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CONTENTS
Bragg`s Law
X-ray Powder Diffraction
X-ray Powder Diffractometer
X-ray diffraction
When a beam of X-ray radiation is incident upon a
substance, the electrons constituting the atoms of
the substance become as small oscillators.
When
certain
geometric
requirements
are
met,
X-rays
scattered from a crystalline solid can
constructively interfere, producing a
diffracted beam.
Braggs law
Above figure shows a monochromatic beam of Xrays incident on the surface of a crystal at an
angle .
Laue
Rotating Crystal
Powder
Orientation
Single Crystal
Polychromatic Beam
Fixed Angle
Lattice constant
Single Crystal
Monochromatic Beam
Variable Angle
Lattice Parameters
Polycrystal (powdered)
Monochromatic Beam
Variable Angle
POWDER
DIFFRACTOMETER
Application of XRD
XRD is a nondestructive technique. Some of
the uses of x-ray diffraction are;
4.
5.
6.
1.
2.
3.
REFERENCES
Instrumental Methods of Chemical
Analysis by Gurdeep R. Chatwal and
Sham K. Anand.
X-Ray METHODS BY Clive Whiston.
Internet source.
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