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1 AS 2365.1.

1—1990

Australian Standard
Methods for the sampling and analysis of
indoor air

Method 1.1: Determination of nitrogen


dioxide—Spectrophotometric method—
Treated mesh/passive tube sampling
procedure
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PREFACE

This Standard was prepared by the Standards Australia Committee on Methods for
Examination of Air under the direction of the Chemical Standards Board.

CONTENTS
Page
1 SCOPE . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ... .. .. .. . 1
2 APPLICATION . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ..... .... . 1
3 REFERENCED DOCUMENTS . . . . . . . . . . . . . . . . . . . .. ... ..... 2
4 PRINCIPLE . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. . . .... 2
5 DEFINITION . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ..... .. . .. 2
6 REAGENTS AND MATERIALS . . . . . . . . . . . . . . . . . . ... .. ..... 2
7 APPARATUS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ..... ... .. 2
8 PREPARATION OF PASSIVE SAMPLING TUBE . . . . . . ... . . .... 3
9 SAMPLING . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ..... ..... 3
10 PROCEDURE . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ..... ... .. 3
11 CALCULATION AND EXPRESSION OF RESULTS . . . . .. .. . .. .. 4
12 PRECISION . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ..... .. ... 4
13 TEST REPORT . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ..... .... . 4
14 BIBLIOGRAPHY . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ... .. ..... 5

METHOD

1 SCOPE. This Standard sets out a spectrophotometric method for the


determination of nitrogen dioxide in indoor air using a passive tube sampling
technique. This method is applicable to indoor air in which the expected nitrogen
dioxide concentration is within the range 0 to 30 p.p.m. by volume (0 to 6 000 µg/m3 )
for an exposure time of 1 h, and has a detection limit of 0.06 p.p.m. for a 4 h sampling
period.
2 APPLICATION. The sampling procedure specified is not recommended for
sampler exposure times of less than 4 h. The sampling procedure gives best results for
exposure times of between 4 h and 7 days.
Passive sampling tubes exhibit collection rates which are dependent only on the
dimensions of the tube used to form the diffusion-controlling region in front of the
absorbing screens. The agreement between the theoretically determined rate and that
observed in practice is within 3%. If an increased sensitivity is required, the passive
sampling badge procedure described in AS 2365.1.2 should be used. The sampling
procedure specified is not suitable for indoor air that falls below 0°C.

COPYRIGHT
This is a free preview. Purchase the entire publication at the link below:

AS 2365.1.1-1990, Methods for the sampling and


analysis of indoor air Determination of nitrogen
dioxide - Spectrophotometric method - Treated
This is a free 1 page sample. Access the full version at http://infostore.saiglobal.com.

mesh/passive tube sampling procedures

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