxane, 0.25mm x 30m, 0.25μ Column: dimethyl polysiloxane 0.53mm x 15m, 1.5μ
Carrier gas: He 45cm/s (constant linear velocity mode) Carrier gas: He 130cm/s (constant linear velocity mode)
Column oven: 80°C (1min) - 10°C /min - 2°C - 5°C /min - 250°C Column oven: 80°C (1min) - 8°C /min - 250°C
Sample injection unit: Split / splitless (high-pressure splitless mode 1min) 250°C Sample injection unit: split/splitless (high-pressure splitless mode 0.5min) 230°C
Detector: FTD H2 1.5mL/min, Air 140mL/min, makeup (He) 25mL/min 0.5pA 280°C Detector: FPD (P mode) H2 80mL/min, Air 20mL/min 260°C

OCI/PTV-2010 quick on-column injection GC-2010 Series Dual Injection System

Connection of the 0.32mm-diameter column

Full-volume sample injection

is possible regardless of the
column's internal diameter.
Column connection is easy
because a press-tight
connector is not used.
High-resolution
0.53mm
guard column chromatograms can be
obtained for thermally labile
samples.
Quick OCI Standard syringes can be
insert
used, eliminating the need to
procure special syringes. Select any type of sample injection unit and detector. It is possible to
Press tight
connector
mount both the same and different types of injection units and detectors.
0.32mm 0.32mm When mounting the same type of detectors, two samples can be
column column
analyzed in parallel.
When mounting different types of detectors, different groups of
Conventional method: Quick OCI method: components in a sample can be analyzed in parallel (sample needs to
OCI syringe general syringe be put into two vials ).

Founded in 1875, Shimadzu Corporation, a leader in the

development of advanced technologies, has a distinguished
history of innovation built on the foundation of contributing to
society through science and technology. We maintain a global
network of sales, service, technical support and applications
centers on six continents, and have established long-term JQA-0376
relationships with a host of highly trained distributors located
in over 100 countries. For information about Shimadzu, and to
contact your local office, please visit our Web site at
www.shimadzu.com

SHIMADZU CORPORATION. International Marketing Division

3. Kanda-Nishikicho 1-chome, Chiyoda-ku, Tokyo 101-8448, Japan
Phone: 81(3)3219-5641 Fax. 81(3)3219-5710
URL http://www.shimadzu.com The contents of this brochure are subject to change without notice.

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